1,2,4,5,7,8-hexaoxacyclononane, 3,6,9-trimethyl, 3,6,9-triethyl


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5RTX-5 MSRTX-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.300.300.300.300.
Heat rate (K/min) 10.20.5.10.20.
Initial hold (min) 5.5.5.5.5.
Final hold (min)      
I 1353.11352.91368.61371.11370.3
ReferenceBarreto, Cañizo, et al., 2006Barreto, Cañizo, et al., 2006Barreto, Cañizo, et al., 2006Barreto, Cañizo, et al., 2006Barreto, Cañizo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase RTX-5 MSRTX-5 MS
Column length (m) 30.30.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (μm) 0.250.25
Tstart (C) 60.60.
Tend (C) 300.300.
Heat rate (K/min) 5.10.
Initial hold (min) 5. 
Final hold (min)   
I 1374.31361.4
ReferenceBarreto, Cañizo, et al., 2006Barreto, Cañizo, et al., 2006
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Barreto, Cañizo, et al., 2006
Barreto, G.P.; Cañizo, A.I.; Eyler, G.N., Use of Retention Data as the First Step in the Identification of Cyclic Organic Peroxides in Temperature-Programmed Gas Chromatography, Chromatographia, 2006, 63, 5-6, 261-266, https://doi.org/10.1365/s10337-006-0716-y . [all data]


Notes

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