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Pregnan-2,3,20-triol, TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryMethyl Silicone2899.Meng and Sjövall, 199725. m/0.32 mm/0.25 «mu»m; Program: 60 0C 30 K/min -> 210 0C (1.5 min) 2.5 K/min -> 320 0C (20 min)
CapillaryMethyl Silicone2935.Meng and Sjövall, 199725. m/0.32 mm/0.25 «mu»m; Program: 60 0C 30 K/min -> 210 0C (1.5 min) 2.5 K/min -> 320 0C (20 min)
CapillaryCross-Linked Methylsilicone2949.Meng, Griffiths, et al., 199625. m/0.32 mm/0.32 «mu»m; Program: 60C => 30C/min => 210C (1.5min) => 2.5C/min => 320C (20min)

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Meng and Sjövall, 1997
Meng, L.-J.; Sjövall, J., Method for combined analysis of profiles of conjugated progesterone metabolites and bile acids in serum and urine of pregnant women, J. Chromatogr. B, 1997, 688, 1, 11-26, https://doi.org/10.1016/S0378-4347(97)88051-6 . [all data]

Meng, Griffiths, et al., 1996
Meng, L.J.; Griffiths, W.J.; Sjövall, J., The identification of novel steroid N-acetylglucosaminides in the urine of pregnant women, J. Steroid Biochem., 1996, 58, 5/6, 585-598, https://doi.org/10.1016/0960-0760(96)00080-5 . [all data]


Notes

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