GA3, MeTMSi


Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-5MSDB-5MSCP Sil 5 CB
Column length (m) 25.25.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Program 60C (1min) => 20C/min => 170C => 4C/min => 290C60C (1min) => 20C/min => 170C => 4C/min => 290C50C(1min) => 30C/min => 240C => 10C/min => 280C50C(1min) => 30C/min => 240C => 10C/min => 280C60C(0.7min) => 20C/min => 220C => 4C/min => 300C
I 2746.2746.2692.2692.2729.
ReferenceBlake, Taylor, et al., 2002Blake, Taylor, et al., 2002Gutiérrez-Mañero, Ramos-Solano, et al., 2001Gutiérrez-Mañero, Ramos-Solano, et al., 2001Taylor, Blake, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBOV-1CP-Sil5 CB MS
Column length (m) 25.25.25.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm)    0.25 
Program 60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)90C(1min) => 20C/min => 220C => 4C/min => 290C
I 2730.2729.2730.2692.2712.
ReferenceTaylor, Blake, et al., 2000Taylor, Blake, et al., 2000, 2Taylor, Blake, et al., 2000, 2Davis, Kobayashi, et al., 1999Roberts, Blake, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil5 CB MSOV-1BP-1DB-1DB-1
Column length (m) 25.25.25.30.30.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.20.20.250.25
Phase thickness (μm)  0.250.1  
Program 90C(1min) => 20C/min => 220C => 4C/min => 290C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C40C (2min) => 10C/min => 150C => 3C/min => 300C40C (2min) => 10C/min => 150C => 3C/min => 300C
I 2713.2692.2699.2696.2696.
ReferenceRoberts, Blake, et al., 1999Webb, Appleford, et al., 1998Webb, Appleford, et al., 1998Grünzweig, Rabinowitch, et al., 1997Grünzweig, Rabinowitch, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-1OV-1OV-1CP Sil 5 CB
Column length (m) 25.25.25.25.25.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.20.20.20.20.25
Phase thickness (μm) 0.10.250.250.25 
Program 60C(2min) => 10C/min => 150C => 3C/min => 300C(10min)60C(2min) => 10min/C => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C50C(1min) => 15C/min => 220C => 2C/min => 300C
I 2686.2697.2692.2699.2712.
ReferenceMacMillan and Gaskin, 1996Spray, Kobayashi, et al., 1996Santes, Hedden, et al., 1995Santes, Hedden, et al., 1995Blake and Browning, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1SE-52SE-52OV-1
Column length (m) 25.15.25.25.25.
Carrier gas He HeHe 
Substrate      
Column diameter (mm) 0.250.220.220.220.22
Phase thickness (μm)  0.250.250.250.25
Program 50C(1min) => 15C/min => 220C => 2C/min => 300C60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min50C => 15C/min => 240C => 4C/min => 300C50C => 15C/min => 240C => 4C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 310C
I 2713.2700.2692.2693.2692.
ReferenceBlake and Browning, 1994Pearce, Koshioka, et al., 1994Hedden, Hoad, et al., 1993Hedden, Hoad, et al., 1993Waycott, Smith, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-1
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.2
Phase thickness (μm)  
Program 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
I 2686.
ReferenceGaskin, Gilmour, et al., 1984
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Blake, Taylor, et al., 2002
Blake, P.S.; Taylor, J.M.; Finch-Savage, W.E., Identification of abscisic acid, indole-3-acetic acid, jasmonic acid, indole-3-acetonitrile, methyl jasmonate and gibberellins in developing, dormant and startified seeds of ash (Fraxinus excelsior), Plant Growth Regul., 2002, 37, 2, 119-125, https://doi.org/10.1023/A:1020504610172 . [all data]

Gutiérrez-Mañero, Ramos-Solano, et al., 2001
Gutiérrez-Mañero, F.J.; Ramos-Solano, B.; Probanza, A.; Mehouachi, J.; Tadeo, R.; Talon, M., The plant-growth-promoting rhizobacteria Bacillus pumilus and Baillus licheniformis produce high amounts of physiologically active gibberellins, Physiol. Plant., 2001, 111, 2, 206-211, https://doi.org/10.1034/j.1399-3054.2001.1110211.x . [all data]

Taylor, Blake, et al., 2000
Taylor, D.R.; Blake, P.S.; Crisp, C.M., Identification of gibberellins in leaf exudates of strawberry (Fragaria ananassa Duch.), Plant Growth Regul., 2000, 30, 3, 221-223, https://doi.org/10.1023/A:1006385617161 . [all data]

Taylor, Blake, et al., 2000, 2
Taylor, D.R.; Blake, P.S.; Crisp, C.M., Identification of gibberellins in leaf tissues of day-neutral strawberry (Fragaria × ananassa Duch.) cultivars, Plant Growth Regul., 2000, 30, 1, 5-7, https://doi.org/10.1023/A:1006275024517 . [all data]

Davis, Kobayashi, et al., 1999
Davis, G.; Kobayashi, M.; Phinney, B.O.; Lange, T.; Croker, S.J.; Gaskin, P.; MacMillan, J., Gibberellin biosynthesis in maize. Metabolic studies with GA15, GA24, GA25, GA7, and 2,3-dehydro-GA9, Plant Physiol., 1999, 121, 3, 1037-1045, https://doi.org/10.1104/pp.121.3.1037 . [all data]

Roberts, Blake, et al., 1999
Roberts, A.V.; Blake, P.S.; Lewis, R.; Taylor, J.M.; Dunstan, D.I., The effect of gibberellins on flowering in roses, J. Plant Growth Regul., 1999, 18, 3, 113-119, https://doi.org/10.1007/PL00007058 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

MacMillan and Gaskin, 1996
MacMillan, J.; Gaskin, P., Gibberellins in endosperm and embryos of Marah macrocarpus, Phytochemistry, 1996, 42, 5, 1263-1266, https://doi.org/10.1016/0031-9422(96)00179-3 . [all data]

Spray, Kobayashi, et al., 1996
Spray, C.R.; Kobayashi, M.; Suzuki, Y.; Phinney, B.O.; Gaskin, P.; MacMillan, J., The dwarf-1 (dl) mutant of Zea mays blocks three steps in the gibberellin-biosynthetic pathway, Proc. Nat. Acad. Sci. U.S.A., 1996, 93, 19, 10515-10518, https://doi.org/10.1073/pnas.93.19.10515 . [all data]

Santes, Hedden, et al., 1995
Santes, C.M.; Hedden, P.; Gaskin, P.; Garcia-Martinez, J.L., Gibberellins and related compounds in young fruits of pea and their relationship to fruit-set, Phytochemistry, 1995, 40, 5, 1347-1355, https://doi.org/10.1016/0031-9422(95)00489-T . [all data]

Blake and Browning, 1994
Blake, P.S.; Browning, G., Gibberellins in developing fruits of Prunus avium, Phytochemistry, 1994, 35, 6, 1383-1386, https://doi.org/10.1016/S0031-9422(00)86860-0 . [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Hedden, Hoad, et al., 1993
Hedden, P.; Hoad, G.V.; Gaskin, P.; Lewis, M.J.; Green, J.R.; Furber, M.; Mander, L.N., Kaurenoids and gibberellins, including the newly characterized gibberellin A88, in developing apple seeds, Phytochemistry, 1993, 32, 2, 231-237, https://doi.org/10.1016/S0031-9422(00)94973-2 . [all data]

Waycott, Smith, et al., 1991
Waycott, W.; Smith, V.A.; Gaskin, P.; MacMillan, J.; Taiz, L., The endogenous gibberellins of dwarf mutants of lettuce, Plant Physiol., 1991, 95, 4, 1169-1173, https://doi.org/10.1104/pp.95.4.1169 . [all data]

Gaskin, Gilmour, et al., 1984
Gaskin, P.; Gilmour, S.J.; Lenton, J.R.; MacMillan, J.; Sponsel, V.M., Endogenous gibberellins and kauranoids identified from developing and germinating barley grain, J. Plant Growth Regul., 1984, 2, 1-4, 229-242, https://doi.org/10.1007/BF02042252 . [all data]


Notes

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