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GA44, Me-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Kovats' RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryHP-52814.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillaryHP-52816.Morvan-Bertrand, Ernstsen, et al., 2001Program: not specified
CapillaryDB-12780.Koshioka, Miyamoto, et al., 199815. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-12784.Nakayama, Yokota, et al., 1996He; Column length: 15. m; Column diameter: 0.258 mm; Program: 130C (2min) => 32C/min => 220C (4min) => 8C/min => 270C (5min)
CapillaryUltra-22786.Talon M., Koornneef M., et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22786.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22786.Talon, Koornneef, et al., 199025. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryUltra-22789.Talon and Zeevaart, 199025. m/0.32 mm/0.52 «mu»m, He; Program: 50C => 40C/min => 220C => 6C/min => 280C
CapillaryBP-12823.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C
CapillaryBP-12824.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryHP-12789.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryHP-12789.Kim, Lee, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1min) => 15C/min => 200C => 5C/min => 285C
CapillaryHP-12795.Pearce, Hutt, et al., 2002Column length: 12. m; Column diameter: 0.22 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryHP-12796.Pearce, Hutt, et al., 2002Column length: 12. m; Column diameter: 0.22 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-52821.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-52826.Pearce, Hutt, et al., 2002Column length: 15. m; Column diameter: 0.25 mm; Program: 60C(0.5min) => 20C/min => 200C => 5C/min => 300C
CapillaryOV-12791.Kobayashi, MacMillan, et al., 2000He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryOV-12803.Kobayashi, MacMillan, et al., 2000He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryOV-12786.Davis, Kobayashi, et al., 199925. m/0.2 mm/0.25 «mu»m, He; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)
CapillaryOV-12786.Webb, Appleford, et al., 199825. m/0.2 mm/0.25 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12805.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryBP-12805.Webb, Appleford, et al., 199825. m/0.2 mm/0.1 «mu»m; Program: 60C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12793.Grünzweig, Rabinowitch, et al., 1997He; Column length: 30. m; Column diameter: 0.25 mm; Program: 40C (2min) => 10C/min => 150C => 3C/min => 300C
CapillaryCP Sil 5 CB2786.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryCP Sil 5 CB2788.Kappers, Jordi, et al., 199730. m/0.25 mm/0.4 «mu»m, He; Program: 200C => 25C/min => 250C => 4C/min => 280C(4min)
CapillaryOV-12800.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12801.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryOV-12802.Kobayashi, Spray, et al., 199625. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C
CapillaryDB-12781.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12781.Ridoutt, Pharis, et al., 199515. m/0.25 mm/0.25 «mu»m, He; Program: 60C(1min) => 20C/min => 200C => 4C/min => 260C
CapillaryDB-12800.Pearce, Koshioka, et al., 199415. m/0.22 mm/0.25 «mu»m; Program: 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min
CapillaryCP Sil 5 CB2831.Taylor, Blake, et al., 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 60C(0.3min) => 20C/min => 220C => 4C/min => 300C
CapillaryCP Sil 5 CB2833.Taylor, Blake, et al., 1994He; Column length: 25. m; Column diameter: 0.25 mm; Program: 60C(0.3min) => 20C/min => 220C => 4C/min => 300C
CapillarySE-522778.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySE-522778.Hedden, Hoad, et al., 199325. m/0.22 mm/0.25 «mu»m, He; Program: 50C => 15C/min => 240C => 4C/min => 300C
CapillarySPB-12811.Poling and Maier, 198830. m/0.25 mm/0.25 «mu»m, He; Program: 60C(2min) => 20C/min => 160C => 5C/min => 290C
CapillarySPB-12812.Poling and Maier, 198830. m/0.25 mm/0.25 «mu»m, He; Program: 60C(2min) => 20C/min => 160C => 5C/min => 290C
CapillaryOV-12778.Heupel R.C., Phinney B.O., et al., 1985He; Program: 50C(1min) => 15C/min => 200C => 4C/min => 260C

Normal alkane RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryPolydimethyl siloxane2779.Fujioka, Yamane, et al., 1988200. C @ 2. min, 5. K/min; Tend: 320. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column typeActive phaseIReferenceComment
CapillaryDB-12767.Chung, Kuo, et al., 200315. m/0.25 mm/0.25 «mu»m; Program: 60 0C (0.1 min) 20 0C -> 200 0C 5 0C/min -> 300 0C
CapillaryDB-12791.Nakayama, Koshioka, et al., 200130. m/0.25 mm/0.25 «mu»m, He; Program: 60C (2min) => 2C/min => 210C => 2C/min => 280C(5min)
CapillaryHP-12823.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryHP-12823.Fos, Nuez, et al., 200025. m/0.20 mm/0.33 «mu»m, Helium; Program: 60 0C (1 min) 20 0C/min -> 240 0C 4 0C/min -> 300 0C
CapillaryDB-12779.Motosugi, Nishijima, et al., 199615. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-12760.Nishijima, Murakami, et al., 199315; Column diameter: 0.257 mm; Phase thickness: 0.25 «mu»m; Program: not specified
CapillaryUltra 22785.Talon, Zacarias, et al., 199222. m/0.32 mm/0.52 «mu»m, Helium; Program: not specified
CapillaryHP-12794.Beall, Morgan, et al., 199112. m/0.2 mm/0.33 «mu»m, He; Program: 60C(1min) => 15C/min => 200C => 5C/min => 270C
CapillaryHP-12787.Matheussen, Morgan, et al., 199112. m/0.2 mm/0.33 «mu»m, He; Program: 60C(1min) => 15C/min => 200C => 5C/min => 270C
CapillaryUltra-22787.Talon, Zeevaart, et al., 199125. m/0.32 mm/0.52 «mu»m; Program: 50C => 40C/min => 220C => 8C/min => 280C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Morvan-Bertrand, Ernstsen, et al., 2001
Morvan-Bertrand, A.; Ernstsen, A.; Lindgård, B.; Koshioka, M.; le Saos, J.; Boucaud, J.; Prud'homme, M.-P.; Junttila, O., Endogenous gibberellins in Lolium perenne and influence of defoliation on their contents in elongating leaf bases and in leaf sheaths, Physiol. Plant., 2001, 111, 2, 225-231. [doi:10.1034/j.1399-3054.2001.1110214.x] [all data]

Koshioka, Miyamoto, et al., 1998
Koshioka, M.; Miyamoto, K.; Horio, T.; Namura, S.; Hisamatsu, T.; Kubota, S.; Ernstsen, A.; Junttila, O.; Mander, L.N., Identification of endogenous gibberellins in stems and leaves in vegetative growth stage of Gentiana triflora, J. Plant Physiol., 1998, 153, 1-2, 230-232. [doi:10.1016/S0176-1617(98)80071-0] [all data]

Nakayama, Yokota, et al., 1996
Nakayama, M.; Yokota, T.; Sohma, R.; Mander, L.N.; Twitchin, B.; Komatsu, H.; Matsui, H.; Bukovac, M.J., Gibberellins in immature seed of Prunus cerasus: structure determination and synthesis of gibberellin, GA95 (1,2-didehydro-GA20), Phytochemistry, 1996, 42, 4, 913-920. [doi:10.1016/0031-9422(96)00035-0] [all data]

Talon M., Koornneef M., et al., 1990
Talon M.; Koornneef M.; Zeevaart J.A.D., Accumulation of C19-gibberelins in the gibbrellin-insensitive dwarf mutant gai if Arabidopsis thaliana (L.) Heynh, Planta, 1990, 182, 4, 501-505. [doi:10.1007/BF02341024] [all data]

Talon, Koornneef, et al., 1990
Talon, M.; Koornneef, M.; Zeevaart, J.A.D., Endogenous gibberellins in Arabidopsis thaliana and possible steps blocked in the biosynthetic pathways of the semidwarf ga4 and ga5 mutants, Proc. Nat. Acad. Sci. U.S.A., 1990, 87, 20, 7983-7987. [doi:10.1073/pnas.87.20.7983] [all data]

Talon and Zeevaart, 1990
Talon, M.; Zeevaart, J.A.D., Gibberellins and stem growth as related to photoperiod in Silene armeria L., Plant Physiol., 1990, 92, 4, 1094-1100. [doi:10.1104/pp.92.4.1094] [all data]

Hedden, Croker, et al., 1989
Hedden, P.; Croker, S.J.; Rademacher, W.; Jung, J., Effects of the triazole plant growth retardant BAS 111..W on gibberellin levels in oilseed rape, Brassica napus, Physiol. Plant., 1989, 75, 4, 445-451. [doi:10.1111/j.1399-3054.1989.tb05607.x] [all data]

Kim, Lee, et al., 2003
Kim, S.-K.; Lee, S.-C.; Shin, D.-H.; Jang, S.-W.; Nam, J.-W.; Park, T.-S.; Lee, I.-J., Quantification of endogenous gibberellins in leaves and tubers of Chinese yam, Dioscorea opposita Thunb. cv. Tsukune during tuber enlargement, Plant Growth Regul., 2003, 39, 2, 125-130. [doi:10.1023/A:1022569506883] [all data]

Pearce, Hutt, et al., 2002
Pearce, D.W.; Hutt, O.E.; Rood, S.B.; Mander, L.N., Gibberellins in shoots and developing capsules of Populus species, Phytochemistry, 2002, 59, 6, 679-687. [doi:10.1016/S0031-9422(02)00009-2] [all data]

Kobayashi, MacMillan, et al., 2000
Kobayashi, M.; MacMillan, J.; Phinney, B.; Gaskin, P.; Spray, C.R.; Hedden, P., Gibberellin biosynthesis: metabolic evidence for three steps in the early 13-hydroxylation pathway of rice, Phytochemistry, 2000, 55, 4, 317-321. [doi:10.1016/S0031-9422(00)00265-X] [all data]

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045. [doi:10.1104/pp.121.3.1037] [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677. [doi:10.1016/S0031-9422(97)00684-5] [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815. [doi:10.1016/S0031-9422(97)00383-X] [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225. [doi:10.1007/PL00007000] [all data]

Kobayashi, Spray, et al., 1996
Kobayashi, M.; Spray, C.R.; Phinney, B.O.; Gaskin, P.; MacMillan, J., Gibberellin metabolism in maize. The stepwise conversion of gibberellin A12-aldehyde to gibberellin A20, Plant Physiol., 1996, 110, 413-418. [all data]

Ridoutt, Pharis, et al., 1995
Ridoutt, B.G.; Pharis, R.P.; Sands, R., Identification and quantification of cambial region hormones of Eucalyptus globulus, Plant Cell Physiol., 1995, 36, 6, 1143-1147. [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122. [doi:10.1016/0021-9673(94)85210-3] [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240. [doi:10.1007/BF00029896] [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237. [doi:10.1016/S0031-9422(00)94973-2] [all data]

Poling and Maier, 1988
Poling, S.M.; Maier, V.P., Identification of endogenous gibberellins in navel orange shoots, Plant Physiol., 1988, 88, 3, 639-642. [doi:10.1104/pp.88.3.639] [all data]

Heupel R.C., Phinney B.O., et al., 1985
Heupel R.C.; Phinney B.O.; Spray C.R.; Gaskin P.; MacMillan J.; Hedden P.; Graebe J.E., Native gibberellins and the metabolism of [14C] gibberellin A53 and of [17-C-13,17-3H)] gibberellin A-20 in tassels of Zea-mays, Phytochemistry, 1985, 24, 1, 47-53. [doi:10.1016/S0031-9422(00)80805-5] [all data]

Fujioka, Yamane, et al., 1988
Fujioka, S.; Yamane, H.; Spray, C.R.; Gaskin, P.; Macmillan, J.; Phinney, B.O.; Takahashi, N., Qualitative and quantitative analyses of gibberellins in vegetative shoots of normal, dwarf-1, dwarf-2, dwarf-3, and dwarf-5 seedlings of Zea mays L., Plant Physiol., 1988, 88, 4, 1367-1372. [doi:10.1104/pp.88.4.1367] [all data]

Chung, Kuo, et al., 2003
Chung, J.-D.; Kuo, S.-R.; Chien, C.-T., Identification and quantification of gibberellin transformation and dosage changes in good and poor flowering clones of Calocedrus formosana grafts, Taiwan J. For. Sci., 2003, 18, 4, 387-400. [all data]

Nakayama, Koshioka, et al., 2001
Nakayama, M.; Koshioka, M.; Matsui, H.; Ohara, H.; Mander, L.N.; Leitch, S.K.; Twitchin, B.; Kraft-Klaunzer, P.; Pharis, R.P.; Yokota, T., Endogenous gibberellins in immature seeds of Prunus persica L.: identification of GA118, GA119, GA120, GA121, GA122 and GA126, Phytochemistry, 2001, 57, 5, 749-758. [doi:10.1016/S0031-9422(01)00154-6] [all data]

Fos, Nuez, et al., 2000
Fos, M.; Nuez, F.; Garcia-Martinez, J.L., The gene pat-2, which induces natural partenocarpy, alters the gibberellin content in unpollinated tomato ovaries, Plant Physiol., 2000, 122, 2, 471-479. [doi:10.1104/pp.122.2.471] [all data]

Motosugi, Nishijima, et al., 1996
Motosugi, H.; Nishijima, T.; Hiehata, N.; Koshioka, M.; Sugiura, A., Endogenous gibberellins in the xylem exudate from apple trees, Biosci. Biotechnol. Biochem., 1996, 60, 9, 1500-1502. [doi:10.1271/bbb.60.1500] [all data]

Nishijima, Murakami, et al., 1993
Nishijima, T.; Murakami, F.; Koshioka, M.; Yamazaki, H., Endogenous gibberellins in Aralia cordata, Japan Society for Biosci. Biotechnol. Agrochem., 1993, 57, 1, 1953-1954. [doi:10.1271/bbb.57.1953] [all data]

Talon, Zacarias, et al., 1992
Talon, M.; Zacarias, L.; PRimo-Millo, E., Gibberellins and Partenocarpic ability in developing ovaries of seedless mandarins, Plant Physiol., 1992, 99, 4, 1575-1581. [doi:10.1104/pp.99.4.1575] [all data]

Beall, Morgan, et al., 1991
Beall, F.D.; Morgan, P.W.; Mander, L.N.; Miller, F.R.; Babb, K.H., Genetic regulation of development in Sorghum bicolor. V. The ma3R allele results in gibberellin enrichment, Plant Physiol., 1991, 95, 1, 116-125. [doi:10.1104/pp.95.1.116] [all data]

Matheussen, Morgan, et al., 1991
Matheussen, A.-M.; Morgan, P.W.; Frederiksen, R.A., Implication of gibberellins in head smut (Sporisorium reilianum) of Sorghum bicolor, Plant Physiol., 1991, 96, 2, 537-544. [doi:10.1104/pp.96.2.537] [all data]

Talon, Zeevaart, et al., 1991
Talon, M.; Zeevaart, J.A.D.; Gage, D.A., Identification of gibberellins in spinach and effects of light and darkness on their levels, Plant Physiol., 1991, 97, 4, 1521-1526. [doi:10.1104/pp.97.4.1521] [all data]


Notes

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