p-Octopamine, DTFMB-TMS
- Formula: C23H29F6NO3Si2
- Molecular weight: 537.6427
- IUPAC Standard InChI: InChI=1S/C23H29F6NO3Si2/c1-34(2,3)32-19-9-7-15(8-10-19)20(33-35(4,5)6)14-30-21(31)16-11-17(22(24,25)26)13-18(12-16)23(27,28)29/h7-13,20H,14H2,1-6H3,(H,30,31)
- IUPAC Standard InChIKey: HIZOWXWPEDBLRZ-UHFFFAOYSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: p-Octopamine, N-DTFMB-TMS
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- Other data available:
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Normal alkane RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | HP-1 | Methyl Silicone |
| Column length (m) | 12.5 | 12.5 |
| Carrier gas | He | He |
| Substrate | ||
| Column diameter (mm) | 0.20 | 0.20 |
| Phase thickness (μm) | ||
| Tstart (C) | 100. | 100. |
| Tend (C) | 300. | 280. |
| Heat rate (K/min) | 10. | 20. |
| Initial hold (min) | 1. | 1. |
| Final hold (min) | ||
| I | 2256. | 2256. |
| Reference | Shafi, Midgley, et al., 1989 | Midgley, MacLachlan, et al., 1988 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Shafi, Midgley, et al., 1989
Shafi, N.; Midgley, J.M.; Watson, D.G.; Smail, G.A.; Strang, R.; MacFarlane, R.G.,
Analysis of biogenic amines in the brain of the American Cockroach (Periplaneta Americana) by gas chromatography-negative ion chemical ionisation mass spectrometry,
J. Chromatogr., 1989, 490, 9-19, https://doi.org/10.1016/S0378-4347(00)82756-5
. [all data]
Midgley, MacLachlan, et al., 1988
Midgley, J.M.; MacLachlan, J.; Watson, D.G.,
An extraction-derivatization method suitable for the analysis of biogenic amines by gas chromatography negative ion mass spectrometry,
Biomed. Environ. Mass Spectrom., 1988, 15, 10, 535-539, https://doi.org/10.1002/bms.1200151005
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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