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Etiocholanolone, MO TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-30221.2492.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm
CapillarySE-30231.2504.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm
CapillarySE-30241.2522.Mitra, 1982N2; Column length: 30. m; Column diameter: 0.25 mm
CapillaryOV-1255.2575.Luyten and Rutten, 1974He; Column length: 20. m; Column diameter: 0.25 mm

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
PackedOV-1012540.Hurter and van Ree, 1979Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C
PackedSE-302539.Hurter and van Ree, 1979Gas-Chrom P (80-100 mesh), 1. K/min; Column length: 3.6 m; Tstart: 180. C
PackedOV-12522.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C
CapillaryOV-12544.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 220. C
CapillarySE-302545.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 200. C
PackedSE-302522.Luyten and Rutten, 1974He, 1. K/min; Column length: 20. m; Column diameter: 0.25 mm; Tstart: 180. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-12554.Hähnel, Wilkinson, et al., 1985He; Column length: 25. m; Column diameter: 0.3 mm; Program: 40C (1min) => 20C/min => 200C => 2C/min => 300C (11min)

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryOV-101240.2568.Krupcik, Rutten, et al., 1976Column length: 30. m; Column diameter: 0.25 mm
CapillaryOV-101251.2579.Krupcik, Rutten, et al., 1976Column length: 30. m; Column diameter: 0.25 mm

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mitra, 1982
Mitra, G.D., Determination of precise retention indices of steroids using an all-glass solid injection system, J. Chromatogr., 1982, 234, 1, 214-217, https://doi.org/10.1016/S0021-9673(00)81795-1 . [all data]

Luyten and Rutten, 1974
Luyten, J.A.; Rutten, G.A.F.M., Analysis of Steroids by High-Resolution Gas-Liquid Chromatography. II. Application to Urinary Samples, J. Chromatogr., 1974, 91, 393-406, https://doi.org/10.1016/S0021-9673(01)97918-X . [all data]

Hurter and van Ree, 1979
Hurter, P.; van Ree, T., Programmed-Temperature Gas Chromatography on Mixed Phases. Separation of Steroid Derivatives on Binary Mixtures, J. Chromatogr., 1979, 169, 93-100, https://doi.org/10.1016/0021-9673(75)85034-5 . [all data]

Hähnel, Wilkinson, et al., 1985
Hähnel, E.; Wilkinson, S.P.; Hähnel, R., Urinary steroid profiles in pregnancy by capillary column gas chromatography, Clin. Chim. Acta, 1985, 151, 3, 259-271, https://doi.org/10.1016/0009-8981(85)90089-0 . [all data]

Krupcik, Rutten, et al., 1976
Krupcik, J.; Rutten, G.A.F.M.; Rijks, J.A., The influence of temperature on the separation and characterization of steroids on non-polar glass capillary columns, Chem. zvesti, 1976, 30, 4, 469-479. [all data]


Notes

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