3-Hydroxy-stearic acid, methyl ester, 3-tBDMS ether


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase Methyl Silicone
Column length (m) 30.
Carrier gas He
Substrate  
Column diameter (mm) 0.25
Phase thickness (μm) 0.25
Tstart (C) 80.
Tend (C) 340.
Heat rate (K/min) 5.
Initial hold (min) 4.
Final hold (min)  
I 2535.
ReferenceChance, Gerhardt, et al., 1998
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Chance, Gerhardt, et al., 1998
Chance, D.L.; Gerhardt, K.O.; Mawhinney, T.P., Gas-liquid chromatography--mass spectrometry of hydroxy fatty acids as their methyl esters tert.-butyldimethylsilyl ethers, J. Chromatogr. A, 1998, 793, 1, 91-98, https://doi.org/10.1016/S0021-9673(97)00876-5 . [all data]


Notes

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