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11-Deoxycortisol, bis(trimethylsilyl) ether, bis(O-methyloxime)


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1250.3070.Baillie, Brooks, et al., 1972N2, Gas Chrom Q (100-120 mesh); Column length: 2. m

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryZB-13124.Ebner, Corol, et al., 200630. m/0.25 mm/0.25 «mu»m, He; Program: 70C(5min) => 20C/min => 220C(0.33min) => 5C/min => 315C (4min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Baillie, Brooks, et al., 1972
Baillie, T.A.; Brooks, C.J.W.; Middleditch, B.S., Comparison of Corticosteroid Derivatives by Gas-Chromatography-Mass Spectrometry, Anal. Chem., 1972, 44, 1, 30-37, https://doi.org/10.1021/ac60309a016 . [all data]

Ebner, Corol, et al., 2006
Ebner, M.J.; Corol, D.I.; Havlíková, H.; Honour, J.W.; Fry, J.P., Identification of neuroactive steroids and their precursors and metabolites in adult male rat brain, Endocrinology, 2006, 147, 1, 179-190, https://doi.org/10.1210/en.2005-1065 . [all data]


Notes

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