5-Cholesten-3-β,27-diol-17,22-dione, TMS


Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase Methyl Silicone
Column length (m) 25.
Carrier gas  
Substrate  
Column diameter (mm) 0.32
Phase thickness (μm) 0.25
Tstart (C) 60.
Tend (C) 290.
Heat rate (K/min) 30.
Initial hold (min)  
Final hold (min)  
I 3795.
ReferenceShoda, Axelson, et al., 1993
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Shoda, Axelson, et al., 1993
Shoda, J.; Axelson, M.; Sjövall, J., Synthesis of potential C27-intermediates in bile acid biosynthesis and their deuterium-labeled analogs, Steroids, 1993, 58, 3, 119-125, https://doi.org/10.1016/0039-128X(93)90048-R . [all data]


Notes

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