5-«alpha»,16-Androsten-3-one, TMS


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type Capillary
Active phase OV-1
Column length (m) 25.
Carrier gas  
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.25
Program 80 0C (5 min) 40 K/min -> 120 0C (2 min) 2 K/min -> 200 0C (for androstanes), or 80 0C (5 min) 40 K/min -> 190 0C (2 min) 2 K/min -> 270 0C (for sterols)
I 2155.
ReferenceBrooks, Cole, et al., 1983
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Brooks, Cole, et al., 1983
Brooks, C.J.W.; Cole, W.J.; Lawrie, T.D.V.; MacLachlan, J.; Borthwick, J.H.; Barrett, G.M., Selective reactions in the analytical characterisation of steroids by gas chromatography-mass spectrometry, J. Steroid Biochem., 1983, 19, 1, 189-201, https://doi.org/10.1016/S0022-4731(83)80025-9 . [all data]


Notes

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