p-Cymene

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Polydimethyl siloxane: CP-Sil 5 CBHP-5 MSOptima-5RTX-1
Column length (m) 30.60.60.30.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (μm) 0.251.00.250.250.25
Tstart (C) 60.45.40.60.60.
Tend (C) 300.210.250.246.230.
Heat rate (K/min) 4.3.63.3.2.
Initial hold (min) 3.1.451.1. 
Final hold (min) 15.2.7220. 5.
I 1024.1016.1028.1032.1015.
ReferenceBertuzzi, Tirillini, et al., 2013Bramston-Cook, 2013Sardashti, Valizadeh, et al., 2013Al-Qudah, Muhaidat, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1BP-1Mega-5HP-5 MSHP-5 MS
Column length (m) 60.30.25.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.40.35.
Tend (C) 230.275.220.250.300.
Heat rate (K/min) 2.4.3.3.3.
Initial hold (min)   1.1.5.
Final hold (min) 5. 5.3.15.
I 1015.1026.1025.1025.1020.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Dehshahri, Afsharypuor, et al., 2012Dell'Agli, Sanna, et al., 2012Jian-Yu, Zhu, et al., 2012Kotowska, Zalikowski, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Petrocol DHPetrocol DHHP-5HP-5HP-5
Column length (m) 100.100.25.25.25.
Carrier gas HeliumHeliumHydrogenHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.500.500.520.520.52
Tstart (C) 20.20.40.40.40.
Tend (C) 220.220.280.280.280.
Heat rate (K/min) 15.15.4.4.4.
Initial hold (min) 15.15.   
Final hold (min) 30.30.10.10.10.
I 1014.1016.1021.1021.1021.
ReferenceSupelco, 2012Supelco, 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5 MSHP-1CP-Sil 5 CBHP-5
Column length (m) 60.30.30.25.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.150.25
Tstart (C) 60.50.60.50.60.
Tend (C) 230.250.240.220.240.
Heat rate (K/min) 2.7.3. 3.
Initial hold (min)  1.   
Final hold (min) 45.5.   
I 1008.1027.1024.1022.1025.
ReferenceYapi, Boti, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011Ameen, Usman, et al., 2011Bertoli, Lepnardi, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP-Sil 5 CBDB-1VF-5 MSVF-5 MS
Column length (m) 30.25.30.60.60.
Carrier gas HeliumHydrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.150.250.250.25
Tstart (C) 40.50.40.30.30.
Tend (C) 250.230.210.260.260.
Heat rate (K/min) 3.3.5.2.2.
Initial hold (min) 5.    
Final hold (min) 20.  28.28.
I 1031.1022.1028.1025.1027.
ReferenceCao, Li, et al., 2011Esseien, Aboaba, et al., 2011Fathi, Sahari, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30 MSCP-Sil 5 CBMethylsiloxane + 5 % Ph-groupsZB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumNitrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.260.250.250.25
Tstart (C) 50.45.60.40.50.
Tend (C) 250.280.230.200.300.
Heat rate (K/min) 5.3.7.5.50.
Initial hold (min) 5. 2.5.5.
Final hold (min) 10.22.20. 5.
I 1025.1015.1026.1025.1026.
ReferenceMenichini, Tundis, et al., 2011Mothana, Hasson, et al., 2011Nadim, Malik, et al., 2011Vazques, Aimar, et al., 2011Bi Kouame, Bedi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5 MSZB-5 MSDB-5 MSDB-5 MSRTx-1
Column length (m) 30.30.25.25.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.300.300.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.60.
Tend (C) 290.290.240.240.230.
Heat rate (K/min) 5.5.3.3.2.
Initial hold (min)      
Final hold (min)     35.
I 1026.1027.1025.1025.1015.
ReferenceBoix, Victorio, et al., 2010Boix, Victorio, et al., 2010Chalchat, Figueredo, et al., 2010Chalchat, Figueredo, et al., 2010Dib, Bendahou, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1SPB-1DB-5DB-1DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.30.60.50.50.
Tend (C) 230.250.280.265.250.
Heat rate (K/min) 2.4.3.2.52.
Initial hold (min)  3. 1. 
Final hold (min) 30.10. 20. 
I 1015.1046.1020.1018.1025.
ReferenceDib, Djabou, et al., 2010Escalona-Arranz, Perez-Roses, et al., 2010Georgiou, Koutsaviti, et al., 2010Hajimahdipoor, Samadi, et al., 2010Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5 MSDB-5 MSBP-1
Column length (m) 30.30.30.60. 
Carrier gas NitrogenHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.70.70.40.60.
Tend (C) 240.200.290.250.220.
Heat rate (K/min) 3.3.5.5.5.
Initial hold (min) 1.2. 15.10.
Final hold (min) 9.18. 15.30.
I 1026.1031.1028.1029.1015.
ReferenceJardim, Jham, et al., 2010Jerkovic and Marijanovic, 2010Lazarevic, Radulovic, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5SPB-1HP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (μm) 0.250.250.200.250.25
Tstart (C) 40.50.70.60.60.
Tend (C) 260.240.220.220.220.
Heat rate (K/min) 4.3.3.5.5.
Initial hold (min)  5. 10.10.
Final hold (min) 5. 15.  
I 1026.1023.1011.1028.1029.
ReferenceMiyazawa, Kawauchi, et al., 2010Monsef-Esfahani, Miri, et al., 2010Neves, Rosa, et al., 2010Ogunwande, Flamini, et al., 2010Ogunwande, Flamini, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5 MSDB-1SLB-5 MS
Column length (m) 30.30.30.60.10.
Carrier gas HeliumHydrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.10
Phase thickness (μm) 0.250.250.250.250.10
Tstart (C) 70.70.70.60.50.
Tend (C) 290.290.290.250.250.
Heat rate (K/min) 5.5.5.4.10.
Initial hold (min)    1. 
Final hold (min) 10. 10.10. 
I 1027.1029.1027.1014.1024.
ReferenceRadulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Safaei-Ghomi, Meshkatalsadat, et al., 2010Scandinaro, Tranchida, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSDB-1-MSDB-5DB-5HP-5MS
Column length (m) 10.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.100.250.250.250.25
Phase thickness (μm) 0.100.250.250.250.25
Tstart (C) 50.30.80.40.50.
Tend (C) 250.200.240.250.250.
Heat rate (K/min) 10.2.3.10.7.
Initial hold (min)  4. 1.1.
Final hold (min)  35.2.3.5.
I 1025.1008.1024.1032.1031.
ReferenceScandinaro, Tranchida, et al., 2010Takeoka, Hobbs, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010Yang, Zhang, et al., 2010Zouari, Zouari, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101SE-54HP-5 MSZB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.70.60.60.50.
Tend (C) 240.220.260.250.240.
Heat rate (K/min) 3.2.2.2.3.
Initial hold (min)   5.8. 
Final hold (min)   999.15.1.
I 1025.1014.1024.1030.1009.
ReferenceAlim, Goze, et al., 2009Benites, Moiteiro, et al., 2009Dayisoylu and Alma, 2009Farhat, Ginies, et al., 2009Gardini, Beletti, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5DB-5DB-5
Column length (m) 60.30.50.30.30.
Carrier gas NitrogenHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.350.250.200.250.25
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 60.50.60.50.70.
Tend (C) 230.250.220.250.240.
Heat rate (K/min) 4.5.5.5.5.
Initial hold (min)  2.3.  
Final hold (min) 40.    
I 1028.1025.1026.1033.1026.
ReferenceGauvin-Bialecki and Marodon, 2009Ho, Wang, et al., 2009Kazemi and Akhavani, 2009Koba, Catherine, et al., 2009Lawal and Oyedelji, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5RTX-1RTX-1BP-1
Column length (m) 60.25.60.60.50.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.220.220.22
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 250.240.230.230.220.
Heat rate (K/min) 3.3.2.2.2.
Initial hold (min)      
Final hold (min)  7.30.30.20.
I 1026.1024.1013.1015.1013.
ReferenceMales, Plazibat, et al., 2009Maridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Ottavioli, Bighelli, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-5DB-55 % Phenyl methyl siloxaneMega 5 MS
Column length (m) 60.30.30.60.60.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.45.40.90.40.
Tend (C) 330.250.250.225.240.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 12.3.1. 2.
Final hold (min) 30.5.10.3. 
I 1012.1024.1015.1025.1015.
ReferencePatil, Jayaprakasha, et al., 2009Porto, Decorti, et al., 2009Rahimi-Nasrabadi, Gholivand, et al., 2009Retta, Gattuso, et al., 2009Romeo, Verzera, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1 MSDB-5SPB-5DB-5 MS
Column length (m) 30.30.50.60.30.
Carrier gas NitrogenHeliumNitrogen Helium
Substrate      
Column diameter (mm) 0.250.250.200.320.25
Phase thickness (μm) 0.250.250.321.000.25
Tstart (C) 40.40.60.40.40.
Tend (C) 230.250.220.230.250.
Heat rate (K/min) 2.6.5.3.4.
Initial hold (min)  1.3.5.2.
Final hold (min)  4.5.10.2.
I 1025.1012.1026.1034.1028.
ReferenceScrivanti, Anton, et al., 2009Seo, Kim, et al., 2009Shafaghat and Sadeghi, 2009Sivadier, Ratel, et al., 2009Su, Wang, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSHP-5 MSHP-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.50.50.70.
Tend (C) 240.325.280.280.220.
Heat rate (K/min) 5.10.4.9.3.
Initial hold (min)  6. 3.1.
Final hold (min)  10. 3. 
I 1026.1024.1024.1026.1020.
ReferenceWannes, Mhamdi, et al., 2009Zaibunnisa, Norashikin, et al., 2009Zhao, Zeng, et al., 2009Aicha, Ines, et al., 2008Ali, Wurster, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas  N2NitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 60.60.60.100.100.
Tend (C) 280.220.240.300.300.
Heat rate (K/min) 3.5.3.20.20.
Initial hold (min)  10.1.2.2.
Final hold (min)   9.10.10.
I 1022.1028.1026.1006.1009.
ReferenceBaziou, Couladis, et al., 2008Flamini, Tebano, et al., 2008Jardin, Jham, et al., 2008Khokra, Prakash, et al., 2008Khokra, Prakash, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSZB-1HP-5 MSBPX-5RTX-5
Column length (m) 30.30.30.7.520.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.100.18
Phase thickness (μm) 0.250.250.2510.0.20
Tstart (C) 50.45.50.60.50.
Tend (C) 250.230.240.240.280.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min) 2.   1.
Final hold (min) 10.    
I 1024.1007.991.1032.1029.
ReferenceLo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Sarikurkcu, Tepe, et al., 2008Shellie, 2008Skalicka-Wozniak, Los, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5OV-1HP-5HP-5 MSSE-54
Column length (m) 25.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 60.65.60.50.60.
Tend (C) 240.260.250.230.260.
Heat rate (K/min) 4.6.5.3.2.
Initial hold (min) 2. 30.10.5.
Final hold (min)    10.20.
I 1028.1019.1025.1026.1023.
ReferenceVerdian-rizi, 2008Wang, Yi, et al., 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Alma, Ertas, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSCP Sil 5 CBHP-5MSSE-52
Column length (m) 50.30.30.30.30.
Carrier gas NitrogenHeliumN2He 
Substrate      
Column diameter (mm) 0.200.250.320.250.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.200.300.280.220.
Heat rate (K/min) 5.4.4.3.3.
Initial hold (min) 3.   1.
Final hold (min) 5.20.  5.
I 1017.1022.1013.1021.1011.
ReferenceAmiri, 2007Araque, Rojas, et al., 2007Baran, von Reuss, et al., 2007Basta, Tzakou, et al., 2007Bicchi, Cordero, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5DB-5DB-5MS
Column length (m) 30.30.30.60.30.
Carrier gas HeHeliumN2HeHe
Substrate      
Column diameter (mm) 0.260.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.40.60.
Tend (C) 240.280.240.220.240.
Heat rate (K/min) 3.4.5.3.3.
Initial hold (min)  5.1.  
Final hold (min)   4.  
I 1019.1024.1026.1039.1026.
ReferenceBos, Woerdenbag, et al., 2007Capetanos, Saroglou, et al., 2007Cheraif, Ben Jannet, et al., 2007Chyau, Tsai, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1DB-55 % Phenyl methyl siloxane
Column length (m) 30.30.60.30.60.
Carrier gas HeliumHeliumNitrogenHeHe
Substrate      
Column diameter (mm) 0.260.250.250.250.25
Phase thickness (μm) 0.250.260.250.250.25
Tstart (C) 60.60.60.60.90.
Tend (C) 290.240.250.210.225.
Heat rate (K/min) 3.4.4.30.3.
Initial hold (min)  2.1.3. 
Final hold (min)  20.10. 15.
I 1019.1023.1018.1019.1012.
ReferenceElfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007Ghasempour, Shirinpour, et al., 2007Ghasemi, Yamini, et al., 2007Gil A., Van Baren C.M., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Col-Elite 5MSHP-1DBP-5RTX-5 MSDB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.220.250.25
Tstart (C) 30.60.40.45.60.
Tend (C) 246.240.250.210.300.
Heat rate (K/min) 3.2.3.3.3.
Initial hold (min)   1.  
Final hold (min)  20.10.  
I 1024.1009.998.1024.1017.
ReferenceGudaityte and Venskutonis R.P., 2007Hachicha, Skanji, et al., 2007Heravi and Sereshti, 2007Hudaib and Aburjai, 2007Limberger, Scopel, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30HP-5DB-5MSAT-5ZB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 250.250.280.260.220.
Heat rate (K/min) 5.5.3.4.4.
Initial hold (min) 5.5.  5.
Final hold (min) 10.10.30. 20.
I 1025.1023.998.1031.1025.
ReferenceLoizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Marongiu B., Piras A., et al., 2007Meccia, Rojas, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5DB-5HP-5
Column length (m) 30.30.30.30.25.
Carrier gas HeliumHeliumHeliumHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.320.33
Tstart (C) 50.60.60.50.60.
Tend (C) 260.300.220.250.240.
Heat rate (K/min) 2.53.4.5.3.
Initial hold (min) 1.    
Final hold (min) 20.    
I 1007.1002.1027.1014.1028.
ReferenceMonser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Nori-Shargh, Raftari, et al., 2007Oliveira, Leitão, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-1DB-5SPB-5BPX-5
Column length (m) 50.30.30.30.50.
Carrier gas HeHeHydrogenHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.22
Phase thickness (μm) 0.250.20.250.251.
Tstart (C) 95.70.50.50.50.
Tend (C) 240.220.250.250.300.
Heat rate (K/min) 4.3.4.2.4.
Initial hold (min)     1.
Final hold (min)  15.  10.
I 1023.1012.1021.1021.1046.
ReferencePala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007Pontes, de Olivera, et al., 2007Raal, Orav, et al., 2007Rali, Wossa, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5DB-1HP-5DB-1DB-1
Column length (m) 50.60.30.60.60.
Carrier gas HeNitrogenHelium He
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 50.60.40.60.60.
Tend (C) 300.250.260.250.250.
Heat rate (K/min) 4.4.4.5.5.
Initial hold (min) 1.1.   
Final hold (min) 10.10.   
I 1045.1018.1019.1022.1014.
ReferenceRali, Wossa, et al., 2007Reza, Ebrahim, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Salehi, Asghari, et al., 2007Salehi, Fakhari, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DBP-5DB-5DB-5HP-5 MS
Column length (m) 30.25.30.30.30.
Carrier gas HeHelium  Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.220.250.250.25
Tstart (C) 50.40.40.40.60.
Tend (C) 240.250.210.250.280.
Heat rate (K/min) 4.3.2.2.3.
Initial hold (min)  1.   
Final hold (min)  10.33.33. 
I 1023.998.1025.1025.1025.
ReferenceSefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007Sylvestre, Longtin, et al., 2007Sylvestre, Pichette, et al., 2007Vagionas, Graikou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5HP-5CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (μm) 0.250.320.250.25 
Tstart (C) 40.60.50.50.80.
Tend (C) 250.250.280.280.270.
Heat rate (K/min) 3.5.9.9.10.
Initial hold (min) 5.30.3.3. 
Final hold (min) 10. 3.3. 
I 1020.1025.1023.1024.1015.
ReferenceVichi, Riu-Aumatell, et al., 2007Yassa and Akhani, 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Ayoub, Al-Azizi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1ZB-5AT-5BP-1
Column length (m) 30.50.30.60.50.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.22
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 50.60.40.60.60.
Tend (C) 265.250.300.200.220.
Heat rate (K/min) 2.52.2.4.2.
Initial hold (min) 1.    
Final hold (min) 20.20. 20.20.
I 1023.1011.1025.1023.1010.
ReferenceBazargani, Almasirad, et al., 2006Berlioz, Cordella, et al., 2006Biondi, Sari, et al., 2006Borges, Rojas, et al., 2006Boti, Muselli, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5MSHP-1HP-1HP-1
Column length (m) 50.30.50.50.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.20.20.2
Phase thickness (μm) 0.250.250.330.330.33
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.250.250.250.
Heat rate (K/min) 2.3.2.2.2.
Initial hold (min)   4.4.4.
Final hold (min) 20. 30.30.30.
I 1013.1026.1006.1012.1014.
ReferenceBoti, Yao, et al., 2006Bozin, Mimicá-Dukic, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1SPB-1DB-1DB-5
Column length (m) 50.50.30.60.30.
Carrier gas HeHeHeliumNitrogenN2
Substrate      
Column diameter (mm) 0.20.20.200.250.25
Phase thickness (μm) 0.50.330.20 0.25
Tstart (C) 60.60.70.40.70.
Tend (C) 250.250.220.200.230.
Heat rate (K/min) 2.2.3.2.2.
Initial hold (min)  4. 1.2.
Final hold (min) 120.30.15.9.20.
I 1017.1017.1011.1010.1027.
ReferenceCastel, Fernandez, et al., 2006, 2Castel, Fernandez, et al., 2006, 2Cavaleiro, Pinto, et al., 2006Chen, Sheu, et al., 2006Choi, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5MSDB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas He  HeliumHe
Substrate      
Column diameter (mm) 0.320.320.250.260.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 246.230.280.290.220.
Heat rate (K/min) 3.3.4.3.2.
Initial hold (min)      
Final hold (min)  15.  20.
I 1023.1026.1028.1019.1011.
ReferenceCoronel, Cerda-Garcia-Rojas, et al., 2006Damjanovic, Skala, et al., 2006Ebrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Fanciullino, Tomi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-1HP-5HP-1DB-1
Column length (m) 50.50.30.50.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.20.250.20.25
Phase thickness (μm) 0.250.330.250.330.25
Tstart (C) 60.60.50.60.60.
Tend (C) 220.250.300.250.240.
Heat rate (K/min) 2.2.5.2.5.
Initial hold (min)   5. 2.
Final hold (min) 20.60.5.40. 
I 1011.1009.1029.1012.1017.
ReferenceFanciullino, Tomi, et al., 2006Fernandez, Pintaric, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-1DB-5
Column length (m) 30.60.30.60.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 240.240.240.250.250.
Heat rate (K/min) 5.5.5.5.3.
Initial hold (min) 2.2.2.  
Final hold (min)    10.10.
I 1026.1017.1026.1016.1025.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Hadian, Sonboli, et al., 2006Havlik, Kokoska, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5HP-5MSDB-5CP Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas  HeHeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 40.60.60.60.50.
Tend (C) 220.240.260.260.230.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min)      
Final hold (min) 3.    
I 1025.1026.1026.1025.1016.
ReferenceHymete, Rohloff, et al., 2006Ibañez and Usubillaga, 2006Ibanez and Usubillaga, 2006Javidnia, Miri, et al., 2006Kasali, Ekundayo, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSMethyl SiliconeRTX-1DB-1CP Sil 5 CB
Column length (m) 30.25.30.60.30.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.90.60.70.50.
Tend (C) 280.220.300.230.300.
Heat rate (K/min) 5.7.4.2.4.
Initial hold (min) 4.2. 2. 
Final hold (min) 10.  20. 
I 1027.1013.1012.1012.1017.
ReferenceKim, El-Aty, et al., 2006Kitchlu, Bakshi, et al., 2006Kula, Izydorczyk, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Lis and Milczarek, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5 MSHP-5DB-5MS5 % Phenyl methyl siloxane
Column length (m) 30.30.30.30.30.
Carrier gas N2NitrogenN2HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.520.250.25
Tstart (C) 50.50.50.60.60.
Tend (C) 200.280.280.280.280.
Heat rate (K/min) 5.5.5.3.3.
Initial hold (min)      
Final hold (min)  5.5.30.30.
I 1020.1026.1026.1003.999.
ReferenceMartin, Joseph, et al., 2006Marzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Maronigiu, Piras, et al., 2006Marongiu, Piras, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 250.220.220.220.265.
Heat rate (K/min) 3.4.4.4.2.5
Initial hold (min) 5. 5.5.0.5
Final hold (min)      
I 1024.1027.1027.1027.1013.
ReferenceMirza, Navaei, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani K., Akbarzadeh M., et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Nickavar B., Kamalinejad M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBNB-30DB-5SE-52DB-5
Column length (m) 25.30.25.50.30.
Carrier gas HydrogenHeN2HeliumHe
Substrate      
Column diameter (mm) 0.250.20.250.250.32
Phase thickness (μm) 0.150.250.15 0.25
Tstart (C) 50.50.50.50.60.
Tend (C) 230.250.200.240.280.
Heat rate (K/min) 3.2.4.3.5.
Initial hold (min)   3. 0.5
Final hold (min)     2.
I 1016.1015.1020.1026.1027.
ReferenceOlawore, Usman, et al., 2006Orav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Ozcan, Chalchat, et al., 2006Ozel, Gogus, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSSPB-5DB-5DB-5
Column length (m) 50.30.30.30.30.
Carrier gas N2HeHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 95.40.60.70.70.
Tend (C) 240.260.250.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min)   2.4.4.
Final hold (min)   20.  
I 1018.1025.1025.1025.1026.
ReferencePala-Paul J., Perez-Alonso M.J., et al., 2006Petrovic, Ristic, et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5MSHP-5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HydrogenH2HeH2 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.50.60.60.50.
Tend (C) 280.280.280.240.250.
Heat rate (K/min) 4.4.3.3.10.
Initial hold (min) 4.2.  5.
Final hold (min)  10.   
I 1026.1026.994.1028.1024.
ReferencePino, Marbot, et al., 2006Pino, Sauri-Duch, et al., 2006Pitarokili, Tzakou, et al., 2006Potzernheim, Bizzo, et al., 2006Robinson, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSZB-5DB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.40.70.
Tend (C) 280.260.243.300.230.
Heat rate (K/min) 10.5.3.2.2.
Initial hold (min) 2.   2.
Final hold (min)     20.
I 1024.1025.1022.1025.1015.
ReferenceRomanenko and Tkachev, 2006Sabulal, Dan, et al., 2006Sabulal, Dan, et al., 2006, 2Sari M., Biondi D.M., et al., 2006Sawamura, Onishi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-2FSOT-RSL-200DB-5DB-5DB-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHydrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.320.250.250.250.25
Tstart (C) 50.40.50.50.40.
Tend (C) 270.280.240.240.240.
Heat rate (K/min) 2.6.4.4.4.
Initial hold (min)  5.   
Final hold (min)  5.   
I 1029.1024.1027.1028.1025.
ReferenceSchlumpberger B.O., Clery R.A., et al., 2006Schmidt, Jirovetz, et al., 2006Sefidkon, Abbasi, et al., 2006Sefidkon, Abbasi, et al., 2006Sefidkon and Jamzad, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5DB-1SPB-5
Column length (m) 60.25.30.60. 
Carrier gas HeN2H2HeliumHe
Substrate      
Column diameter (mm) 0.250.20.200.25 
Phase thickness (μm)  0.330.180.25 
Tstart (C) 40.30.60.60.50.
Tend (C) 250.280.240.250.250.
Heat rate (K/min) 4.3.3.5.5.
Initial hold (min)     3.
Final hold (min)    10.15.
I 1014.1029.1025.1013.1026.
ReferenceSefidkon, Jamzad, et al., 2006Shafi, Jose, et al., 2006Silva, Oliveira, et al., 2006Sonboli, Mirjalili, et al., 2006Stojanovic, Palic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBMethyl SiliconeSPB-5DB-5
Column length (m) 25.25.25.60.30.
Carrier gas H2 N2HeN2
Substrate      
Column diameter (mm) 0.250.250.30.320.25
Phase thickness (μm)   0.151.0.25
Tstart (C) 50.50.50.40.60.
Tend (C) 230.230.210.230.240.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)   5.5. 
Final hold (min)    2. 
I 1021.1020.1034.1034.1025.
ReferenceTesso, König, et al., 2006Tesso, Kubeczka, et al., 2006Tonzibo, Coffy, et al., 2006Tornambe, Cornu, et al., 2006Trilles, Bombarda, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5SPB-1SPB-1DB-5
Column length (m) 50.30.50.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 90.60.50.50.40.
Tend (C) 240.250.220.250.250.
Heat rate (K/min) 4.10.4.4.4.
Initial hold (min)  2.1.1. 
Final hold (min)  10.10.10. 
I 1005.1030.1011.1007.1072.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2006Wang, Yang, et al., 2006Wong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-30DB-5HP-5MSHP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.25 0.250.250.2
Phase thickness (μm) 0.25 0.250.250.5
Tstart (C) 40.90.60.60.60.
Tend (C) 250.220.210.280.250.
Heat rate (K/min) 4.7.3.3.2.
Initial hold (min)  2.5.  
Final hold (min)     60.
I 1013.1018.1015.1020.1016.
ReferenceYadegarinia, Gachkar, et al., 2006Ahuja, Bakshi, et al., 2005Askari and Sefidkon, 2005Basta, Tzakou, et al., 2005Bendimerad and Bendiab, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSDB-1DB-5Methyl Silicone
Column length (m) 30.30.25.50.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.2490.250.250.30.3
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.50.60.50.
Tend (C) 290.240.250.240.240.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min)   3.  
Final hold (min)      
I 1019.1027.1018.1025.1020.
ReferenceBos, Stojanova, et al., 2005Busman, Zoghbi, et al., 2005Cégiéla-Carlioz, Bessière, et al., 2005Chagonda and Chalchat, 2005Chalchat and Özcan, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1HP-1HP-5
Column length (m) 60.60.60.50.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.320.250.250.20.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 230.250.250.250.30.
Heat rate (K/min) 3.5.5.2.4.
Initial hold (min) 5.  60.3.
Final hold (min)   10. 15.
I 1033.1016.1019.1011.1025.
ReferenceCornu, Kondjoyan, et al., 2005Fakhari, Salehi, et al., 2005Fakhari A.R., Sonboli A., et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Ferretti, Maggi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5MSCP Sil 5 CBRSL-200
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 50.60.50.60.40.
Tend (C) 300.200.250.250.280.
Heat rate (K/min) 5.4.3.5.6.
Initial hold (min) 5.30.3. 2.
Final hold (min) 5. 10.10.10.
I 1029.1023.1027.1019.1016.
ReferenceFiguérédo, Cabassu, et al., 2005Gauvin and Smadja, 2005Ghasemi Y., Faridi P., et al., 2005Jassbi, Mehrdad, et al., 2005Jirovetz, Buchbauer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1DB-5HP-5MS
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 50.60.50.35.38.
Tend (C) 265.240.250.280.220.
Heat rate (K/min) 2.53.4.4.5.
Initial hold (min) 1. 5.2.1.
Final hold (min) 30.   2.
I 1007.1024.1025.1024.1029.
ReferenceKhalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Khayyat and Karimi, 2005Khajeh, Yamini, et al., 2005Kowalski and Wolski, 2005Krist, Stuebiger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 60.30.30.25.25.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.150.15
Tstart (C) 30.60.60.50.50.
Tend (C) 260.230.220.230.230.
Heat rate (K/min) 2.3.4.3.3.
Initial hold (min) 2. 5.  
Final hold (min) 28.    
I 1027.11019.1025.1016.1016.
ReferenceLeffingwell and Alford, 2005Limberger, Sobral, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005Ogunwande, Olawore, et al., 2005Olawore, Ogunwande, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1RTX-5 MSSPB-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.40.95.50.60.
Tend (C) 240.250.240.280.250.
Heat rate (K/min) 5.5.4.8.4.
Initial hold (min)  0.5 2.2.
Final hold (min)  2. 2.20.
I 1017.1027.1023.1029.1025.
ReferenceOyedeji, Yani, et al., 2005Özel, Gögüs, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Pellati, Benvenuti, et al., 2005Pino, Marbot, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSCP Sil 5 CBCP Sil 5 CBDB-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.320.250.250.25 
Tstart (C) 60.40.40.60.60.
Tend (C) 250.220.220.200.240.
Heat rate (K/min) 5.4.4.2.5.
Initial hold (min) 3.1.1.  
Final hold (min)    80. 
I 1014.1025.1025.1029.1026.
ReferencePourmortazavi, Ghadiri, et al., 2005Rohloff and Bones, 2005Rohloff and Bones, 2005Rout, Misra, et al., 2005Saeidnia, Gohari, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.275.280.220.
Heat rate (K/min) 6.4.4.4.3.
Initial hold (min) 3.   4.
Final hold (min)      
I 1032.1025.1026.1022.1022.
ReferenceSafaei-Ghomi, Bamoniri, et al., 2005Sajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Salehi, Sefidkon, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5PE-5DB-5HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 250.240.230.230.280.
Heat rate (K/min) 5.4.5.3.3.
Initial hold (min)   2.  
Final hold (min) 10. 4.20. 
I 1015.1025.1033.1025.1021.
ReferenceSalehi, Sonboli, et al., 2005Sefidkon and Jamzad, 2005Singh, Raina, et al., 2005Skoula and Grayer, 2005Slavkovska, Couladis, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1DB-5CP Sil 8 CBHP-5MS
Column length (m) 60.60.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.60.40.60.50.
Tend (C) 250.25.210.290.240.
Heat rate (K/min) 5.5.2.3.3.
Initial hold (min)   2.5.3.
Final hold (min) 10.10.33.  
I 1016.1013.1027.1030.1018.
ReferenceSonboli A., Fakhari A.R., et al., 2005Sonboli, Salehi, et al., 2005Stevanovic, Garneau, et al., 2005Suárez, Vásquez, et al., 2005Tepe B., Sokmen M., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5 MSHP-5MSDB-5DB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.500.250.250.25
Tstart (C) 60.60.60.60.90.
Tend (C) 285.260.280.280.240.
Heat rate (K/min) 4.33.3.3.4.
Initial hold (min)      
Final hold (min)  20.   
I 1026.1024.994.998.1005.
ReferenceTesevic, Nikicevic, et al., 2005Topçu, Barla, et al., 2005Tzakou, Bazos, et al., 2005Tzakou and Constantinidis, 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSSPB-1HP-5CP Sil 5 CB
Column length (m) 50.30.50.30.30.
Carrier gas   HeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.320.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.40.50.60.50.
Tend (C) 240.220.220.260.200.
Heat rate (K/min) 3.3.4.5.5.
Initial hold (min)  5.3.2. 
Final hold (min)  10.30.13. 
I 1010.1020.1012.1029.1014.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2005, 2Vichi, Riu-Aumatell, et al., 2005Wong, Lee, et al., 2005Yayli, Yasar, et al., 2005Agnaniet, Menut, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1SE-52RTX-1DB-1
Column length (m) 30.50.25.60.60.
Carrier gas He N2HeN2
Substrate      
Column diameter (mm) 0.250.220.320.220.25
Phase thickness (μm) 0.250.250.150.250.25
Tstart (C) 90.60.45.60.70.
Tend (C) 220.220.200.230.230.
Heat rate (K/min) 7.2.3.2.2.
Initial hold (min) 2. 5. 2.
Final hold (min) 5.20.30.45.20.
I 1012.1011.1035.1015.1021.
ReferenceAgnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004Cakir, Kordali, et al., 2004Cavalli, Tomi, et al., 2004Choi, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5HP-5 MSHP-5MSDB-1
Column length (m) 30.60.30.30.25.
Carrier gas HeHeHeliumHe 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.251.0.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.200.275.275.180.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min)     10.
Final hold (min)  30.  10.
I 1025.1027.1028.1022.1024.
ReferenceCicció, 2004Gauvin, Ravaomanarivo, et al., 2004Ghannadi, Sajjadi, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004bin Jantan, Ayop, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1SE-54HP-5MSDB-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.50.60.
Tend (C) 280.300.260.230.240.
Heat rate (K/min) 4.4.2.5.3.
Initial hold (min) 4. 5.2. 
Final hold (min)    10. 
I 1022.1016.1025.1019.1026.
ReferenceKalvandi, Sefidkon, et al., 2004Kalemba and Thiem, 2004Kilic, Hafizoglu, et al., 2004Li and Jiang, 2004paz Lima, Silva, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1DB-5HP-5MSDB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.60.
Tend (C) 300.300.210.280.280.
Heat rate (K/min) 3.4.2.3.3.
Initial hold (min)   2.  
Final hold (min)   33. 30.
I 1021.1015.1026.1024.999.
ReferenceLimberger, Sobral, et al., 2004Lis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004Malencic, Couladis, et al., 2004Marongiu, Piras, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5MSNB-30NB-30DB-1
Column length (m) 30.30.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.20.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.70.
Tend (C) 280.275.250.250.220.
Heat rate (K/min) 3.4.2.2.4.
Initial hold (min)      
Final hold (min) 30.    
I 994.1029.1016.1015.1015.
ReferenceMarongiu, Porcedda, et al., 2004Mehrabani, Asadipour, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004Palá-Paúl, García-Jiménez, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1DB-1
Column length (m) 50.60.60.60.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 95.35.35.35.35.
Tend (C) 240.230.230.230.230.
Heat rate (K/min) 4.2.2.2.2.
Initial hold (min)  4.4.4.4.
Final hold (min)  25.25.25.25.
I 1009.1006.1006.1008.1010.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30NB-30DB-5Methyl SiliconeHP-5 MS
Column length (m) 50.50.30.60.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.20.200.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.35.60.60.
Tend (C) 250.250.220.200.200.
Heat rate (K/min) 2.2.2.54.4.
Initial hold (min)    1.1.
Final hold (min)   6.20.20.
I 1015.1013.1025.1022.1022.
ReferenceRaal, Arak, et al., 2004Raal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Rojas, Usubillaga, et al., 2004Royas, Usubillaga, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1DB-1DB-5DB-1
Column length (m) 30.60.60.30.60.
Carrier gas He Nitrogen He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.70.70.50.40.
Tend (C) 280.230.230.250.280.
Heat rate (K/min) 4.2.2.3.4.
Initial hold (min)  2.2.5.5.
Final hold (min)  20.   
I 1025.1021.1021.1025.1014.
ReferenceSajjadi and Shahpiri, 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Sefidkon, Jamzad, et al., 2004Sefidkon and Shaabani, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5HP-5DB-5CP Sil 5 CB
Column length (m) 30.25.25.30.20.
Carrier gas HeN2H2HeHe
Substrate      
Column diameter (mm) 0.250.20.320.250.25
Phase thickness (μm) 0.330.50.520.250.25
Tstart (C) 40.30.40.60.100.
Tend (C) 260.280.240.240.270.
Heat rate (K/min) 2.3.4.3.8.
Initial hold (min) 5.   2.
Final hold (min) 20.    
I 1015.1029.1026.1023.1018.
ReferenceSenatore, Napolitano, et al., 2004Shafi, Nambiar, et al., 2004Simic, Sokovic, et al., 2004Tellez, Khan, et al., 2004Thappa, Bakshi, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BPX-5CP Sil 8 CBCP Sil 8 CBDB-5
Column length (m) 60.25.30.30.30.
Carrier gas N2HeHe He
Substrate      
Column diameter (mm) 0.250.220.250.320.249
Phase thickness (μm) 0.251.0.250.250.25
Tstart (C) 80.60.50.50.60.
Tend (C) 210.250.200.200.300.
Heat rate (K/min) 3.3.10.5.3.
Initial hold (min)  5.3.5. 
Final hold (min) 15.10.2.  
I 1017.1037.1023.1028.1022.
ReferenceUeno, Masuda, et al., 2004Vilaseca, Guy, et al., 2004Wang and Guo-Y. -L., 2004Wang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5DB-1HP-5MS
Column length (m) 30.30.30.60.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.60.
Tend (C) 275.220.240.230.280.
Heat rate (K/min) 4.5.4.2.3.
Initial hold (min)  10. 2. 
Final hold (min)    20. 
I 1026.1022.1016.1021.1022.
ReferenceAfsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Cabanillas, Lopez, et al., 2003Choi, 2003Couladis, Özcan, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RTX-5SilDB-1DB-5DB-5
Column length (m) 60.30.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm)  0.250.25  
Tstart (C) 50.70.50.50.50.
Tend (C) 250.200.250.220.200.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)      
Final hold (min)  10.   
I 1013.1027.1013.1017.1017.
ReferenceDabiri and Sefidkon, 2003Dudai, Larkov, et al., 2003Ebrahimzadeh, Yamini, et al., 2003Edris and Farrag, 2003Edris, Shalaby, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-1DB-1HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.60.70.50.60.
Tend (C) 220.220.200.200.280.
Heat rate (K/min) 3.5.10.5.4.
Initial hold (min)  20.   
Final hold (min)  20.   
I 1019.1030.1014.1011.1026.
ReferenceEdris, Shalaby, et al., 2003, 2Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RSL-200RSL-200RSL-200DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeH2H2H2He
Substrate      
Column diameter (mm) 0.250.320.250.320.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.40.50.
Tend (C) 275.280.280.280.220.
Heat rate (K/min) 4.6.6.6.3.
Initial hold (min)  5.2.5.2.
Final hold (min)  5.10.5.10.
I 1021.1017.1016.1019.1022.
ReferenceGhannadi and Zolfaghari, 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Jirovetz, Buchbauer, et al., 2003, 3Juteau, Jerkovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CP Sil 5 CBDB-5DB-5MSDB-5
Column length (m) 12.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.30.250.250.250.25
Tstart (C) 70.35.60.60.60.
Tend (C) 220.280.240.240.280.
Heat rate (K/min) 3.5.3.3.3.
Initial hold (min)  2.5   
Final hold (min)     30.
I 1008.1010.1027.1027.1016.
ReferenceKambouche and El-Abed, 2003Kanjilal, Kotoky, et al., 2003Machado, Zoghbi, et al., 2003Maia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5ZB-1DB-1HP-5
Column length (m) 30.50.30.60.30.
Carrier gas HeHeN2HeHelium
Substrate      
Column diameter (mm) 0.250.20.250.250.32
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.50.45.50.70.
Tend (C) 280.220.230.270.210.
Heat rate (K/min) 3.3.3.4.2.
Initial hold (min)  2.   
Final hold (min) 30.   60.
I 1013.1028.1007.1023.1024.
ReferenceMarongiu, Porcedda, et al., 2003Masotti, Juteau, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mirza, Nik, et al., 2003Mookdasanit, Tamura, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101CP Sil 5 CBDB-1DB-5HP-5
Column length (m) 50.25.50.30.30.
Carrier gas HeH2N2H2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.50.150.250.250.25
Tstart (C) 50.50.95.60.60.
Tend (C) 250.230.240.280.280.
Heat rate (K/min) 2.3.4.4.3.
Initial hold (min)    10. 
Final hold (min)    40. 
I 1010.1019.1019.1026.1010.
ReferenceOrav, Kailas, et al., 2003Oyedeji, Ekundayo, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5NB-30DB-1DB-1DB-5
Column length (m) 30.50.60.60.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.20.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Tstart (C) 75.50.40.40.40.
Tend (C) 220.250.220.220.230.
Heat rate (K/min) 3.2.4.4.2.
Initial hold (min) 4.    
Final hold (min)      
I 1025.1013.1012.1023.1025.
ReferencePriestap, van Baren, et al., 2003Raal, Arak, et al., 2003Rasooli and Mirmostafa, 2003Rasooli and Mirmostafa, 2003Rotman, Ahumada, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5SPB-5DB-1DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeliumHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.251.00.250.25
Tstart (C) 60.60.30.40.40.
Tend (C) 275.280.230.260.260.
Heat rate (K/min) 4.4.3.4.2.
Initial hold (min)    5.5.
Final hold (min)      
I 1026.1024.1031.1013.1025.
ReferenceSadraei, Ghannadi, et al., 2003Sajjadi and Mehregan, 2003Sebastian, Viallon-Fernandez, et al., 2003Sefidkon, Naderi Nik, et al., 2003Senatore and Bruno, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-1Cross-Linked Methylsilicone
Column length (m) 60.30.60.60.25.
Carrier gas HeHe N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 50.60.40.70.70.
Tend (C) 280.240.250.230.250.
Heat rate (K/min) 4.3.5.2.4.
Initial hold (min)   15.2. 
Final hold (min)    20. 
I 1012.1025.1027.1024.1005.
ReferenceShahmir, Ahmadi, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003Tu, Onishi, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5
Column length (m) 25.25.25.25.25.
Carrier gas H2H2HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.530.530.530.530.53
Tstart (C) 40.40.40.40.40.
Tend (C) 280.280.280.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min)      
Final hold (min)      
I 1025.1029.1020.1020.1021.
ReferenceVelickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5DB-1CP Sil 5 CB
Column length (m) 25.30.25.60.25.
Carrier gas HeliumHeN2HeN2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.530.250.250.250.4
Tstart (C) 40.60.50.50.60.
Tend (C) 280.240.250.280.260.
Heat rate (K/min) 4.3.4.4.5.
Initial hold (min)      
Final hold (min)   10. 40.
I 1026.1024.1026.1014.1007.
ReferenceVelickovic, Ristic, et al., 2003Zoghbi, Andrade, et al., 2003Zrira, Elamrani, et al., 2003Ahmadi, Mirza, et al., 2002Azaz. D., Demirci, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-101DB-5HP-1
Column length (m) 60.30.25.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.2490.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.60.50.60.70.
Tend (C) 220.300.200.280.220.
Heat rate (K/min) 4.3.5.3.3.
Initial hold (min)      
Final hold (min)  5. 30.15.
I 1013.1022.1014.1016.1011.
ReferenceBaher, Mirza, et al., 2002Bos, Koulman, et al., 2002Boyom, Keumedjio, et al., 2002Caredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5MSBP-1DB-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.250.250.500.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.60.60.50.50.
Tend (C) 200.280.220.250.250.
Heat rate (K/min) 3.3.5.4.4.
Initial hold (min) 4.   5.
Final hold (min) 8. 10.  
I 1025.1028.1013.1026.1026.
ReferenceCicció and Gómez-Laurito, 2002Congiu, Falconieri, et al., 2002Das, Ram, et al., 2002Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1PTE-5BP-1SE-30
Column length (m) 30.30.60.25.50.
Carrier gas HeH2H2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.20.25
Phase thickness (μm) 0.250.250.300.10.25
Tstart (C) 60.40.60.40.70.
Tend (C) 240.245.285.250.240.
Heat rate (K/min) 3.3.4.38.4.
Initial hold (min)  20. 5. 
Final hold (min)      
I 1028.1004.1026.1017.1025.
ReferenceFlamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002Gudzic, Djokovic, et al., 2002Hayes R.A., Richardson B.J., et al., 2002Iñigo, Palá-Paúl, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RSL-200RSL-200CP Sil 8 CBDB-1
Column length (m) 30.30.30.30.25.
Carrier gas  H2H2HeHe
Substrate      
Column diameter (mm) 0.250.320.320.250.23
Phase thickness (μm)  0.250.250.250.20
Tstart (C) 50.40.50.50.50.
Tend (C) 200.280.280.220.200.
Heat rate (K/min) 3.6.6.3.3.
Initial hold (min)  5.5.2.3.
Final hold (min)  5.5. 30.
I 1023.1021.1019.1022.1026.
ReferenceIsidorov and Jdanova, 2002Jirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002Juteau, Masotti, et al., 2002Khallouki, Younos, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5OV-101DB-5
Column length (m) 60.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.60.35.50.60.
Tend (C) 240.240.280.200.250.
Heat rate (K/min) 5.3.3.5.3.
Initial hold (min) 3. 2.  
Final hold (min) 10. 15.  
I 1032.1027.1025.1020.1019.
ReferenceKim and Lee, 2002Kobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Kuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSCP Sil 5 CBDB-5DB-1
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.390.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.240.220.220.250.
Heat rate (K/min) 3.3.5.4.4.
Initial hold (min)    5.10.
Final hold (min)      
I 1026.1024.1010.1025.1024.
ReferenceMaia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002Mojab, Rustaiyan, et al., 2002Morteza-Semnani, Saeedi, et al., 2002Norouzi-Arasi, Yavari, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5OV-101ZEBRON-5DB-1
Column length (m) 30.30.50.6.50.
Carrier gas   HeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 60.60.50.40.80.
Tend (C) 240.240.250.200.225.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)    5. 
Final hold (min)    15. 
I 1028.1028.1010.1010.1006.
ReferenceNovak, Langbehn, et al., 2002Novak, Langbehn, et al., 2002Orav, Kailas, et al., 2002Öztürk, Akay, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSPB-5HP-1DB-5DB-1
Column length (m) 30.30.50.30.60.
Carrier gas HeHeliumN2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 40.60.90.60.40.
Tend (C) 280.250.220.300.250.
Heat rate (K/min) 4.4.3.2.4.
Initial hold (min)  2.   
Final hold (min) 5.20.   
I 1026.1020.1021.1020.1011.
ReferencePhutdhawong, Korth, et al., 2002Pino, Marbot, et al., 2002Priestap, van Baren, et al., 2002Ruberto, Biondi, et al., 2002Sefidkon, Dabiri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1HP-5
Column length (m) 60.60.50.50.30.
Carrier gas HeHeN2N2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.95.60.40.
Tend (C) 280.280.240.240.280.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min) 5.5.   
Final hold (min)      
I 1014.1014.1005.1010.1026.
ReferenceSefidkon, Jalili, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2Velickovic, Randjelovic, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5MSDB-5SPB-5DB-1
Column length (m) 60.30.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.60.60.40.40.
Tend (C) 250.270.240.220.280.
Heat rate (K/min) 4.3.3.3.4.
Initial hold (min) 5.  5.5.
Final hold (min)    15. 
I 1014.1024.1023.1022.1012.
ReferenceYamini, Sefidkon, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Cornu, Carnat, et al., 2001Dabiri and Sefidkon, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-1HP-5BP-1RTX-1
Column length (m) 60.30.30.30.30.
Carrier gas HeH2N2N2N2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.30.250.250.25
Tstart (C) 40.50.60.60.60.
Tend (C) 280.250.220.220.300.
Heat rate (K/min) 4.3.5.5.4.
Initial hold (min) 5.1.10.  
Final hold (min)  20.   
I 1012.1010.1028.1014.1014.
ReferenceDabiri and Sefidkon, 2001Gallori, Bilia, et al., 2001Gallori, Flamini, et al., 2001Gupta, Mallavarapu, et al., 2001Kalemba, Marschall, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5BP-1CBP-1DB-5MSDB-1
Column length (m) 60.50.25.30.60.
Carrier gas HeliumHeNitrogenHeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.50.60.50.
Tend (C) 240.230.210.240.270.
Heat rate (K/min) 3.2.3.3.4.
Initial hold (min) 3. 2.  
Final hold (min) 10.35. 30. 
I 1032.1012.1009.1030.1012.
ReferenceKim and Lee, 2001Lota, de Rocca Serra, et al., 2001Ly, Yamauchi, et al., 2001Marongiu, Porcedda, et al., 2001Mirza, Ahmadi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200OV-101OV-101DB-1DB-5
Column length (m) 30.50.50.30.30.
Carrier gas H2HeHeN2 
Substrate      
Column diameter (mm) 0.320.20.20.250.32
Phase thickness (μm) 0.250.5 0.250.5
Tstart (C) 40.50.50.80.35.
Tend (C) 280.250.250.225.275.
Heat rate (K/min) 6.2.2.4.6.
Initial hold (min) 5.    
Final hold (min) 5.    
I 1012.1010.1011.1005.1026.
ReferenceNgassoum, Jirovetz, et al., 2001Orav, Kailas, et al., 2001Orav and Kann, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Rouseff, Jella, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSPTE-5DB-5OV-101
Column length (m) 30.30.60.30.50.
Carrier gas H2HeliumH2HeN2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.250.250.30.25 
Tstart (C) 60.50.60.60.80.
Tend (C) 285.250.285.240.200.
Heat rate (K/min) 3.5.4.33.2.
Initial hold (min)  2.   
Final hold (min)  5.   
I 1022.1019.1025.1026.1017.
ReferenceSantos-Gomes and Fernandes-Ferreira, 2001Shang, Hu, et al., 2001Stojanovic, Palic, et al., 2001Tellez M., Estell R., et al., 2001Yang, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101CP Sil 5 CBCP Sil 5 CBRSL-200HP-5
Column length (m) 50.25.25.60.30.
Carrier gas N2 HeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm)  0.150.40.25 
Tstart (C) 80.50.60.40.80.
Tend (C) 200.230.260.250.200.
Heat rate (K/min) 2.3.5.6.9.
Initial hold (min)   40.  
Final hold (min)     10.
I 1017.1018.1007.1019.1027.
ReferenceYang, 2001, 2Asekun and Ekundayo, 2000Baser, Özek, et al., 2000Jirovetz, Puschmann, et al., 2000Lis-Balchin and Roth, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5BP-1HP-5
Column length (m) 30.25.30.25.30.
Carrier gas HeNitrogenN2N2He
Substrate      
Column diameter (mm) 0.250.500.220.330.25
Phase thickness (μm) 0.250.250.251.00.25
Tstart (C) 60.60.70.60.60.
Tend (C) 240.220.230.275.275.
Heat rate (K/min) 3.5.4.4.4.
Initial hold (min)   2.  
Final hold (min)   20.  
I 1025.1013.1036.1027.1027.
ReferenceMaia, Zoghbi, et al., 2000Mallavarapu, Rao, et al., 2000Mitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5SE-30SPB-1
Column length (m) 30.50.30.25.50.
Carrier gas HeNitrogenHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.20.2
Phase thickness (μm) 0.25 0.25 0.33
Tstart (C) 40.40.60.60.60.
Tend (C) 260.200.240.230.260.
Heat rate (K/min) 2.2.3.3.4.
Initial hold (min) 5.10.   
Final hold (min) 2.    
I 1008.1018.1027.1014.1012.
ReferenceSenatore, Napolitano, et al., 2000Tamura, Boonbumrung, et al., 2000Tellez, Dayan, et al., 2000Ali N.A.M. and Jantan, 1999Choo, Wong, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SE-30RTX-1DB-1CBP-1
Column length (m) 52.30.30.25.25.
Carrier gas HeliumN2N2HeHe
Substrate      
Column diameter (mm) 0.260.250.250.250.3
Phase thickness (μm) 0.130.250.250.25 
Tstart (C) 50.60.60.50.60.
Tend (C) 220.220.300.290.240.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min) 0.10.   
Final hold (min) 0.    
I 1012.1015.1016.1022.1016.
ReferenceDzumayev, Tkachenko, et al., 1999Jassbi, Ahmad, et al., 1999Kalemba, 1999Koulman, 1999Labuckas, Zygadlo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1BP-1DB-5DB-5SE-30
Column length (m) 25.25.30.30.25.
Carrier gas H2N2 HeHe
Substrate      
Column diameter (mm) 0.320.500.320.250.2
Phase thickness (μm) 0.170.251.  
Tstart (C) 40.60.40.40.60.
Tend (C) 260.220.200.230.230.
Heat rate (K/min) 3.5.3.4.3.
Initial hold (min) 5. 5.1.10.
Final hold (min)  10.   
I 1005.1012.1024.1025.1014.
ReferenceLopes, Koketsu, et al., 1999Mallavarapu, Kulkarni, et al., 1999Meynier, Novelli, et al., 1999Mockute and Bernotiene, 1999Mohd and Jantan, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-1OV-1OV-101CP Sil 5 CB
Column length (m) 30.25. 50.25.
Carrier gas HeH2 HeliumHe
Substrate      
Column diameter (mm) 0.250.25 0.200.25
Phase thickness (μm) 0.250.25 0.50 
Tstart (C) 50.40.50.30.50.
Tend (C) 200.220.160.100.230.
Heat rate (K/min) 4.3.2.1.3.
Initial hold (min)  5. 6. 
Final hold (min)  5.   
I 1009.1008.1013.1005.1010.
ReferenceNori-Shargh, Norouzi-Arasi, et al., 1999Oberhofer, Nikiforov, et al., 1999Orav, Kailas, et al., 1999Orav, Kailas, et al., 1999, 2Oyedeji, Olawore, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5SE-30BP-1
Column length (m) 50.50.30.30.25.
Carrier gas HeHeHeHeliumN2
Substrate      
Column diameter (mm) 0.250.250.250.250.5
Phase thickness (μm) 0.250.250.250.20 
Tstart (C) 70.70.40.60.60.
Tend (C) 240.220.250.200.220.
Heat rate (K/min) 4.2.2.3.5.
Initial hold (min)  5.5.4. 
Final hold (min)   60. 10.
I 1005.1015.1014.1017.1013.
ReferencePalá-Paúl, Pérez-Alonso, et al., 1999Pateira, Nogueira, et al., 1999Porta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999Rao, Bhattacharya, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-1DB-1DB-5
Column length (m) 25.25.60.60.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.390.390.25 0.25
Tstart (C) 60.60.40.60.60.
Tend (C) 220.220.280.230.240.
Heat rate (K/min) 5.5.4.3.3.
Initial hold (min) 5. 5.  
Final hold (min) 20.  5. 
I 1016.1018.1013.1016.1027.
ReferenceRustaiyan, Masoudi, et al., 1999Rustaiyan and Nadji, 1999Sefidkon, Dabiri, et al., 1999Shafiee, Javidnia, et al., 1999Tellez, Canel, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5CP Sil 5 CBOV-101DB-5MSSPB-5
Column length (m) 60.25.25.30.50.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.32 0.200.250.32
Phase thickness (μm) 1.0.39 0.250.25
Tstart (C) 40.60.80.60.60.
Tend (C) 200.220.240.240.240.
Heat rate (K/min) 3.5.6.3.3.
Initial hold (min) 5.    
Final hold (min) 2.   20.
I 1032.1016.1018.1023.1026.
ReferenceViallon C., Verdier-Metz I., et al., 1999Weyerstahl, Marschall, et al., 1999Zenkevich, Kosman, et al., 1999Zoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30DB-5HP-5HP-1OV-101
Column length (m) 25.30.25.60.25.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.20.250.20.250.32
Phase thickness (μm)  0.250.330.25 
Tstart (C) 60.60.70.50.50.
Tend (C) 180.240.290.280.200.
Heat rate (K/min) 3.3.3.4.5.
Initial hold (min) 10. 8.5. 
Final hold (min)   20.  
I 1015.1024.1032.1009.1018.
ReferenceJantan, Ahmad, et al., 1998Maia, Zohhbi, et al., 1998Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBBPX-5OV-1
Column length (m) 25.25.25.50.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.220.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.50.40.
Tend (C) 290.290.300.250.270.
Heat rate (K/min) 4.4.6.3.2.
Initial hold (min)    1.4.
Final hold (min)    10. 
I 1008.1008.1008.1034.1010.
ReferenceBos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2D'Arcy, Rintoul, et al., 1997Kökdil, Kurucu, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1SPB-SulfurSPB-SulfurDB-1DB-5
Column length (m) 30.30.30. 30.
Carrier gas  HeHe Helium
Substrate      
Column diameter (mm) 0.320.320.32 0.25
Phase thickness (μm) 0.254.4. 0.25
Tstart (C) 40.45.45.80.60.
Tend (C) 270.240.240.220.240.
Heat rate (K/min) 2.5.5.6.3.
Initial hold (min) 4.13.13.  
Final hold (min)  5.5.  
I 1010.1026.1027.1003.1025.
ReferenceKökdil, Tanker, et al., 1997Mariaca, Berger, et al., 1997Mariaca, Berger, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CBP-1HP-1DB-5OV-101
Column length (m) 30.25.23.30.50.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm)   0.170.25 
Tstart (C) 60.60.60.60.50.
Tend (C) 240.240.250.300.250.
Heat rate (K/min) 4.5.5.4.2.
Initial hold (min)   3.2. 
Final hold (min)   30.5. 
I 1026.1017.1010.1021.71011.
ReferenceZunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Ayedoun, Adeoti, et al., 1996Gawdzik, Mardarowicz, et al., 1996Orav, Kailas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1DB-1DB-5DB-1
Column length (m) 25.25.60.30.60.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.500.500.320.250.25
Phase thickness (μm)   0.50 0.25
Tstart (C) 60.60.50.40.50.
Tend (C) 220.220.250.210.250.
Heat rate (K/min) 5.5.8.2.2.5
Initial hold (min)   1.2.5.
Final hold (min)   6.33. 
I 1018.1019.1018.1026.1019.
ReferenceRajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Sagrero-Nieves and Bartley, 1996Sohounhloue, Dangou, et al., 1996Stashenko, Puertas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1SPB-1OV-101HP-5OV-101
Column length (m) 25.50.52. 50.
Carrier gas HeliumHeHe He
Substrate      
Column diameter (mm) 0.320.20.26 0.2
Phase thickness (μm) 0.250.33  0.5
Tstart (C) 60.40.50.35.70.
Tend (C) 220.200.220.200.180.
Heat rate (K/min) 4.3.3.6.1.
Initial hold (min) 2.3. 2. 
Final hold (min) 20.30.   
I 1010.1010.1010.1024.1016.
ReferenceThanh, Dung, et al., 1996Wong and Lai, 1996Dzumayev, Tsibulskaya, et al., 1995Larsen and Frisvad, 1995Orav, Kuningas, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5OV-1HP-5
Column length (m) 60.60.30.50. 
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.27 
Phase thickness (μm) 0.250.250.250.2 
Tstart (C) 70.70.35.80.40.
Tend (C) 270.270.300.240.210.
Heat rate (K/min) 2.52.510.3.2.
Initial hold (min) 5.5.2.  
Final hold (min)   10.  
I 1013.1013.1030.31015.1025.
ReferenceTirado, Stashenko, et al., 1995Tirado, Stashenko, et al., 1995Wang and Fingas, 1995Ramanoelina, Viano, et al., 1994Collin, Deslauriers, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101Methyl SiliconeMethyl SiliconeCP Sil 5 CBMethyl Silicone
Column length (m) 50.50.50.25.25.
Carrier gas H2N2N2  
Substrate      
Column diameter (mm) 0.320.250.250.250.50
Phase thickness (μm) 0.30.170.17  
Tstart (C) 65.80.80.60.60.
Tend (C) 300.200.200.280.220.
Heat rate (K/min) 2.2.3.5.5.
Initial hold (min) 5.    
Final hold (min)      
I 1011.1020.1018.1016.1019.
ReferenceDemarne and van der Walt, 1993Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Mallavarapu, Ramesh, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1DB-1CP Sil 5 CB
Column length (m) 60.30.30.60.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.251.20.45
Tstart (C) 40.50.50.30.0.
Tend (C) 200.240.240.240.320.
Heat rate (K/min) 3.5.5.3.3.
Initial hold (min) 2.3.3.10.5.
Final hold (min)     10.
I 1038.1012.1014.1018.1008.
ReferenceShimoda, Shibamoto, et al., 1993Shiota, 1993Shiota, 1993Ciccioli, Cecinato, et al., 1992Hartgers, Damste, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5DB-1OV-101DB-1
Column length (m) 30.60.30.54.60.
Carrier gas Hydrogen N2Helium 
Substrate      
Column diameter (mm) 0.250.25 0.260.32
Phase thickness (μm) 0.250.25   
Tstart (C) 60.40.80.50.50.
Tend (C) 250.250.220.240.230.
Heat rate (K/min) 2.2.4.5.4.
Initial hold (min) 5.5. 0. 
Final hold (min) 2.  0.10.
I 1024.1026.1010.1010.1010.
ReferenceKollmannsberger, Nitz, et al., 1992Lee, Macku, et al., 1991Velasco-Negueruela, Pérez Alonso, et al., 1991Zenkevich and Ventura, 1991Binder, Benson, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBRSL-150BP-1OV-101OV-101
Column length (m) 25.30.25.50.50.
Carrier gas    N2N2
Substrate      
Column diameter (mm) 0.200.320.330.250.25
Phase thickness (μm)  0.20   
Tstart (C) 60.30.45.80.80.
Tend (C) 230.200.180.200.200.
Heat rate (K/min) 3.3.3.2.2.
Initial hold (min) 10. 3.  
Final hold (min)      
I 1036.1010.1009.1018.1018.
ReferenceJantan and Goh, 1990Ronse and De Pooter, 1990Wyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1SE-30OV-101OV-101DB-5
Column length (m) 50.40.50.50.30.
Carrier gas H2HeN2N2Hydrogen
Substrate      
Column diameter (mm) 0.300.500.250.250.35
Phase thickness (μm)  0.75  1.0
Tstart (C) 40.30.80.80.45.
Tend (C) 250.220.200.200.220.
Heat rate (K/min) 10.3.2.2.2.
Initial hold (min) 1.    
Final hold (min)      
I 1013.1010.1018.1019.1024.
ReferenceBrophy, Davies, et al., 1989de Pooter, de Buyck, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Georgilopoulos and Gallois, 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101OV-1OV-101
Column length (m) 25.50.50.60.50.
Carrier gas HydrogenHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.200.250.250.500.30
Phase thickness (μm)    1.2 
Tstart (C) 70.40.40.40.40.
Tend (C) 180.200.200.220.230.
Heat rate (K/min) 3.2.5.2.3.5
Initial hold (min) 5.0.0. 5.
Final hold (min)  0.0.  
I 1020.1002.1005.1009.1010.
ReferenceMacLeod, MacLeod, et al., 1988Tkachenko and Zenkevich, 1987Tkachenko and Zenkevich, 1987Wahab, Aboutabl, et al., 1987Nykanen, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-1OV-1OV-101
Column length (m) 50.50.40. 30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.300.300.5 0.5
Phase thickness (μm)   0.75 0.8
Tstart (C) 40.40.30.40.40.
Tend (C) 230.230.220.220.220.
Heat rate (K/min) 3.53.53.2.2.
Initial hold (min) 5.5.   
Final hold (min)      
I 1016.1027.1010.1011.1010.
ReferenceNykanen, 1986Nykanen, 1986de Pooter, de Buyck, et al., 1986De Pooter, De Buyck, et al., 1986De Pooter and Schamp, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1SE-30SE-30+IgepalSE-30+Igepal
Column length (m) 50.60.50.100.100.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.310.320.50.250.25
Phase thickness (μm)      
Tstart (C) 0.50.40.70.70.
Tend (C) 225.250.170.170.170.
Heat rate (K/min) 3.4.3.1.1.
Initial hold (min) 1.0.13.  
Final hold (min)  5.   
I 1005.1011.1011.1010.1018.
Referencedel Rosario, de Lumen, et al., 1984Flath, Mon, et al., 1983Heydanek and McGorrin, 1981Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SF-96
Column length (m) 111.
Carrier gas Nitrogen
Substrate  
Column diameter (mm) 0.76
Phase thickness (μm)  
Tstart (C)  
Tend (C) 130.
Heat rate (K/min) 3.
Initial hold (min) 8.
Final hold (min) 40.
I 1014.
ReferenceDonetzhuber, Johansson, et al., 1976
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Lazarevic, Radulovic, et al., 2010
Lazarevic, J.; Radulovic, N.; Palic, R.; Zlatkovic, B., Chemical Analusis of volatile constituents of Berula erecta (Hudson) Coville subsp. erecta (Apiaceae) from Serbia, J. Essential Oil. Res., 2010, 22, 3, 153-156, https://doi.org/10.1080/10412905.2010.9700290 . [all data]

Mesa-Arango, Betancur-Galvis, et al., 2010
Mesa-Arango, A.C.; Betancur-Galvis, L.; Montiel, J.; Bueno, J.G.; Baena, A.; Duran, D.C.; Martinez, J.R.; Stashenko, E.E., Antifungal activity and chemical composition of the essential oils of Lippia alba (Miller) N.E. Brown grown in different regions of Colombia, J. Essential Oil Res., 2010, 22, 6, 568-574, https://doi.org/10.1080/10412905.2010.9700402 . [all data]

Mishra, Chaudhary, et al., 2010
Mishra, R.K.; Chaudhary, S.; Pandey, R.; Gupta, S.; Mallavarapu, G.R.; Kumar, S., Analysis of linalool content in the inflorescence (flower) essential oil and leaf oil of Lippia alba cultivar Kavach, J. Essen. Oil Res., 2010, 22, 1, 3-7, https://doi.org/10.1080/10412905.2010.9700253 . [all data]

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Monsef-Esfahani, Miri, et al., 2010
Monsef-Esfahani, H.R.; Miri, A.; Amini, M.; Amanzadeh, Y.; Hadjiakhoondi, A.; Hajiaghaee, R.; Ajani, Y., Seasonal variations in the chemical composition, antioxidant activity and total phenolic content of Teucrium persicum Boiss. essential oils, Res. J. Biol. Sci., 2010, 5, 7, 492-498, https://doi.org/10.3923/rjbsci.2010.492.498 . [all data]

Neves, Rosa, et al., 2010
Neves, A.; Rosa, S.; Goncalves, J.; Rufino, A.; Judas, F.; Salgueiro, L.; Lopes, M.C.; Cavaleiro, C.; Mendes, A.F., Screening of five essential oils for identification of potential inhibitors of IL-1-unduced Nf-kB activation and NO production in human clondrocytes: characterization of the inhibitory activity of alpha-pinene, Plante Med., 2010, 76, 03, 303-308, https://doi.org/10.1055/s-0029-1186085 . [all data]

Ogunwande, Flamini, et al., 2010
Ogunwande, I.A.; Flamini, G.; Cioni, P.L.; Omikorede, O.; Azeez, R.A.; Ayodele, A.A.; Kamil, Y.O., Aromatic plants growing in Nigeria: essential oil constituents of Cassia alata (Linn.) Roxb. and Helianthus annuus L., Rec. Nat. Prod., 2010, 4, 4, 211-217. [all data]

Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Radulovic, Dordevic, et al., 2010
Radulovic, N.S.; Dordevic, N.D.; Palic, R.M., Volatiles of Pleurospermum austriacum (L.) Hoffm. (Apiaceae), J. Serbian Chem. Soc., 2010, 75, 12, 1-11, https://doi.org/10.2298/JSC100323127R . [all data]

Radulovic, Dordevic, et al., 2010, 2
Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Safaei-Ghomi, Meshkatalsadat, et al., 2010
Safaei-Ghomi, J.; Meshkatalsadat, M.H.; Asadi, M., Analysis of the essential oil of Salvia brachycalyx Boiss. by nano scale injection and antioxidative activity of methanol extract of this plant, Digest J. Nanomaterials and Biostructures, 2010, 5, 2, 545-549. [all data]

Scandinaro, Tranchida, et al., 2010
Scandinaro, M.; Tranchida, P.Q.; Costa, R.; Dugo, P.; Mondello, L., Rapid Quality Control of Flavours and Fragrances using Fast GC-MS and Multi-MS Library Search Procedures, LCGC Europe, 2010, 23, 9, 456-464. [all data]

Takeoka, Hobbs, et al., 2010
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Cicció, J.F., A source of almost pure methyl chavicol: volatile oil from the aerial parts of Tagetes lucida (Asteraceae) cultivated in Costa Rica, Rev. Biol. Trop., 2004, 52, 4, 853-857, retrieved from http://www.tropiweb.com. [all data]

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Afsharypuor, S.; Jahromy, M.M., Constituents of the essential oil from Tanacetum lingulatum (Boiss.) Bornm., J. Essent. Oil Res., 2003, 15, 2, 74-76, https://doi.org/10.1080/10412905.2003.9712069 . [all data]

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Choi, H.-S., Characterization of citrus unshiu (C. unshiu Marcov. forma Miyagawa-wase) blossom aroma by solid-phase microextraction in conjunction with an electronic nose, J. Agric. Food Chem., 2003, 51, 2, 418-423, https://doi.org/10.1021/jf0114280 . [all data]

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Edris, A.E.; Farrag, E.S., Antifungal activity of peppermint and sweet basil essential oils and their major aroma constituents on some plant pathogenic fungi from the vapor phase, Nahrung/Food, 2003, 47, 2, 117-121, https://doi.org/10.1002/food.200390021 . [all data]

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Ghannadi, A.; Zolfaghari, B., Compositional analysis of the essential oil of Lallemantia royleana (Benth. in Wall.) Benth. from Iran, Flavour Fragr. J., 2003, 18, 3, 237-239, https://doi.org/10.1002/ffj.1215 . [all data]

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Kim and Lee, 2002
Kim, N.-S.; Lee, D.-S., Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry, J. Chromatogr. A, 2002, 982, 1, 31-47, https://doi.org/10.1016/S0021-9673(02)01445-0 . [all data]

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Notes

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