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3-epi-GA1 methyl ester TMS ether


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-12790.Emery, Pearce, et al., 2001He; Column diameter: 0.25 mm; Phase thickness: 0.25 «mu»m; Program: 60C(0.1min) => 20C/min => 200C => 5C/min => 300C
CapillaryDB-12790.Emery, Pearce, et al., 2001He; Column diameter: 0.25 mm; Phase thickness: 0.25 «mu»m; Program: 60C(0.1min) => 20C/min => 200C => 5C/min => 300C
CapillaryBP-12807.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C
CapillaryBP-12807.Hedden, Croker, et al., 198925. m/0.32 mm/0.33 «mu»m, He; Program: 50C(1min) => 20C/min => 240C => 4C/min => 295C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryOV-12793.Kobayashi, MacMillan, et al., 2000He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryCP Sil 5 CB2824.Taylor, Blake, et al., 2000He; Column length: 25. m; Column diameter: 0.25 mm; Program: 60C(0.7min) => 20C/min => 220C => 4C/min => 300C
CapillaryOV-12783.Davis, Kobayashi, et al., 199825. m/0.2 mm/0.25 «mu»m, He; Program: 60C(2min) => 10min/C => 150C => 3C/min => 300C
CapillaryOV-12793.Kobayashi, Gaskin, et al., 1994He; Column length: 25. m; Column diameter: 0.2 mm; Program: 60C(2min) => 13C/min => 150C => 3C/min => 280C(10min)
CapillaryOV-12793.Kobayashi, Gaskin, et al., 199325. m/0.2 mm/0.25 «mu»m; Program: 50C(2min) => 10C/min => 150C => 3C/min => 300C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Emery, Pearce, et al., 2001
Emery, R.J.N.; Pearce, D.W.; Pharis, R.P.; Reid, D.M.; Chinnappa, C.C., Stem elongation and gibberellins in alpine and prairie ecotypes of Stellaria longipes, Plant Growth Regul., 2001, 35, 1, 17-29, https://doi.org/10.1023/A:1013823517189 . [all data]

Hedden, Croker, et al., 1989
Hedden, P.; Croker, S.J.; Rademacher, W.; Jung, J., Effects of the triazole plant growth retardant BAS 111..W on gibberellin levels in oilseed rape, Brassica napus, Physiol. Plant., 1989, 75, 4, 445-451, https://doi.org/10.1111/j.1399-3054.1989.tb05607.x . [all data]

Kobayashi, MacMillan, et al., 2000
Kobayashi, M.; MacMillan, J.; Phinney, B.; Gaskin, P.; Spray, C.R.; Hedden, P., Gibberellin biosynthesis: metabolic evidence for three steps in the early 13-hydroxylation pathway of rice, Phytochemistry, 2000, 55, 4, 317-321, https://doi.org/10.1016/S0031-9422(00)00265-X . [all data]

Taylor, Blake, et al., 2000
Taylor, D.R.; Blake, P.S.; Crisp, C.M., Identification of gibberellins in leaf exudates of strawberry (Fragaria ananassa Duch.), Plant Growth Regul., 2000, 30, 3, 221-223, https://doi.org/10.1023/A:1006385617161 . [all data]

Davis, Kobayashi, et al., 1998
Davis, G.; Kobayashi, M.; Phinney, B.O.; MacMillan, J.; Gaskin, P., The Metabolism of GA9 in maize (ZEA mays), Phytochemistry, 1998, 47, 4, 635-639, https://doi.org/10.1016/S0031-9422(97)87974-5 . [all data]

Kobayashi, Gaskin, et al., 1994
Kobayashi, M.; Gaskin, P.; Spray, C.R.; Phinney, B.O.; MacMillan, J., The metabolism of gibberellin A20 to gibberellin A1 by tall and dwarf mutants of Oryza sativa and Arabidopsis thaliana, Plant Physiol., 1994, 106, 1367-1372. [all data]

Kobayashi, Gaskin, et al., 1993
Kobayashi, M.; Gaskin, P.; Spray, C.R.; Suzuki, Y.; Phinney, B.O.; MacMillan, J., Metabolism and biological activity of Gibberellin A4 in vegetative shoots of Zea mays, Oryza sativa, and Arabidopsis thaliana, Plant Physiol., 1993, 102, 379-386. [all data]


Notes

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