7-Hydroxylupanine
- Formula: C15H24N2O2
- Molecular weight: 264.3633
- IUPAC Standard InChI: InChI=1S/C15H24N2O2/c18-14-6-3-4-12-11-8-15(19,10-17(12)14)13-5-1-2-7-16(13)9-11/h11-13,19H,1-10H2/t11?,12-,13+,15-/m0/s1
- IUPAC Standard InChIKey: KKYBYUIURCNNKY-FLTXBFBQSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Permanent link for this species. Use this link for bookmarking this species for future reference.
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 MS | 2265. | Cook, Lee, et al., 2009 | Column length: 30. m; Column diameter: 0.25 mm; Program: 100 0C (1 min) 40 0C/min -> 200 0C 5 0C/min -> 275 0C (15 min) |
| Capillary | DB-1 | 2275. | Wink, Meissner, et al., 1995 | Column length: 30. m; Column diameter: 0.3 mm; Program: not specified |
| Capillary | DB-1 | 2270. | Greinwald, Witte, et al., 1991 | He; Column length: 30. m; Column diameter: 0.32 mm; Program: 150C (2min) => 10C/min => 250C => 20C/min => 300C (5min) |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Cook, Lee, et al., 2009
Cook, D.; Lee, S.T.; GArdner, D.R.; Pfister, J.A.; Welch, K.D.; Green, B.T.; Davis, T.Z.; Panter, K.E.,
The alkaloids profiles of lupinus sulphureus,
J. Agric. Food Chem., 2009, 57, 4, 1646-1653, https://doi.org/10.1021/jf803468q
. [all data]
Wink, Meissner, et al., 1995
Wink, M.; Meissner, C.; Witte, L.,
Patterns of quinolizidine alkaloids in 56 species of the genus Lupinus,
Phytochemistry, 1995, 38, 1, 139-153, https://doi.org/10.1016/0031-9422(95)91890-D
. [all data]
Greinwald, Witte, et al., 1991
Greinwald, R.; Witte, L.; Wray, V.; Czygan, F.-C.,
The alkaloid pattern of Cytisophyllum sessilitolium (Fabaceae-Genisteae),
Biochem. Syst. Ecol., 1991, 19, 3, 253-258, https://doi.org/10.1016/0305-1978(91)90010-W
. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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