Salicyluric acid, tris(trimethylsilyl)- deriv.
- Formula: C18H33NO4Si3
- Molecular weight: 411.7154
- IUPAC Standard InChI: InChI=1S/C18H33NO4Si3/c1-24(2,3)21-16-13-11-10-12-15(16)18(23-26(7,8)9)19-14-17(20)22-25(4,5)6/h10-13H,14H2,1-9H3
- IUPAC Standard InChIKey: JBFNXVAKDSIUSE-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Hippuric acid, 2-hydroxy, TMS, #1; o-Hydroxyhippuric acid, tri-TMS; o-hydroxyhippuric acid, TMS (III)
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-1 | 1954. | Butts, 1972 | He, Chromosorb W HP (80-100 mesh), 10. K/min; Column length: 2. m; Tstart: 100. C; Tend: 325. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Packed | OV-101 | 1909. | Tanaka and Hine, 1982 | Program: not specified |
References
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Tanaka and Hine, 1982
Tanaka, K.; Hine, D.G.,
Compilation of Gas Chromatographic Retention Indices of 163 Metabolically Important Organic Acids, and Their Use in Detection of Patients with Organic Acidurias,
J. Chromatogr., 1982, 239, 301-322, https://doi.org/10.1016/S0021-9673(00)81990-1
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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