m-Synephrine, N-DTFMB-TMS


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillary
Active phase HP-1Methyl Silicone
Column length (m) 12.512.5
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.200.20
Phase thickness (μm)   
Tstart (C) 100.100.
Tend (C) 300.280.
Heat rate (K/min) 10.20.
Initial hold (min) 1.1.
Final hold (min)   
I 2220.2220.
ReferenceShafi, Midgley, et al., 1989Midgley, MacLachlan, et al., 1988
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shafi, Midgley, et al., 1989
Shafi, N.; Midgley, J.M.; Watson, D.G.; Smail, G.A.; Strang, R.; MacFarlane, R.G., Analysis of biogenic amines in the brain of the American Cockroach (Periplaneta Americana) by gas chromatography-negative ion chemical ionisation mass spectrometry, J. Chromatogr., 1989, 490, 9-19, https://doi.org/10.1016/S0378-4347(00)82756-5 . [all data]

Midgley, MacLachlan, et al., 1988
Midgley, J.M.; MacLachlan, J.; Watson, D.G., An extraction-derivatization method suitable for the analysis of biogenic amines by gas chromatography negative ion mass spectrometry, Biomed. Environ. Mass Spectrom., 1988, 15, 10, 535-539, https://doi.org/10.1002/bms.1200151005 . [all data]


Notes

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