Methionine-asparagine-threonine, N(α,ε)-trifluoroacetyl-N-O-permethyl derivative


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillary
Active phase CP Sil 5 CBSE-54
Column length (m) 5.5.
Carrier gas HeHe
Substrate   
Column diameter (mm) 0.340.34
Phase thickness (μm) 0.40.4
Tstart (C) 80.80.
Tend (C) 320.320.
Heat rate (K/min) 4.4.
Initial hold (min) 1.1.
Final hold (min)   
I 2959.3033.
ReferenceRose, Bairoch, et al., 1983Rose, Bairoch, et al., 1983
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Rose, Bairoch, et al., 1983
Rose, K.; Bairoch, A.; Offord, R.E., Amino acid sequence determination by gas chromatography-mass spectrometry of permethylated peptides. The application of capillary columns, J. Chromatogr., 1983, 268, 197-206, https://doi.org/10.1016/S0021-9673(01)95406-8 . [all data]


Notes

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