3«alpha»,6«beta»,7«alpha»,12«beta»-Tetrahydroxy-5«beta»-cholanoic acid, MeTMS


Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CB
Column length (m) 25.25.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.220.22
Phase thickness (mum)   
Tstart (C) 100.100.
Tend (C) 278.278.
Heat rate (K/min) 35.35.
Initial hold (min) 2.2.
Final hold (min)   
I 3243.3243.
ReferenceBatta and Salen, 1999Batta, Aggarwal, et al., 1995
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Batta and Salen, 1999
Batta, A.K.; Salen, G., Gas chromatography of bile acids, J. Chromatogr. B, 1999, 723, 1-2, 1-16, https://doi.org/10.1016/S0378-4347(98)00528-3 . [all data]

Batta, Aggarwal, et al., 1995
Batta, A.K.; Aggarwal, S.K.; Tint, G.S.; Batta, M.; Salen, G., Capillary gas-liquid chromatography of 6-hydroxylated bile acids, J. Chromatogr. A, 1995, 704, 1, 228-233, https://doi.org/10.1016/0021-9673(95)00183-N . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References