D-Val, N-ethoxycarbonyl, (S)-1-phenylethylamide


Normal alkane RI, non-polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase DB-5
Column length (m) 30.
Carrier gas Helium
Substrate  
Column diameter (mm) 0.25
Phase thickness (μm) 0.25
Program 80 0C (2 min) 20 0C/min -> 150 0C 3 0C/min -> 230 0C 10 0C/min -> 290 0C (20 min)
I 2093.
ReferencePaik, Lee, et al., 2008
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Paik, Lee, et al., 2008
Paik, M.-J.; Lee, J.; Kim, K.-R., N-Ethoxycarbonylation combined with (S)-1-phenylethylamidation for enantioseparation of amino acids by achiral gas chromatography and gas chromatography - mass spectrometry, J. Chromatogr. A, 2008, 1214, 1-2, 151-156, https://doi.org/10.1016/j.chroma.2008.10.068 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References