Bromazepam M (3-hydroxy-), hydrolysis, acetylated


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCross-Linked Methylsilicone2490.Maurer and Pfleger, 198712. m/0.2 mm/0.33 μm, He, 100. C @ 3. min, 30. K/min, 310. C @ 5. min

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS2490.Augsburger, Rivier, et al., 199830. m/0.25 mm/0.25 μm; Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Maurer and Pfleger, 1987
Maurer, H.; Pfleger, K., Identification and differentiation of benzodiazepines and their metabolites in urine by computerized gas chromatography-mass spectrometry, J. Chromatogr., 1987, 422, 85-101, https://doi.org/10.1016/0378-4347(87)80442-5 . [all data]

Augsburger, Rivier, et al., 1998
Augsburger, M.; Rivier, L.; Mangin, P., Comparison of different immunoassays and GC-MS screening of benzodiazepines in urine, J. Pharm. Biomed. Anal., 1998, 18, 4-5, 681-687, https://doi.org/10.1016/S0731-7085(98)00266-0 . [all data]


Notes

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