2,6,10,10-Tetramethyl- 1-oxaspiro[ 4.5]dec-6-ene-2,8-diol, TMS
- Formula: C19H38O3Si2
- Molecular weight: 370.6742
- IUPAC Standard InChI: InChI=1S/C19H38O3Si2/c1-15-13-16(20-23(5,6)7)14-17(2,3)19(15)12-11-18(4,21-19)22-24(8,9)10/h13,16H,11-12,14H2,1-10H3
- IUPAC Standard InChIKey: BVCQQQOKCRYHIH-UHFFFAOYSA-N
- Chemical structure:
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary |
|---|---|
| Active phase | DB-5 |
| Column length (m) | 30. |
| Carrier gas | He |
| Substrate | |
| Column diameter (mm) | 0.25 |
| Phase thickness (μm) | 0.25 |
| Tstart (C) | 60. |
| Tend (C) | 300. |
| Heat rate (K/min) | 5. |
| Initial hold (min) | |
| Final hold (min) | |
| I | 1528. |
| Reference | Winterhalter, 1991 |
| Comment | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Winterhalter, 1991
Winterhalter, P.,
1,1,6-Trimethyl-1,2-dihydronaphthalene (TDN) Formation in Wine. 1. Studies on the Hydrolysis of 2,6,10,10-Tetramethyl-l-oxaspiro[4.5]dec-6-ene-2,8-diol Rationalizing the Origin of TDN and Related C13 Norisoprenoids in Riesling Wine,
J. Agric. Food Chem., 1991, 39, 10, 1825-1829, https://doi.org/10.1021/jf00010a027
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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