alanine, N(O,S)-isoBOC TBDMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51702.7Oh, Mabry, et al., 199530. m/0.25 mm/0.25 μm, N2, 150. C @ 2. min, 3. K/min; Tend: 280. C
CapillaryDB-51703.Oh, Kim, et al., 199430. m/0.25 mm/0.25 μm, 150. C @ 2. min, 3. K/min; Tend: 280. C
CapillaryDB-51702.Kim, Kim, et al., 199230. m/0.25 mm/0.24 μm, 150. C @ 2. min, 3. K/min; Tend: 280. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Oh, Mabry, et al., 1995
Oh, C.-H.; Mabry, T.J.; Kim, K.-R.; Kim, J.-H., GC-MS Analysis of nonprotein amino acids in Gymnocladus dioicus as N(O,S)-Isobutyloxycarbonyl silyl derivatives, J. Chromatogr. Sci., 1995, 33, 7, 399-404, https://doi.org/10.1093/chromsci/33.7.399 . [all data]

Oh, Kim, et al., 1994
Oh, C.-H.; Kim, J.-H.; Kim, K.-R.; Brownson, D.M.; Mabry, T.J., Simultaneous gas chromatographic analysis of non-protein and protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives, J. Chromatogr. A, 1994, 669, 1-2, 125-137, https://doi.org/10.1016/0021-9673(94)80344-7 . [all data]

Kim, Kim, et al., 1992
Kim, K.-R.; Kim, J.-H.; Oh, C.-H.; Mabry, T.J., Capillary gas chromatography of protein amino acids as N(O,S)-isobutyloxycarbonyl tert.-butyldimethylsilyl derivatives in aqueous samples, J. Chromatogr., 1992, 605, 2, 241-249, https://doi.org/10.1016/0021-9673(92)85242-L . [all data]


Notes

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