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GA44, Me-TMS


Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1HP-1DB-5
Column length (m) 30.30.12.12.15.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (mum) 0.250.25   
Program 60C (1min) => 15C/min => 200C => 5C/min => 285C60C (1min) => 15C/min => 200C => 5C/min => 285C60C(0.5min) => 20C/min => 200C => 5C/min => 300C60C(0.5min) => 20C/min => 200C => 5C/min => 300C60C(0.5min) => 20C/min => 200C => 5C/min => 300C
I 2789.2789.2795.2796.2821.
ReferenceKim, Lee, et al., 2003Kim, Lee, et al., 2003Pearce, Hutt, et al., 2002Pearce, Hutt, et al., 2002Pearce, Hutt, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-1OV-1OV-1OV-1
Column length (m) 15.25.25.25.25.
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.250.20.20.20.2
Phase thickness (mum)    0.250.25
Program 60C(0.5min) => 20C/min => 200C => 5C/min => 300C60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)60C(2min) => 10C/min => 150C => 3C/min => 300C
I 2826.2791.2803.2786.2786.
ReferencePearce, Hutt, et al., 2002Kobayashi, MacMillan, et al., 2000Kobayashi, MacMillan, et al., 2000Davis, Kobayashi, et al., 1999Webb, Appleford, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1DB-1CP Sil 5 CBCP Sil 5 CB
Column length (m) 25.25.30.30.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.20.20.250.250.25
Phase thickness (mum) 0.10.1 0.40.4
Program 60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C40C (2min) => 10C/min => 150C => 3C/min => 300C200C => 25C/min => 250C => 4C/min => 280C(4min)200C => 25C/min => 250C => 4C/min => 280C(4min)
I 2805.2805.2793.2786.2788.
ReferenceWebb, Appleford, et al., 1998Webb, Appleford, et al., 1998Grünzweig, Rabinowitch, et al., 1997Kappers, Jordi, et al., 1997Kappers, Jordi, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1OV-1OV-1DB-1DB-1
Column length (m) 25.25.25.15.15.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.20.20.20.250.25
Phase thickness (mum) 0.250.250.250.250.25
Program 50C(2min) => 10C/min => 150C => 3C/min => 300C50C(2min) => 10C/min => 150C => 3C/min => 300C50C(2min) => 10C/min => 150C => 3C/min => 300C60C(1min) => 20C/min => 200C => 4C/min => 260C60C(1min) => 20C/min => 200C => 4C/min => 260C
I 2800.2801.2802.2781.2781.
ReferenceKobayashi, Spray, et al., 1996Kobayashi, Spray, et al., 1996Kobayashi, Spray, et al., 1996Ridoutt, Pharis, et al., 1995Ridoutt, Pharis, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBCP Sil 5 CBSE-52SE-52
Column length (m) 15.25.25.25.25.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.220.22
Phase thickness (mum) 0.25  0.250.25
Program 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min60C(0.3min) => 20C/min => 220C => 4C/min => 300C60C(0.3min) => 20C/min => 220C => 4C/min => 300C50C => 15C/min => 240C => 4C/min => 300C50C => 15C/min => 240C => 4C/min => 300C
I 2800.2831.2833.2778.2778.
ReferencePearce, Koshioka, et al., 1994Taylor, Blake, et al., 1994Taylor, Blake, et al., 1994Hedden, Hoad, et al., 1993Hedden, Hoad, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase SPB-1SPB-1OV-1
Column length (m) 30.30. 
Carrier gas HeHeHe
Substrate    
Column diameter (mm) 0.250.25 
Phase thickness (mum) 0.250.25 
Program 60C(2min) => 20C/min => 160C => 5C/min => 290C60C(2min) => 20C/min => 160C => 5C/min => 290C50C(1min) => 15C/min => 200C => 4C/min => 260C
I 2811.2812.2778.
ReferencePoling and Maier, 1988Poling and Maier, 1988Heupel R.C., Phinney B.O., et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kim, Lee, et al., 2003
Kim, S.-K.; Lee, S.-C.; Shin, D.-H.; Jang, S.-W.; Nam, J.-W.; Park, T.-S.; Lee, I.-J., Quantification of endogenous gibberellins in leaves and tubers of Chinese yam, Dioscorea opposita Thunb. cv. Tsukune during tuber enlargement, Plant Growth Regul., 2003, 39, 2, 125-130, https://doi.org/10.1023/A:1022569506883 . [all data]

Pearce, Hutt, et al., 2002
Pearce, D.W.; Hutt, O.E.; Rood, S.B.; Mander, L.N., Gibberellins in shoots and developing capsules of Populus species, Phytochemistry, 2002, 59, 6, 679-687, https://doi.org/10.1016/S0031-9422(02)00009-2 . [all data]

Kobayashi, MacMillan, et al., 2000
Kobayashi, M.; MacMillan, J.; Phinney, B.; Gaskin, P.; Spray, C.R.; Hedden, P., Gibberellin biosynthesis: metabolic evidence for three steps in the early 13-hydroxylation pathway of rice, Phytochemistry, 2000, 55, 4, 317-321, https://doi.org/10.1016/S0031-9422(00)00265-X . [all data]

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045, https://doi.org/10.1104/pp.121.3.1037 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Kobayashi, Spray, et al., 1996
Kobayashi, M.; Spray, C.R.; Phinney, B.O.; Gaskin, P.; MacMillan, J., Gibberellin metabolism in maize. The stepwise conversion of gibberellin A12-aldehyde to gibberellin A20, Plant Physiol., 1996, 110, 413-418. [all data]

Ridoutt, Pharis, et al., 1995
Ridoutt, B.G.; Pharis, R.P.; Sands, R., Identification and quantification of cambial region hormones of Eucalyptus globulus, Plant Cell Physiol., 1995, 36, 6, 1143-1147. [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240, https://doi.org/10.1007/BF00029896 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Poling and Maier, 1988
Poling, S.M.; Maier, V.P., Identification of endogenous gibberellins in navel orange shoots, Plant Physiol., 1988, 88, 3, 639-642, https://doi.org/10.1104/pp.88.3.639 . [all data]

Heupel R.C., Phinney B.O., et al., 1985
Heupel R.C.; Phinney B.O.; Spray C.R.; Gaskin P.; MacMillan J.; Hedden P.; Graebe J.E., Native gibberellins and the metabolism of [14C] gibberellin A53 and of [17-C-13,17-3H)] gibberellin A-20 in tassels of Zea-mays, Phytochemistry, 1985, 24, 1, 47-53, https://doi.org/10.1016/S0031-9422(00)80805-5 . [all data]


Notes

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