5β-Androst-1-en-17β-ol-3-one, TMS
- Formula: C25H44O2Si2
- Molecular weight: 432.7867
- IUPAC Standard InChI: InChI=1S/C25H44O2Si2/c1-24-15-13-19(26-28(3,4)5)17-18(24)9-10-20-21-11-12-23(27-29(6,7)8)25(21,2)16-14-22(20)24/h13,15,17-18,20-23H,9-12,14,16H2,1-8H3/t18-,20?,21?,22?,23+,24+,25+/m0/s1
- IUPAC Standard InChIKey: MHYUVCDDDLAFJG-VTHHSRKNSA-N
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: 5β-Androst-1-en-17β-ol-3-one,bis-TMS; 1,3(5β)-androsten-3,17β-diol di-TMS
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Normal alkane RI, non-polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary |
|---|---|---|
| Active phase | SE-54 | SE-54 |
| Column length (m) | 20. | 15. |
| Carrier gas | He | He |
| Substrate | ||
| Column diameter (mm) | 0.25 | 0.2 |
| Phase thickness (μm) | 0.33 | 0.33 |
| Tstart (C) | 200. | 200. |
| Tend (C) | 300. | 300. |
| Heat rate (K/min) | 5. | 5. |
| Initial hold (min) | ||
| Final hold (min) | ||
| I | 2467. | 2480. |
| Reference | Schänzer and Donike, 1992 | Schänzer and Donike, 1992 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Schänzer and Donike, 1992
Schänzer, W.; Donike, M.,
Metabolism of boldenone in man: gas chromatographic/mass spectrometric identification of urinary excreted metabolites and determination of excretion rates,
Biol. Mass Spectrom., 1992, 21, 1, 3-16, https://doi.org/10.1002/bms.1200210104
. [all data]
Notes
Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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