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3«alpha»,16«alpha»,17«beta»-Trihydroxy-5«alpha»-androstane, tris-TMS


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-302774.Ludwig-Köhn, Sziedat, et al., 1980He, 2. K/min; Column length: 20. m; Tstart: 150. C; Tend: 295. C
PackedSE-302778.Grote and Spiteller, 1977Chromosorb W AW DMCS, 1. K/min; Column length: 1.5 m; Tstart: 200. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryBP-12785.Hähnel, Wilkinson, et al., 1985He; Column length: 25. m; Column diameter: 0.3 mm; Program: 40C (1min) => 20C/min => 200C => 2C/min => 300C (11min)

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ludwig-Köhn, Sziedat, et al., 1980
Ludwig-Köhn, H.; Sziedat, A.; Spiteller, G.; Matthaei, D.; Henning, H.V.; Scheler, F., Occurrence of highly oxygen-substituted androgens in hemofiltrates of uremic patients, Biomed. Mass Spectrom., 1980, 7, 7, 284-287, https://doi.org/10.1002/bms.1200070704 . [all data]

Grote and Spiteller, 1977
Grote, H.; Spiteller, G., Location of Functional Groups with the Aid of Mass Spectrometry. XVI-Mass Spectra of Trimethylsilylated Androstan-3,16,17«beta»-triols, Biomed. Mass Spectrom., 1977, 4, 4, 216-219, https://doi.org/10.1002/bms.1200040405 . [all data]

Hähnel, Wilkinson, et al., 1985
Hähnel, E.; Wilkinson, S.P.; Hähnel, R., Urinary steroid profiles in pregnancy by capillary column gas chromatography, Clin. Chim. Acta, 1985, 151, 3, 259-271, https://doi.org/10.1016/0009-8981(85)90089-0 . [all data]


Notes

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