Pregnan-2,3,20-triol, TMS


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase Methyl SiliconeMethyl SiliconeCross-Linked Methylsilicone
Column length (m) 25.25.25.
Carrier gas    
Substrate    
Column diameter (mm) 0.320.320.32
Phase thickness (μm) 0.250.250.32
Program 60 0C 30 K/min -> 210 0C (1.5 min) 2.5 K/min -> 320 0C (20 min)60 0C 30 K/min -> 210 0C (1.5 min) 2.5 K/min -> 320 0C (20 min)60C => 30C/min => 210C (1.5min) => 2.5C/min => 320C (20min)
I 2899.2935.2949.
ReferenceMeng and Sjövall, 1997Meng and Sjövall, 1997Meng, Griffiths, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Meng and Sjövall, 1997
Meng, L.-J.; Sjövall, J., Method for combined analysis of profiles of conjugated progesterone metabolites and bile acids in serum and urine of pregnant women, J. Chromatogr. B, 1997, 688, 1, 11-26, https://doi.org/10.1016/S0378-4347(97)88051-6 . [all data]

Meng, Griffiths, et al., 1996
Meng, L.J.; Griffiths, W.J.; Sjövall, J., The identification of novel steroid N-acetylglucosaminides in the urine of pregnant women, J. Steroid Biochem., 1996, 58, 5/6, 585-598, https://doi.org/10.1016/0960-0760(96)00080-5 . [all data]


Notes

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