Benzaldehyde, 2-hydroxy, oxime, bis-TMS
- Formula: C13H23NO2Si2
- Molecular weight: 281.4982
- IUPAC Standard InChI: InChI=1S/C13H23NO2Si2/c1-17(2,3)15-13-10-8-7-9-12(13)11-14-16-18(4,5)6/h7-11H,1-6H3
- IUPAC Standard InChIKey: FDGZOPGIGYPOQJ-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Benzaldehyde, 2-hydroxy, oxime, TMS
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Packed | Packed |
|---|---|---|
| Active phase | SE-30 | OV-1 |
| Column length (m) | 2. | 2. |
| Carrier gas | He | N2 |
| Substrate | Gas Chrom Q | Supelcoport |
| Column diameter (mm) | ||
| Phase thickness (μm) | ||
| Tstart (C) | 50. | 80. |
| Tend (C) | 240. | |
| Heat rate (K/min) | 6. | 4. |
| Initial hold (min) | ||
| Final hold (min) | ||
| I | 1560. | 1550. |
| Reference | Staniewski and Szymanowski, 1990 | Mattsson and Petersson, 1977 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Staniewski and Szymanowski, 1990
Staniewski, J.; Szymanowski, J.,
Gas chromatographic analyses of hydroxyoxime extractants of metals and their intermediates. I. Alkylsalicylaldehyde oximes,
J. Chromatogr., 1990, 503, 442-448, https://doi.org/10.1016/S0021-9673(01)81524-7
. [all data]
Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G.,
Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives,
J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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