L-fucose, TMS diethyldithioacetal derivative


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase SE-54
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.25
Phase thickness (μm) 0.25
Tstart (C) 165.
Tend (C) 235.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 2217.
ReferencePitthard and Finch, 2001
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pitthard and Finch, 2001
Pitthard, V.; Finch, P., GC-MS Analysis of Monosaccharide Mixtures as their Diethyldithioacetal Derivatives: Application to Plant Gums Used in Art Works, Chromatographia, 2001, 53, S1, s317-s321, https://doi.org/10.1007/BF02490349 . [all data]


Notes

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