(3R,4R)-4-azido-3-tert-butyldimethylsilyloxy-1-tert-butoxycarbonylazepane


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase Optima-5
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm) 0.2
Phase thickness (mum) 0.1
Program not specified
I 2066.
ReferenceHerdeis, Mohareb, et al., 1999
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Herdeis, Mohareb, et al., 1999
Herdeis, C.; Mohareb, R.M.; Neder, R.B.; Schwabenländer, F.; Telser, J., Studies on the synthesis of chiral nonracemic 3,4-disubstituted azepanes, a formal synthesis of (+)- and (-)-balanol, Tetrahedron: Asymmetry, 1999, 10, 23, 4521-4537, https://doi.org/10.1016/S0957-4166(99)00466-8 . [all data]


Notes

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