3α,11β-dihydroxy-5α-androstan-17-one, MO-TMS
- Formula: C28H55NO3Si3
- Molecular weight: 537.9977
- IUPAC Standard InChI: InChI=1S/C28H55NO3Si3/c1-27-17-16-21(30-33(3,4)5)18-20(27)12-13-22-23-14-15-25(29-32-35(9,10)11)28(23,2)19-24(26(22)27)31-34(6,7)8/h20-24,26H,12-19H2,1-11H3/t20-,21+,22?,23?,24-,26?,27-,28-/m1/s1
- IUPAC Standard InChIKey: TVBYBJXCGVRLFJ-NXOPZDHZSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary |
|---|---|
| Active phase | OV-1 |
| Column length (m) | |
| Carrier gas | He |
| Substrate | |
| Column diameter (mm) | |
| Phase thickness (μm) | |
| Tstart (C) | 180. |
| Tend (C) | 250. |
| Heat rate (K/min) | 1. |
| Initial hold (min) | |
| Final hold (min) | |
| I | 2681. |
| Reference | Bègue, Dumas, et al., 1979 |
| Comment | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Bègue, Dumas, et al., 1979
Bègue, R.-J.; Dumas, M.; Morinière, M.; Nivois, C.; Padieu, P.,
Steroids and hypertension. 1-Gas-liquid chromatography and gas chromatography mass spectrometry of 3,15- and 3,16-dihydroxy-17-oxosteroids,
Biomed. Mass Spectrom., 1979, 6, 11, 476-481, https://doi.org/10.1002/bms.1200061104
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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