Acetic acid 4,5-dimethoxy-2-methoxy methyl-tetrahydro-pyran-3-yl ester


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillary
Active phase HP-1HP-5DB-5
Column length (m) 30.30.30.
Carrier gas    
Substrate    
Column diameter (mm) 0.250.530.25
Phase thickness (μm) 0.251.0.25
Tstart (C) 110.110.80.
Tend (C) 240.240.300.
Heat rate (K/min) 2.2.1.
Initial hold (min) 2.2. 
Final hold (min) 20.20. 
I 1509.741528.581535.79
ReferenceLee, Kim, et al., 1999Lee, Kim, et al., 1999Lee and Gray, 1995
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lee, Kim, et al., 1999
Lee, C.K.; Kim, E.J.; Jun, J.H., Determination of relative reactivities of free hydroxyl groups in β-cyclodextrin, amylose, and cellulose by reduction-cleavage method, Bull. Korean Chem. Soc., 1999, 20, 10, 1153-1158. [all data]

Lee and Gray, 1995
Lee, C.K.; Gray, G.R., Analysis of positions of substitution of O-acetyl groups in partially O-acetylated cellulose by the reductive-cleavage method, Carbohyd. Res., 1995, 269, 1, 167-174, https://doi.org/10.1016/0008-6215(94)00354-I . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References