Succinylacetone, O-pentafluorobenzyloxime, TMS
- Formula: C24H22F10N2O4Si
- Molecular weight: 620.5120
- IUPAC Standard InChI: InChI=1S/C24H22F10N2O4Si/c1-10(35-38-8-12-15(25)19(29)23(33)20(30)16(12)26)7-11(5-6-14(37)40-41(2,3)4)36-39-9-13-17(27)21(31)24(34)22(32)18(13)28/h5-9H2,1-4H3
- IUPAC Standard InChIKey: SYVIKTYZHWOGPK-UHFFFAOYSA-N
- Chemical structure:
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Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|
| Active phase | DB-1 | DB-1 | DB-1 | DB-1 |
| Column length (m) | 30. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He |
| Substrate | ||||
| Column diameter (mm) | 0.53 | 0.53 | 0.53 | 0.53 |
| Phase thickness (μm) | 1. | 1. | 1. | 1. |
| Tstart (C) | 70. | 70. | 70. | 70. |
| Tend (C) | 290. | 290. | 290. | 290. |
| Heat rate (K/min) | 4. | 4. | 4. | 4. |
| Initial hold (min) | ||||
| Final hold (min) | ||||
| I | 2434. | 2446. | 2461. | 2497. |
| Reference | Hoffmann, Aramaki, et al., 1989 | Hoffmann, Aramaki, et al., 1989 | Hoffmann, Aramaki, et al., 1989 | Hoffmann, Aramaki, et al., 1989 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Hoffmann, Aramaki, et al., 1989
Hoffmann, G.; Aramaki, S.; Blum-Hoffmann, E.; Nyhan, W.L.; Sweetman, L.,
Quantitative analysis for organic acids in biological samples: batch isolation followed by gas chromatographic-mass spectrometric analysis,
Clin. Chem., 1989, 35, 4, 587-595. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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