3A,17A,20A,21-Tetrahydroxy-5B-pregnan-11-one, tetrakis-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-13038.Ludwig-Koehn and Henning, 198630. m/0.25 mm/0.25 μm, H2, 2. K/min; Tstart: 120. C; Tend: 280. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-1013066.Pfeifer and Spiteller, 1981H2, 2. K/min; Column length: 50. m; Column diameter: 0.30 mm; Tstart: 150. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ludwig-Koehn and Henning, 1986
Ludwig-Koehn, H.; Henning, H.V., Some aspects of quantification of neutral steroid metabolites in body fluids of healthy and uremic subjects by capillary gas chromatography, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 1, 35-38, https://doi.org/10.1002/jhrc.1240090106 . [all data]

Pfeifer and Spiteller, 1981
Pfeifer, P.; Spiteller, G., Steroid Profiles of Healthy Individuals, J. Chromatogr., 1981, 223, 1, 21-32, https://doi.org/10.1016/S0378-4347(00)80064-X . [all data]


Notes

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