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17-«alpha»-Methyl-5-«beta»-androstan-3-«alpha»,17-«beta»-diol, per-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1210.2620.Brooks, Thawley, et al., 1971 

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-542637.Schänzer, Opfermann, et al., 19925. K/min; Column length: 17. m; Phase thickness: 0.33 «mu»m; Tstart: 200. C; Tend: 320. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Brooks, Thawley, et al., 1971
Brooks, C.J.W.; Thawley, A.R.; Rocher, P.; Middleditch, B.S.; Anthony, G.M.; Stillwell, W.G., Characterization of Steroidal Drug Metabolites by Combined Gas Chromatography-Mass Spectrometry, J. Chromatogr. Sci., 1971, 9, 1, 35-43, https://doi.org/10.1093/chromsci/9.1.35 . [all data]

Schänzer, Opfermann, et al., 1992
Schänzer, W.; Opfermann, G.; Donike, M., 17-Epimerization of 17«alpha»-methyl anabolic steroids in humans: metabolism and synthesis of 17«alpha»-hydroxy-17«beta»-methyl steroids, Steroids, 1992, 57, 11, 537-550, https://doi.org/10.1016/0039-128X(92)90023-3 . [all data]


Notes

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