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Sorbose, acyclic, TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySE-54180.1866.García-Raso, Martínez-Castro, et al., 1987Column length: 40. m; Column diameter: 0.18 mm

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryFFAP170.1847.Garcia-Raso, Fernandez-Diaz, et al., 1989Column length: 24. m; Column diameter: 0.22 mm

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11828.Yang and Cashman, 199230. m/0.32 mm/1.0 «mu»m, He; Program: 3 min at 100 0C; 100 - 200 0C at 8 deg/min; 1 min at 200 0C; 200 - 280 0C at 5 deg/min; 30 min at 280 0C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

García-Raso, Martínez-Castro, et al., 1987
García-Raso, A.; Martínez-Castro, I.; Páez, M.I.; Sanz, J.; García-Raso, J.; Saura-Calixto, F., Gas Chromatographic Behaviour of Carbohydrate Trimethylsilyl Ethers. I. Aldopentoses, J. Chromatogr., 1987, 398, 9-20, https://doi.org/10.1016/S0021-9673(01)96491-X . [all data]

Garcia-Raso, Fernandez-Diaz, et al., 1989
Garcia-Raso, A.; Fernandez-Diaz, M.; Paez, M.I.; Sanz, J.; Martinez-Castro, I., Gas Chromatographic Retention of Carbohydrate Trimethylsilyl Ethers. III. Ketohexoses, J. Chromatogr., 1989, 471, 205-216, https://doi.org/10.1016/S0021-9673(00)94168-2 . [all data]

Yang and Cashman, 1992
Yang, Z.C.; Cashman, J.R., Structure-retention index relationships for derivatized monosaccharides on non-polar gas chromatography columns, J. Chromatogr., 1992, 596, 1, 79-84, https://doi.org/10.1016/0021-9673(92)80205-9 . [all data]


Notes

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