Trp isoBOC TBDMS


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillary
Active phase DB-5DB-5
Column length (m) 30.30.
Carrier gas   
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (μm) 0.250.24
Tstart (C) 150.150.
Tend (C) 280.280.
Heat rate (K/min) 3.3.
Initial hold (min) 2.2.
Final hold (min)   
I 2870.2867.
ReferenceOh, Kim, et al., 1994Kim, Kim, et al., 1992
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Oh, Kim, et al., 1994
Oh, C.-H.; Kim, J.-H.; Kim, K.-R.; Brownson, D.M.; Mabry, T.J., Simultaneous gas chromatographic analysis of non-protein and protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives, J. Chromatogr. A, 1994, 669, 1-2, 125-137, https://doi.org/10.1016/0021-9673(94)80344-7 . [all data]

Kim, Kim, et al., 1992
Kim, K.-R.; Kim, J.-H.; Oh, C.-H.; Mabry, T.J., Capillary gas chromatography of protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives in aqueous samples, J. Chromatogr., 1992, 605, 2, 241-249, https://doi.org/10.1016/0021-9673(92)85242-L . [all data]


Notes

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