GA29, MeTMSi


Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 25.15.15.25.25.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25    
Program 60C (1min) => 20C/min => 170C => 4C/min => 290C60C(0.5min) => 20C/min => 200C => 5C/min => 300C60C(0.5min) => 20C/min => 200C => 5C/min => 300C60C(0.7min) => 20C/min => 220C => 4C/min => 300C60C(0.7min) => 20C/min => 220C => 4C/min => 300C
I 2722.2672.2672.2712.2712.
ReferenceBlake, Taylor, et al., 2002Pearce, Hutt, et al., 2002Pearce, Hutt, et al., 2002Taylor, Blake, et al., 2000Taylor, Blake, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil5 CB MSCP-Sil5 CB MSOV-1BP-1BP-1
Column length (m) 25.25.25.25.25.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.250.250.20.20.2
Phase thickness (μm)   0.250.10.1
Program 90C(1min) => 20C/min => 220C => 4C/min => 290C90C(1min) => 20C/min => 220C => 4C/min => 290C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C
I 2684.2698.2684.2689.2689.
ReferenceRoberts, Blake, et al., 1999Roberts, Blake, et al., 1999Webb, Appleford, et al., 1998Webb, Appleford, et al., 1998Webb, Appleford, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1CP Sil 5 CBCP Sil 5 CBOV-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm)   0.40.40.25
Program 40C (2min) => 10C/min => 150C => 3C/min => 300C40C (2min) => 10C/min => 150C => 3C/min => 300C200C => 25C/min => 250C => 4C/min => 280C(4min)200C => 25C/min => 250C => 4C/min => 280C(4min)60C(2min) => 10min/C => 150C => 3C/min => 300C
I 2686.2690.2691.2691.2687.
ReferenceGrünzweig, Rabinowitch, et al., 1997Grünzweig, Rabinowitch, et al., 1997Kappers, Jordi, et al., 1997Kappers, Jordi, et al., 1997Spray, Kobayashi, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1OV-1OV-1OV-1
Column length (m) 15.15.25.25.25.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.20.20.2
Phase thickness (μm) 0.250.250.250.25 
Program 60C(1min) => 20C/min => 200C => 4C/min => 260C60C(1min) => 20C/min => 200C => 4C/min => 260C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 300C60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
I 2679.2679.2684.2690.2690.
ReferenceRidoutt, Pharis, et al., 1995Ridoutt, Pharis, et al., 1995Santes, Hedden, et al., 1995Santes, Hedden, et al., 1995Talo, Spray, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1CP Sil 5 CBBP-1BP-1OV-1
Column length (m) 25.25.25.25.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.220.220.2
Phase thickness (μm)   0.250.25 
Program 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)50C(1min) => 15C/min => 220C => 2C/min => 300C60C => 30C/min => 240C => 3C/min => 290C60C => 30C/min => 240C => 3C/min => 290C60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
I 2690.2698.2695.2696.2688.
ReferenceTalo, Spray, et al., 1995Blake and Browning, 1994Hasan, Ridoutt, et al., 1994Hasan, Ridoutt, et al., 1994Kobayashi, Gaskin, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBOV-1SPB-1SPB-1
Column length (m) 15.25.25.30.30.
Carrier gas  He HeHe
Substrate      
Column diameter (mm) 0.220.250.220.250.25
Phase thickness (μm) 0.25 0.250.250.25
Program 60(0.1 min)-200 0C at 20 deg/min; 200-300 0C at 5 deg/min60C(0.3min) => 20C/min => 220C => 4C/min => 300C60C(2min) => 10C/min => 150C => 3C/min => 310C60C(2min) => 20C/min => 160C => 5C/min => 290C60C(2min) => 20C/min => 160C => 5C/min => 290C
I 2690.2699.2684.2694.2694.
ReferencePearce, Koshioka, et al., 1994Taylor, Blake, et al., 1994Waycott, Smith, et al., 1991Poling and Maier, 1988Poling and Maier, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-1
Column length (m)  
Carrier gas He
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Program 50C(1min) => 15C/min => 200C => 4C/min => 260C
I 2681.
ReferenceHeupel R.C., Phinney B.O., et al., 1985
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Blake, Taylor, et al., 2002
Blake, P.S.; Taylor, J.M.; Finch-Savage, W.E., Identification of abscisic acid, indole-3-acetic acid, jasmonic acid, indole-3-acetonitrile, methyl jasmonate and gibberellins in developing, dormant and startified seeds of ash (Fraxinus excelsior), Plant Growth Regul., 2002, 37, 2, 119-125, https://doi.org/10.1023/A:1020504610172 . [all data]

Pearce, Hutt, et al., 2002
Pearce, D.W.; Hutt, O.E.; Rood, S.B.; Mander, L.N., Gibberellins in shoots and developing capsules of Populus species, Phytochemistry, 2002, 59, 6, 679-687, https://doi.org/10.1016/S0031-9422(02)00009-2 . [all data]

Taylor, Blake, et al., 2000
Taylor, D.R.; Blake, P.S.; Crisp, C.M., Identification of gibberellins in leaf tissues of day-neutral strawberry (Fragaria × ananassa Duch.) cultivars, Plant Growth Regul., 2000, 30, 1, 5-7, https://doi.org/10.1023/A:1006275024517 . [all data]

Roberts, Blake, et al., 1999
Roberts, A.V.; Blake, P.S.; Lewis, R.; Taylor, J.M.; Dunstan, D.I., The effect of gibberellins on flowering in roses, J. Plant Growth Regul., 1999, 18, 3, 113-119, https://doi.org/10.1007/PL00007058 . [all data]

Webb, Appleford, et al., 1998
Webb, S.E.; Appleford, N.E.J.; Gaskin, P.; Lenton, J.R., Gibberellins in internodes and ears of wheat containing different dwarfing alleles, Phytochemistry, 1998, 47, 5, 671-677, https://doi.org/10.1016/S0031-9422(97)00684-5 . [all data]

Grünzweig, Rabinowitch, et al., 1997
Grünzweig, J.M.; Rabinowitch, H.D.; Katan, J.; Wodner, M.; Ben-Tal, Y., Endogenous gibberellins in foliage of tomato (Lycopersicon esculentum), Phytochemistry, 1997, 46, 5, 811-815, https://doi.org/10.1016/S0031-9422(97)00383-X . [all data]

Kappers, Jordi, et al., 1997
Kappers, I.F.; Jordi, W.; Maas, F.M.; van der Plas, L.H.W., Gibberellins in leaves of Alstroemeria hybrida: identification and quantification in relation to leaf age, J. Plant Growth Regul., 1997, 16, 4, 219-225, https://doi.org/10.1007/PL00007000 . [all data]

Spray, Kobayashi, et al., 1996
Spray, C.R.; Kobayashi, M.; Suzuki, Y.; Phinney, B.O.; Gaskin, P.; MacMillan, J., The dwarf-1 (dl) mutant of Zea mays blocks three steps in the gibberellin-biosynthetic pathway, Proc. Nat. Acad. Sci. U.S.A., 1996, 93, 19, 10515-10518, https://doi.org/10.1073/pnas.93.19.10515 . [all data]

Ridoutt, Pharis, et al., 1995
Ridoutt, B.G.; Pharis, R.P.; Sands, R., Identification and quantification of cambial region hormones of Eucalyptus globulus, Plant Cell Physiol., 1995, 36, 6, 1143-1147. [all data]

Santes, Hedden, et al., 1995
Santes, C.M.; Hedden, P.; Gaskin, P.; Garcia-Martinez, J.L., Gibberellins and related compounds in young fruits of pea and their relationship to fruit-set, Phytochemistry, 1995, 40, 5, 1347-1355, https://doi.org/10.1016/0031-9422(95)00489-T . [all data]

Talo, Spray, et al., 1995
Talo, A.; Spray, C.R.; Somers, D.A.; Donovan, C.M.; Gaskin, P.; Macmillian, J.; Phinney, B.O., Endogenous gibberellins from callus cultures of maize, Phytochemistry, 1995, 40, 1, 11-15, https://doi.org/10.1016/0031-9422(95)00000-W . [all data]

Blake and Browning, 1994
Blake, P.S.; Browning, G., Gibberellins in developing fruits of Prunus avium, Phytochemistry, 1994, 35, 6, 1383-1386, https://doi.org/10.1016/S0031-9422(00)86860-0 . [all data]

Hasan, Ridoutt, et al., 1994
Hasan, O.; Ridoutt, B.G.; Ross, J.J.; Davies, N.W.; Reid, J.B., Identification and quantification of endogenous gibberellins in apical buds and the cambial region of Eucalyptus, Physiol. Plant., 1994, 90, 3, 475-480, https://doi.org/10.1111/j.1399-3054.1994.tb08804.x . [all data]

Kobayashi, Gaskin, et al., 1994
Kobayashi, M.; Gaskin, P.; Spray, C.R.; Phinney, B.O.; MacMillan, J., The metabolism of gibberellin A20 to gibberellin A1 by tall and dwarf mutants of Oryza sativa and Arabidopsis thaliana, Plant Physiol., 1994, 106, 1367-1372. [all data]

Pearce, Koshioka, et al., 1994
Pearce, D.W.; Koshioka, M.; Pharis, R.P., Chromatography of gibberellins, J. Chromatogr. A, 1994, 658, 1, 91-122, https://doi.org/10.1016/0021-9673(94)85210-3 . [all data]

Taylor, Blake, et al., 1994
Taylor, D.R.; Blake, P.S.; Browning, G., Identification of gibberellins in leaf tissues of strawberry (Fragaria × ananassa Duch.) grown under different photoperiods, Plant Growth Regul., 1994, 15, 3, 235-240, https://doi.org/10.1007/BF00029896 . [all data]

Waycott, Smith, et al., 1991
Waycott, W.; Smith, V.A.; Gaskin, P.; MacMillan, J.; Taiz, L., The endogenous gibberellins of dwarf mutants of lettuce, Plant Physiol., 1991, 95, 4, 1169-1173, https://doi.org/10.1104/pp.95.4.1169 . [all data]

Poling and Maier, 1988
Poling, S.M.; Maier, V.P., Identification of endogenous gibberellins in navel orange shoots, Plant Physiol., 1988, 88, 3, 639-642, https://doi.org/10.1104/pp.88.3.639 . [all data]

Heupel R.C., Phinney B.O., et al., 1985
Heupel R.C.; Phinney B.O.; Spray C.R.; Gaskin P.; MacMillan J.; Hedden P.; Graebe J.E., Native gibberellins and the metabolism of [14C] gibberellin A53 and of [17-C-13,17-3H)] gibberellin A-20 in tassels of Zea-mays, Phytochemistry, 1985, 24, 1, 47-53, https://doi.org/10.1016/S0031-9422(00)80805-5 . [all data]


Notes

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