3α,4β-dihydroxy-5β-cholanoic acid, methyl ester-trimethylsilyl-ether derivative


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase DB-1
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm)  
Phase thickness (μm) 0.25
Tstart (C) 225.
Tend (C) 295.
Heat rate (K/min) 2.
Initial hold (min) 5.
Final hold (min) 20.
I 3339.
ReferenceDumaswala, Setchell, et al., 1989
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Dumaswala, Setchell, et al., 1989
Dumaswala, R.; Setchell, K.D.R.; Zimmer-Nechemias, L.; Iida, T.; Goto, J.; Nambara, T., Identification of 3α,4β,7α-trihydroxy-5β-cholanoic acid in human bile: reflection of a new pathway in bile acid metabolism in humans, J. Lipid Res., 1989, 30, 847-856. [all data]


Notes

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