2,6,10,10-Tetramethyl- 1-oxaspiro[ 4.5]dec-6-ene-2,8-diol, TMS


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase DB-5
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.25
Tstart (C) 60.
Tend (C) 300.
Heat rate (K/min) 5.
Initial hold (min)  
Final hold (min)  
I 1528.
ReferenceWinterhalter, 1991
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Winterhalter, 1991
Winterhalter, P., 1,1,6-Trimethyl-1,2-dihydronaphthalene (TDN) Formation in Wine. 1. Studies on the Hydrolysis of 2,6,10,10-Tetramethyl-l-oxaspiro[4.5]dec-6-ene-2,8-diol Rationalizing the Origin of TDN and Related C13 Norisoprenoids in Riesling Wine, J. Agric. Food Chem., 1991, 39, 10, 1825-1829, https://doi.org/10.1021/jf00010a027 . [all data]


Notes

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