17α-hydroxy-5α-androstan-3-one (3-enol), per-TMS


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillary
Active phase Ultra-1HP-5MS
Column length (m) 17.16.5
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.20.25
Phase thickness (μm) 0.110.25
Tstart (C) 140.140.
Tend (C) 320.320.
Heat rate (K/min) 20.20.
Initial hold (min)   
Final hold (min) 2.2.
I 2563.2636.
ReferenceParr, Zapp, et al., 2007Parr, Zapp, et al., 2007
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Parr, Zapp, et al., 2007
Parr, M.K.; Zapp, J.; Becker, M.; Opfermann, G.; Bartz, U.; Schanzer, W., Steroidal isomers with uniform mass spectra of their per-TMS derivatives: Synthesis of 17-hydroxyandrostan-3-ones, androst-1-, and -4-ene-3,17-diols, Steroids, 2007, 72, 6-7, 545-551, https://doi.org/10.1016/j.steroids.2007.03.006 . [all data]


Notes

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