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11-Deoxycortisol enol-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-13162.Pereira, Marques, et al., 200117. m/0.20 mm/0.11 «mu»m, Helium; Program: 180 0C 3 0C/min -> 229 0C 40 0C/min -> 310 0C (5 min)
PackedOV-13178.Chambaz, Defaye, et al., 1973Gas Chrom P; Column length: 2. m; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pereira, Marques, et al., 2001
Pereira, H.M.G.; Marques, M.A.S.; Cardoso, J.N.; Neto, F.R.A., Derivatization study of endogenous and synthetic corticosteroids by gas chromatography mass spectrometry in Recent Advances in Doping Analysis, Schanzer, W.; Geyer, H.; Gotzmann, A.; Mareck-Engelke, U., ed(s)., Sport und Buch Strauss, Koln, 2001, 203-207. [all data]

Chambaz, Defaye, et al., 1973
Chambaz, E.M.; Defaye, G.; Madani, C., Trimethyl silyl ether-enol-trimethyl silyl ether - A new type derivative for the gas phase study of hormonal steroids, Anal. Chem., 1973, 45, 7, 1090-1098, https://doi.org/10.1021/ac60329a035 . [all data]


Notes

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