p-Cymene

Formula: C₁₀H₁₄
Molecular weight: 134.2182
IUPAC Standard InChI: InChI=1S/C10H14/c1-8(2)10-6-4-9(3)5-7-10/h4-8H,1-3H3
IUPAC Standard InChIKey: HFPZCAJZSCWRBC-UHFFFAOYSA-N
CAS Registry Number: 99-87-6
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Isotopologues:
- d14 Cymene
Other names: Benzene, 1-methyl-4-(1-methylethyl)-; p-Cimene; p-Cymol; p-Isopropyltoluene; p-Methylisopropylbenzene; Camphogen; Dolcymene; 1-Isopropyl-4-methylbenzene; 1-Methyl-4-isopropylbenzene; 2-p-Tolylpropane; 4-Isopropyl-1-methylbenzene; 1-Methyl-4-(1-methylethyl)-benzene; Benzene, 1-isopropyl-4-methyl-; Cumene, p-methyl-; p-Isopropylmethylbenzene; Paracymene; Paracymol; p-Methylcumene; 4-Isopropyltoluene; 4-Methylisopropylbenzene; 1-(1-methylethyl)-4-methylbenzene; benzene, 1-methyl-4-methylethyl-; p-Mentha-1,3,5-triene; NSC 4162; Cymene; Cymol
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- Gas Phase Kinetics Database
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Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	DB-5	Equity-5MS	HP-5MS	HP-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	40.
T_end (C)	230.	240.	250.	250.	250.
Heat rate (K/min)	2.	3.	3.	2.	5.
Initial hold (min)				8.	1.
Final hold (min)	30.		10.	30.	10.
I	1011.	1030.	1033.	1025.	1024.
Reference	Bendahou, Muselli, et al., 2008	Baccouri, Ben Temime, et al., 2007	Belsito E.L., Carbone C., et al., 2007	Benkaci-Ali, Baaliouamer, et al., 2007	Benzo, Gilardoni, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	CP-Sil PONA GB	HP-5	BP-1	SPB-5
Column length (m)	50.	100.	25.	50.	60.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	1.
T_start (C)	60.	140.	60.	60.	40.
T_end (C)	220.	230.	240.	220.	230.
Heat rate (K/min)	2.	5.	4.	2.	3.
Initial hold (min)		10.	2.		2.
Final hold (min)	20.	25.		20.	10.
I	1011.	1018.	1030.	1012.	1031.
Reference	Castilho, Liu, et al., 2007	Cunicao, Lopes, et al., 2007	Dehghan, Solaimanian, et al., 2007	Duquesnoy, Castola, et al., 2007	Engel and Ratel, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	240.	220.	220.	246.	280.
Heat rate (K/min)	3.	5.	5.	3.	3.
Initial hold (min)		10.	10.
Final hold (min)
I	1028.	1028.	1028.	1024.	1016.
Reference	Flamini, Cioni, et al., 2007	Flamini, Tebano, et al., 2007	Flamini, Tebano, et al., 2007, 2	Hongratanaworakit and Buchbauer, 2007	Kundakovic, Fokialakis, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	DB-5	DB-5	DB-5
Column length (m)	50.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.32	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.5	0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	220.	240.	240.	265.	240.
Heat rate (K/min)	2.	3.	3.	7.	3.
Initial hold (min)					2.
Final hold (min)	20.			5.
I	1012.	1028.	1028.	1024.	1026.
Reference	Lesueur, de Rocca Serra, et al., 2007	Maccioni, Baldini, et al., 2007	Maccioni, Baldini, et al., 2007	Mahattanatawee K., Perez-Cacho P.R., et al., 2007	Martins, Santos, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	RTX-1	RTX-1	HP-101	HP-5
Column length (m)	60.	60.	60.	25.	30.
Carrier gas	He	He	He	Helium	He
Substrate
Column diameter (mm)	0.22	0.22	0.22	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	60.	60.	60.	70.	50.
T_end (C)	230.	230.	230.	200.	250.
Heat rate (K/min)	2.	2.	2.	3.	4.
Initial hold (min)				2.	4.
Final hold (min)	30.	35.	35.	15.	10.
I	1012.	1012.	1012.	1029.	1024.
Reference	Muselli, Rossi, et al., 2007	Paolini J., Costa J., et al., 2007	Paolini, Muselli, et al., 2007	Politeo, Jukic, et al., 2007	Quijano, Salamanca, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	DB-5	HP-5MS	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	55.
T_end (C)	265.	260.	280.	280.	240.
Heat rate (K/min)	7.	5.	4.	4.	3.
Initial hold (min)			5.	5.	2.
Final hold (min)	5.				15.
I	1026.	1026.	1018.	1024.	1023.
Reference	Ruiz Perez-Cacho, Mahattanatawee, et al., 2007	Sabulal, Dan, et al., 2007	Saroglou, Arfan, et al., 2007	Saroglou, Marin, et al., 2007	Silva, Barbosa, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	CP Sil 5 CB	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	60.	60.
T_end (C)	280.	280.	200.	240.	240.
Heat rate (K/min)	3.	3.	5.	3.	3.
Initial hold (min)				2.	2.
Final hold (min)
I	1026.	1026.	1019.	1022.	1021.
Reference	Vagionas, Ngassapa, et al., 2007	Vagionas, Ngassapa, et al., 2007	Andrianoelisoa H.S., Menut C., et al., 2006	Batista-Pereira, Fernandes, et al., 2006	Batista-Pereira, Fernandes, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	SPB-1	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	240.	220.	250.	250.	240.
Heat rate (K/min)	3.	2.	5.	5.	3.
Initial hold (min)	2.		3.	3.
Final hold (min)		20.	15.	15.
I	1022.	1012.	1047.	1027.	1030.
Reference	Batista-Pereira, Fernandes, et al., 2006	Blanc, Bradesi, et al., 2006	Blagojevic, Radulovic, et al., 2006	Blagojevic, Radulovic, et al., 2006	Block, Flamini, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	RTX-1	HP-5MS	Mega 5MS
Column length (m)	50.	50.	60.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	220.	220.	230.	280.	240.
Heat rate (K/min)	2.	2.	2.	3.	3.
Initial hold (min)
Final hold (min)	20.	20.	45.
I	1008.	1013.	1014.	1024.	1015.
Reference	Boti, Bighelli, et al., 2006	Bousmaha, Boti, et al., 2006	Cavalli, Tomi, et al., 2006	Chorianopoulos N., Evergets E., et al., 2006	Condurso, Verzera, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5	BP-1
Column length (m)	30.	30.	50.	30.	50.
Carrier gas	N2	N2	N2	N2	He
Substrate
Column diameter (mm)	0.32	0.25	0.2	0.25	0.22
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	240.	240.	220.	220.	220.
Heat rate (K/min)	3.	3.	5.	5.	2.
Initial hold (min)	3.	3.	3.	10.
Final hold (min)	5.	3.	5.		20.
I	1026.	1024.	1026.	1028.	1013.
Reference	Dob, Dahmane, et al., 2006	Dob, Dahmane, et al., 2006, 2	Esmaeili, Nematollahi, et al., 2006	Flamini, Tebano, et al., 2006	Gonny, Cavaleiro, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	HP-5MS	DB-1	HP-5MS
Column length (m)	30.	30.	20.	30.	30.
Carrier gas	He	He		N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	260.	250.	240.	220.	280.
Heat rate (K/min)	3.	3.	5.	4.	3.
Initial hold (min)			4.
Final hold (min)			15.
I	1025.	1026.	1027.	1018.	1024.
Reference	Javidnia, Miri, et al., 2006	Javidnia, Miri, et al., 2006, 2	Kallio, Jussila, et al., 2006	Kuiate, Bessière, et al., 2006	Kukic J., Petrovic S., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-1	DB-1	RTX-1
Column length (m)	30.	50.	25.	25.	60.
Carrier gas	He	N2	He		He
Substrate
Column diameter (mm)	0.25	0.2	0.2	0.2	0.22
Phase thickness (μm)	0.25	0.32	0.33	0.33	0.25
T_start (C)	60.	60.	60.	50.	60.
T_end (C)	250.	220.	300.	300.	230.
Heat rate (K/min)	10.	5.	5.	4.	2.
Initial hold (min)	2.	3.	3.
Final hold (min)	10.	5.	30.		35.
I	1030.	1026.	1010.	1022.	1011.
Reference	Liu J.M., Nan P., et al., 2006	Masoudi, Esmaeili, et al., 2006	Nath, Baruah, et al., 2006	Osorio, Alarcon, et al., 2006	Paolini J., Desjobert J.M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	SPB-1	SPB-1	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.2	0.25	0.25
T_start (C)	60.	60.	70.	50.	50.
T_end (C)	280.	280.	220.	250.	265.
Heat rate (K/min)	3.	3.	3.	5.	2.5
Initial hold (min)				3.
Final hold (min)			15.	15.
I	1003.	1020.	1011.	1040.	1020.
Reference	Pavlovic, Kovacevic, et al., 2006	Pavlovic, Tzakou, et al., 2006	Pinto, Pina-Vaz, et al., 2006	Radulovic, Mananjarasoa, et al., 2006	Ramezani, Behravan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	OV-1	SPB-1	HP-5MS
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.2	0.25
T_start (C)	60.	60.	50.	70.	60.
T_end (C)	240.	240.	220.	220.	280.
Heat rate (K/min)	4.	4.	3.	3.	4.
Initial hold (min)			1.		5.
Final hold (min)			5.	15.
I	1036.	1026.	1030.	1012.	1024.
Reference	Rezazadeh, Hamedani, et al., 2006	Rezazadeh, Hamedani, et al., 2006	Rubiolo P., Matteodo M., et al., 2006	Salgueiro L.R., Pinto E., et al., 2006	Saroglou, Dorizas, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	HP-5MS	HP-5	DB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	H2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	40.	50.
T_end (C)	250.	250.	285.	300.	200.
Heat rate (K/min)	5.	5.	4.3	4.	5.
Initial hold (min)	2.	2.		5.
Final hold (min)
I	1025.	1025.	1018.	1021.	1017.
Reference	Su, Ho, et al., 2006	Su, Ho, et al., 2006, 2	Vujisic L., Vuckovic I., et al., 2006	Vundac, Pfeifhofer, et al., 2006	Agnaniet, Makani, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	DB-5	BP-1	SE-54	HP-5
Column length (m)	30.	30.	50.	50.	30.
Carrier gas	He	He	He	H2	N2
Substrate
Column diameter (mm)	0.25	0.2	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.27	0.25
T_start (C)	50.	50.	60.	50.	60.
T_end (C)	250.	250.	220.	300.	220.
Heat rate (K/min)	5.	5.	2.	5.	5.
Initial hold (min)	3.	3.			10.
Final hold (min)	15.	15.	20.
I	1047.	1015.	1013.	1022.	1027.
Reference	Boskovic, Radulovic, et al., 2005	Boskovic, Radulovic, et al., 2005	Boti J.B., Koukoua G., et al., 2005	Brantner, Pfeifhofer, et al., 2005	Celik, Gokturk, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	RTX-1	DB-1	MDN-5
Column length (m)	60.	30.	60.	30.	30.
Carrier gas	N2	N2			He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	60.	50.	50.
T_end (C)	230.	220.	220.	250.	250.
Heat rate (K/min)	2.	5.	2.	2.	3.
Initial hold (min)	2.	10.		8.
Final hold (min)	20.		20.
I	1027.	1028.	1013.	1014.	1021.
Reference	Choi, 2005	Cioni, Flamini, et al., 2005	Cozzani, Muselli, et al., 2005	Dob, Dahmane, et al., 2005	Dugo, Mondello, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 8CB-MS	5 % Phenyl methyl siloxane	DB-1	DB-1	BP-1
Column length (m)	0.	30.	30.	30.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.22
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	40.	40.	40.	40.	60.
T_end (C)	280.	250.	250.	260.	220.
Heat rate (K/min)	4.	7.	3.	2.	2.
Initial hold (min)	2.	10.		5.
Final hold (min)	5.	5.	20.	20.	20.
I	1030.	1050.	1002.	1017.	1011.
Reference	Elmore, Cooper, et al., 2005	Estevez, Ventanas, et al., 2005	Fanciullino, Gancel, et al., 2005	de Feo, Urrunaga Soria, et al., 2005	Ferrari, Tomi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-1	CP Sil 5 CB	DB-1
Column length (m)	30.	30.	30.	50.	25.
Carrier gas	N2	N2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.13	0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	220.	220.	250.	300.	180.
Heat rate (K/min)	5.	5.	3.	4.	3.
Initial hold (min)	10.	10.			10.
Final hold (min)			20.	10.	10.
I	1028.	1027.	1006.	1011.	1024.
Reference	Flamini, Luigi Cioni, et al., 2005	Flamini, Luigi Cioni, et al., 2005, 2	Gancel, Ollitrault, et al., 2005	Idzojtic, Kajba, et al., 2005	bin Jantan, Yalvema, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	RTX-1	HP-5MS	DB-5
Column length (m)	25.	30.	60.	30.	30.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	75.	60.	60.	60.	40.
T_end (C)	210.	260.	230.	250.	260.
Heat rate (K/min)	3.	3.	2.	4.	2.
Initial hold (min)	10.			2.	5.
Final hold (min)	1.		35.	20.	20.
I	1024.	1025.	1012.	1026.	1026.
Reference	bin Jantan, Yalvema, et al., 2005, 2	Javidnia, Miri, et al., 2005	Paolini, Costa, et al., 2005	Pino, Mesa, et al., 2005	Senatore, Napolitano, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	HP-5MS	DB-1	Mega 5MS	DB-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	40.	45.
T_end (C)	200.	200.	200.	240.	180.
Heat rate (K/min)	2.	2.	5.	3.	2.5
Initial hold (min)				2.	10.
Final hold (min)	20.	10.			20.
I	1029.	1019.	1016.	1016.	1023.
Reference	Seo and Baek, 2005	Smadja, Rondeau, et al., 2005	Tchoumbougnang, Zollo, et al., 2005	Verzera, Trozzi, et al., 2005	Zhang, Xu, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	SE-54	SPB-1	HP-5	SPB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.2
T_start (C)	60.	60.	70.	60.	70.
T_end (C)	280.	260.	220.	220.	220.
Heat rate (K/min)	3.	2.	3.	5.	3.
Initial hold (min)		5.		10.
Final hold (min)			15.		15.
I	1022.	1023.	1012.	1026.	1011.
Reference	Aligiannis, Kalpoutzakis, et al., 2004	Alma, Nitz, et al., 2004	Antunes, Sevinate-Pinto, et al., 2004	Bertoli, Pistelli, et al., 2004	Cavaleiro, Salgueiro, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5MS	RTX-5	HP-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas		He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	45.	60.	60.
T_end (C)	220.	280.	300.	240.	240.
Heat rate (K/min)	5.	3.	3.	3.	3.
Initial hold (min)	10.		6.
Final hold (min)			10.
I	1028.	1024.	1023.	1028.	1027.
Reference	Ceccarini, Macchia, et al., 2004	Chorianopoulos, Kalpoutzakis, et al., 2004	Dugo, Mondello, et al., 2004	Flamini, Bader, et al., 2004	Flamini, Cioni, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	BP-1	HP-5MS	HP-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	N2	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	240.	290.	220.	280.	260.
Heat rate (K/min)	3.	4.	2.	4.	3.
Initial hold (min)				5.
Final hold (min)			20.
I	1027.	1032.	1012.	1024.	1024.
Reference	Flamini, Cioni, et al., 2004	Flach A., Dondon R.C., et al., 2004	Gonny, Bradesi, et al., 2004	Grujic-Jovanovic, Skaltsa, et al., 2004	Javidnia, Miri, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	DB-5MS	SPB-1	SPB-1
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.2	0.2
T_start (C)	60.	60.	40.	70.	70.
T_end (C)	260.	280.	280.	220.	220.
Heat rate (K/min)	3.	4.	4.	3.	3.
Initial hold (min)		5.	2.
Final hold (min)				15.	15.
I	1026.	1024.	1023.	1011.	1011.
Reference	Javidnia, Miri, et al., 2004, 2	Karioti, Hadjipavlou-Litina, et al., 2004	Mardarowicz, Wianowska, et al., 2004	Moldão-Martins, Beirão-da-Costa, et al., 2004	Moldão-Martins, Beirão-da-Costa, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	Methyl Silicone	SPB-5	SPB-5	SPB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	40.	50.	60.	60.	60.
T_end (C)	280.	240.	250.	250.	250.
Heat rate (K/min)	6.	3.	4.	4.	4.
Initial hold (min)	5.		2.	2.	2.
Final hold (min)	5.		20.	20.	20.
I	1026.	1026.	1026.	1026.	1026.
Reference	Ngassoum, Ousmaila, et al., 2004	Özcan and Chalchat, 2004	Píno, Marbot, et al., 2004	Pino, Marbot, et al., 2004	Pino, Marbot, et al., 2004, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	DB-5	HP-5MS	HP-5	HP-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	1.
T_start (C)	60.	60.	50.	60.	-30.
T_end (C)	220.	275.	250.	240.	250.
Heat rate (K/min)	5.	4.	3.	3.	10.
Initial hold (min)					1.
Final hold (min)	13.			7.
I	1009.	1030.	1025.	1024.	1024.
Reference	Raina, Kumar, et al., 2004	Ramezani, Khaje-Karamoddin, et al., 2004	Salido, Valenzuela, et al., 2004	Sartoratto, Machado, et al., 2004	Siegmund, Derler, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	BP-1	Optima 5	HP-5MS	DB-5MS
Column length (m)	50.	50.	25.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.2	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.2	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	40.
T_end (C)	250.	220.	280.	200.	200.
Heat rate (K/min)	3.	2.	3.	6.	4.
Initial hold (min)	15.			1.5	5.
Final hold (min)	40.	20.	20.	5.	20.
I	1028.	1012.	1025.	1029.	1028.
Reference	Stashenko, Jaramillo, et al., 2004	Tam, Thuam, et al., 2004	Vérité, Nacer, et al., 2004	Weissbecker, Holighaus, et al., 2004	Yu, Kim, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5	DB-5	DB-5
Column length (m)	25.	30.	30.	30.	30.
Carrier gas	N2	N2	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	75.	60.	60.	60.	60.
T_end (C)	210.	220.	220.	240.	220.
Heat rate (K/min)	3.	5.	5.	3.	5.
Initial hold (min)	10.	10.	10.		10.
Final hold (min)	1.			30.
I	1024.	1028.	1028.	1028.	1028.
Reference	bin Ahmad and bin Jantan, 2003	Angelini, Carpanese, et al., 2003	Angelini, Carpanese, et al., 2003	Bader, Caponi, et al., 2003	Bader, Caponi, et al., 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	OV-1	DB-1	SPB-1
Column length (m)	30.	50.	25.	30.	30.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.3	0.25	0.2
T_start (C)	60.	60.	50.	40.	70.
T_end (C)	240.	230.	200.	250.	220.
Heat rate (K/min)	3.	2.	3.	3.	3.
Initial hold (min)			1.
Final hold (min)		35.	20.	20.	15.
I	1027.	1013.	1010.	1004.	1011.
Reference	Bader, Flamini, et al., 2003	Bianchini, Tomi, et al., 2003	Bicchi, Rubiolo, et al., 2003	Brat, Rega, et al., 2003	Cavaleiro, Salgueiro, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-1	Ultra-2	DB-5	HP-5	DB-1
Column length (m)	60.	25.	30.	30.	30.
Carrier gas	He	H2	N2	N2	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	60.	40.	70.	60.	40.
T_end (C)	230.	280.	230.	220.	250.
Heat rate (K/min)	2.	3.	2.	5.	2.
Initial hold (min)		2.	2.	10.	5.
Final hold (min)	45.	10.	20.		20.
I	1012.	1025.	1027.	1028.	1005.
Reference	Cavalli, Tomi, et al., 2003	Ceva-Antunes, Bizzo, et al., 2003	Choi, 2003	Ertugrul, Dural, et al., 2003	de Feo, Bruno, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	60.	60.
T_end (C)	250.	240.	220.	220.	220.
Heat rate (K/min)	2.	3.	5.	5.	5.
Initial hold (min)	5.		10.	10.	10.
Final hold (min)
I	1008.	1027.	1028.	1028.	1028.
Reference	de Feo, Urrunaga Soria, et al., 2003	Flamini, Luigi Cioni, et al., 2003	Flamini, Luigi Cioni, et al., 2003, 2	Flamini, Luigi Cioni, et al., 2003, 3	Flamini, Luigi Cioni, et al., 2003, 4
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	DB-5	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He			He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.5		0.25	0.25
T_start (C)	40.	40.	25.	75.	75.
T_end (C)	250.	265.	150.	230.	230.
Heat rate (K/min)	3.	7.	3.	3.	3.
Initial hold (min)			5.	10.	10.
Final hold (min)	20.	5.		20.
I	1006.	1033.	1024.	1024.	1026.
Reference	Gancel, Ollitrault, et al., 2003	Högnadóttir and Rouseff, 2003	Isidorov, Vinogorova, et al., 2003	Jantan, Ling, et al., 2003	bin Jantan, Yassin, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5MS	HP-5	HP-5MS
Column length (m)	25.	30.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	40.	60.	60.
T_end (C)	260.	280.	310.	240.	280.
Heat rate (K/min)	4.	4.	3.	3.	3.
Initial hold (min)		5.	1.
Final hold (min)			20.
I	1026.	1026.	1026.	1027.	1025.
Reference	Javidnia, Miri, et al., 2003	Karioti, Skaltsa, et al., 2003	Lalel, Singh, et al., 2003	Macchioni, Cioni, et al., 2003	Mimica-Dukic, Kujundzic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	SPB-5	HP-5MS	DB-1	RTX-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	40.	45.
T_end (C)	280.	250.	250.	270.	250.
Heat rate (K/min)	3.	4.	3.	2.	3.
Initial hold (min)	10.	2.		5.	6.
Final hold (min)	60.	20.		20.
I	1007.	1026.	1025.	1004.	1026.
Reference	Pino, Almora, et al., 2003	Pino, Marbot, et al., 2003	Salido, Altarejos, et al., 2003	Senatore, Lentini, et al., 2003	Shellie, Marriott, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-1	DB-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	40.	60.	60.
T_end (C)	240.	280.	325.	240.	280.
Heat rate (K/min)	3.	4.	3.	3.	3.
Initial hold (min)		5.
Final hold (min)
I	1022.	1024.	1006.8	1027.	1026.
Reference	Shellie and Marriott, 2003	Skaltsa, Demetzos, et al., 2003	Sun and Stremple, 2003	Tampieri, Galuppi, et al., 2003	Tsiri, Kretsi, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	Mega 5MS	HP-5MS	SPB-1	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.20	0.25
T_start (C)	60.	40.	60.	70.	70.
T_end (C)	280.	240.	275.	220.	230.
Heat rate (K/min)	3.	3.	4.	3.	4.
Initial hold (min)		2.			2.
Final hold (min)				15.	20.
I	1024.	1016.	1030.	1012.	1027.
Reference	Tzakou, Couladis, et al., 2003	Verzera, Trozzi, et al., 2003	Afsharypuor and Suleimany, 2002	Cavaleiro, Salgueiro, et al., 2002	Choi, Kim. M.-S.L., et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	CP Sil 8 CB	SE-52	DB-5	DB-5
Column length (m)	30.	60.	25.	30.	30.
Carrier gas	He	He	N2		He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.15	0.25	0.25
T_start (C)	60.	40.	45.	50.	60.
T_end (C)	300.	250.	200.	280.	240.
Heat rate (K/min)	3.	4.	3.	3.	3.
Initial hold (min)		8.	5.	5.
Final hold (min)		10.	20.
I	1023.	1024.	1021.	1026.	1027.
Reference	Couladis, Chinou, et al., 2002	Duckham, Dodson, et al., 2002	Duru, Cakir, et al., 2002	Economakis, Skaltsa, et al., 2002	Flamini, Cioni, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	RTX-5 MS	SE-30	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	N2		He	N2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	45.	60.	60.
T_end (C)	220.	280.	180.	180.	260.
Heat rate (K/min)	5.	3.	2.5	3.	4.
Initial hold (min)	10.	5.	10.	10.
Final hold (min)				10.
I	1028.	1024.	1023.	1015.	1026.
Reference	Flamini, Cioni, et al., 2002, 2	Fokialakis, Magiatis, et al., 2002	Hudaib, Speroni, et al., 2002	bin Jantan, Ayop, et al., 2002	Javidnia, Miri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	BP-1	DB-5	RTX-5	CP Sil 5 CB
Column length (m)	30.	50.	25.	30.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	60.	60.	70.	45.	60.
T_end (C)	280.	220.	260.	300.	280.
Heat rate (K/min)	3.	2.	4.	3.	4.
Initial hold (min)				6.	6.
Final hold (min)		20.		10.
I	1021.	1012.	1026.	1025.	1003.
Reference	Kovacevic, Pavlovic, et al., 2002	Lota, de Rocca Serra, et al., 2002	Miri, Ramezani, et al., 2002	Mondello, Zappia, et al., 2002	Pino, Marbot, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	CP Sil 5 CB	CP Sil 5 CB	DB-1	HP-5
Column length (m)	30.	30.	50.	50.	30.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.4	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	250.	280.	280.	220.	280.
Heat rate (K/min)	4.	2.	3.	2.	3.
Initial hold (min)	2.	10.	10.
Final hold (min)	20.	40.	60.	20.
I	1026.	1007.	1007.	1012.	1002.
Reference	Pino, Marbot, et al., 2002, 2	Pino, Marbot, et al., 2002, 3	Pino, Marbot, et al., 2002, 4	Pintore, Usai, et al., 2002	Pitarokili, Couladis, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	RTX-5	RTX-5	HP-5	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	45.	45.	60.	60.
T_end (C)	250.	250.	250.	280.	280.
Heat rate (K/min)	5.	3.	3.	3.	3.
Initial hold (min)	2.	6.	6.	5.	5.
Final hold (min)	5.
I	1019.	1026.	1028.	1026.	1025.
Reference	Shang, Hu, et al., 2002	Shellie, Mondello, et al., 2002	Shellie, Mondello, et al., 2002	Aligiannis, Kalpoutzakis, et al., 2001	Aligiannis, Kalpoutzakis, et al., 2001, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-5	HP-5	HP-5MS	HP-1
Column length (m)	50.	30.	30.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	230.	260.	380.	280.	250.
Heat rate (K/min)	2.	3.	3.	3.	2.5
Initial hold (min)				5.	5.
Final hold (min)	35.	10.
I	1013.	1022.	1028.	1026.	1022.
Reference	Bianchini, Tomi, et al., 2001	Couladis, Baziou, et al., 2001	Couladis, Tsortanidou, et al., 2001	Giamakis, Kretsi, et al., 2001	Guilliard, Delgado, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-5 MS	HP-5	DB-1	BP-1
Column length (m)	50.	30.	30.	60.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.22
Phase thickness (μm)	0.25	0.25	0.25	1.	0.25
T_start (C)	50.	70.	40.	40.	60.
T_end (C)	250.	210.	180.	220.	220.
Heat rate (K/min)	2.5	4.	3.	2.	2.
Initial hold (min)	5.	10.		5.
Final hold (min)		10.
I	1026.	1024.	1022.	1014.	1012.
Reference	Guilliard, Delgado, et al., 2001	Hudaib, Grazia Bellardi, et al., 2001	Isidorov, Krajewska, et al., 2001	Kim, 2001	Lota, Serra, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	CP Sil 5 CB	CP Sil 5 CB	BP-1	HP-5MS
Column length (m)	50.	50.	50.	50.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.22	0.32	0.32	0.22	0.25
Phase thickness (μm)	0.25	0.4	0.4	0.25	0.25
T_start (C)	60.	60.	60.	60.	50.
T_end (C)	220.	280.	280.	220.	250.
Heat rate (K/min)	2.	3.	3.	2.	3.
Initial hold (min)		10.	10.
Final hold (min)		60.	60.	20.
I	1012.	1007.	1007.	1011.	1025.
Reference	Lota, Serra, et al., 2001	Pino and Marbot, 2001	Pino, Marbot, et al., 2001	Rezzi, Cavaleiro, et al., 2001	Salido, Altarejos, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	OV-101	SE-54	BPX-5	HP-5
Column length (m)	30.	80.	25.	50.	30.
Carrier gas	He	N2		H2	He
Substrate
Column diameter (mm)	0.25	0.22	0.31	0.22	0.20
Phase thickness (μm)	0.25			0.25	0.25
T_start (C)	60.	30.	35.	60.	60.
T_end (C)	280.	130.	230.	180.	180.
Heat rate (K/min)	4.	1.	4.	4.	4.
Initial hold (min)	5.		3.	5.	8.
Final hold (min)			10.	5.	2.
I	1024.	1011.7	1026.28	1036.	1024.
Reference	Skaltsa, Mavrommati, et al., 2001	Yin, Liu, et al., 2001	Yin, Xiu, et al., 2001	Zabaras and Wyllie, 2001	Alonzo, Bosco, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	CP Sil 8 CB	HP-5	BP-1	BP-1
Column length (m)	30.		30.	50.	50.
Carrier gas	H2		He	He	He
Substrate
Column diameter (mm)	0.32		0.25	0.22	0.22
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	60.
T_end (C)	245.	220.	280.	230.	230.
Heat rate (K/min)	3.	4.	4.	2.	2.
Initial hold (min)	3.	5.	5.
Final hold (min)	20.	30.		35.	35.
I	1005.	1023.	1026.	1012.	1012.
Reference	Brat, Brillouet, et al., 2000	Chevance, Farmer, et al., 2000	Lazari, Skaltsa, et al., 2000	Lota, de Rocca Serra, et al., 2000	Lota, de Rocca Serra, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5	SE-30	CP Sil 5 CB	HP-5	HP-5
Column length (m)	10.	50.	50.	30.	30.
Carrier gas	He		H2	He	He
Substrate
Column diameter (mm)	0.1	0.2	0.22	0.25	0.25
Phase thickness (μm)	0.1		0.13	0.25	0.25
T_start (C)	50.	50.	40.	50.	70.
T_end (C)	350.	250.	300.	280.	230.
Heat rate (K/min)	12.3	6.	4.	4.	2.
Initial hold (min)				5.
Final hold (min)			10.
I	1028.	1020.	1014.	1023.	1025.
Reference	Mondello, Zappia, et al., 2000	Paramonov, Khalilova, et al., 2000	Pfeifhofer, 2000	Skaltsa, Lazari, et al., 2000	Song, Sawamura, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Mega 5MS	CP Sil 8 CB	CP Sil 8 CB	DB-1	DB-1
Column length (m)	30.	25.	50.	60.	60.
Carrier gas	He				He
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.25		1.
T_start (C)	40.	40.	60.	-50.	60.
T_end (C)	240.	200.	220.	175.	230.
Heat rate (K/min)	3.	2.	4.	6.	3.
Initial hold (min)	2.	8.	5.	2.
Final hold (min)			30.		5.
I	1016.	1011.	1024.	1021.0	1016.
Reference	Verzera, la Rosa, et al., 2000	Yassaa, Meklati, et al., 2000	Chevance and Farmer, 1999	Helmig, Klinger, et al., 1999	Javidnia and Shafiee, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	BP-1	OV-101	DB-1
Column length (m)	50.	50.	50.	25.	60.
Carrier gas	He	He	He	N2	He
Substrate
Column diameter (mm)	0.22	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	50.	50.
T_end (C)	230.	230.	220.	200.	220.
Heat rate (K/min)	2.	2.	2.	5.	4.
Initial hold (min)
Final hold (min)	35.	35.	20.
I	1012.	1012.	1011.	1014.	1016.
Reference	Lota, Serra, et al., 1999	Lota, Serra, et al., 1999	Mazzoni, Tomi, et al., 1999	Menut, Bessiere, et al., 1999	Mirza and Sefidkon, 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	Methyl Silicone	OV-1	CP Sil 5 CB
Column length (m)	30.	60.	50.	20.	25.
Carrier gas		He	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.17	0.3
T_start (C)	50.	50.	80.	45.	60.
T_end (C)	220.	250.	200.	220.	260.
Heat rate (K/min)	3.	2.5	2.	10.	5.
Initial hold (min)	3.	5.		5.
Final hold (min)				10.
I	1009.	1009.	1022.	1017.	1015.
Reference	Muselli, Hoi, et al., 1999	Stashenko, Cervantes, et al., 1999	Sumathykutty, Rao, et al., 1999	Valero, Sanz, et al., 1999	Weyerstahl, Marschall, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	DB-5	SPB-5	BP-1	Methyl Silicone
Column length (m)	25.	30.	60.	50.
Carrier gas			He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.22
Phase thickness (μm)	0.3	0.25	1.	0.25
T_start (C)	50.	50.	40.	60.	50.
T_end (C)	200.	250.	200.	220.	250.
Heat rate (K/min)	3.	3.	3.	2.	4.
Initial hold (min)	1.		5.
Final hold (min)	20.		2.	20.
I	1011.	1026.	1031.	1017.	1012.
Reference	Bicchi, Rubiolo, et al., 1998	Isidorov, Zenkevich, et al., 1998	Verdier-Metz., Coulon, et al., 1998	Tam, An, et al., 1998	Analytical Methods Committee, 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	PONA	PONA	BP-1	DB-1
Column length (m)	50.	50.	50.	50.	10.
Carrier gas	He			He	H2
Substrate
Column diameter (mm)	0.22	0.2	0.2	0.22	0.25
Phase thickness (μm)	0.25	0.5	0.5	0.25	0.25
T_start (C)	60.	35.	35.	60.	80.
T_end (C)	230.	220.	220.	230.	160.
Heat rate (K/min)	2.	1.	1.	2.	5.
Initial hold (min)		0.5	0.5
Final hold (min)	35.	8.	8.	35.
I	1013.	1008.1	1008.6	1010.	1008.
Reference	Mariotti, Costa, et al., 1997	Martos, Saraullo, et al., 1997	Martos, Saraullo, et al., 1997	Mariotti, Tomi, et al., 1997	Perry, van Klink, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-1	Methyl Silicone	DB-1	CP Sil 5 CB
Column length (m)	30.		25.	60.	25.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.26		0.2	0.25	0.22
Phase thickness (μm)	0.25		0.3	0.25	0.11
T_start (C)	50.	35.	40.	70.	80.
T_end (C)	225.	300.	200.	250.	230.
Heat rate (K/min)	2.	8.	2.	2.5	1.
Initial hold (min)				5.	8.
Final hold (min)	20.			15.	16.
I	1027.	1011.7	1026.	1013.	1010.
Reference	Sagrero-Nieves, Bartley, et al., 1997	Gautzsch and Zinn, 1996	Píry, Príbela, et al., 1995	Combariza, Tirado, et al., 1994	Chanegriha and Baaliouamer, 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-101	DB-1	Petrocol DH	Petrocol DH	Petrocol DH
Column length (m)	50.	30.	100.	100.	100.
Carrier gas	N2		He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)		1.5	0.5	0.5	0.5
T_start (C)	70.	40.	30.	30.	30.
T_end (C)	200.	280.	220.	220.	220.
Heat rate (K/min)	3.	8.	1.	1.	1.
Initial hold (min)		4.
Final hold (min)
I	1025.	1020.	1010.45	1010.9	1011.
Reference	Chung, Eiserich, et al., 1993	Peng, Hua, et al., 1992	White, Douglas, et al., 1992	White, Douglas, et al., 1992	White, Hackett, et al., 1992
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-5	HP-1	OV-101
Column length (m)	50.	50.	60.	50.	50.
Carrier gas	N2	N2	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.32	0.32
Phase thickness (μm)			1.	1.05
T_start (C)	80.	80.	40.	40.	50.
T_end (C)	200.	200.	220.	230.	200.
Heat rate (K/min)	2.	2.	3.	2.	2.
Initial hold (min)
Final hold (min)				40.
I	1017.	1018.	1026.	1016.	1012.
Reference	Yang, Sugisawa, et al., 1992	Yang, Sugisawa, et al., 1992	Le Quere and Latrasse, 1990	Tang, Zhang, et al., 1990	Pieribattesti, Smadja, et al., 1988
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Packed	Capillary
Active phase	CP Sil 5 CB	OV-1	OV-1	OV-101	OV-101
Column length (m)	25.	30.	30.	2.
Carrier gas	N2	He	He	Ar
Substrate				W-AW-DMCS
Column diameter (mm)	0.22	0.5	0.5
Phase thickness (μm)		0.8	0.8
T_start (C)	70.	40.	40.	100.	100.
T_end (C)	295.	220.	220.
Heat rate (K/min)	4.	2.	2.	2.	2.
Initial hold (min)
Final hold (min)
I	1017.	1008.	1012.	1017.	1026.
Reference	Montanarella, Bos, et al., 1986	De Pooter, Omar, et al., 1985	De Pooter, Omar, et al., 1985	Szabolcs, Benecke, et al., 1985	Benecke, Thieme, et al., 1982
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary
Active phase	OV-101
Column length (m)	108.
Carrier gas
Substrate
Column diameter (mm)	0.25
Phase thickness (μm)	0.2
T_start (C)	35.
T_end (C)	200.
Heat rate (K/min)	1.
Initial hold (min)
Final hold (min)
I	1009.
Reference	Hayes and Pitzer, 1981
Comment	MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

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Choi, H.-S., Character impact odorants of Citrus Hallabong [(C. unshiu Marcov × C. sinensis Osbeck) × C. reticulata Blanco] cold-pressed peel oil, J. Agric. Food Chem., 2003, 51, 9, 2687-2692, https://doi.org/10.1021/jf021069o . [all data]

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Gancel, A.-L.; Ollitrault, P.; Froelicher, Y.; Tomi, F.; Jacquemond, C.; Luro, F.; Brillouet, J.-M., Leaf volatile compounds of seven citrus somatic tetraploid hybrids sharing willow leaf mandarin (Citrus deliciosa Ten.) as their common parent, J. Agric. Food Chem., 2003, 51, 20, 6006-6013, https://doi.org/10.1021/jf0345090 . [all data]

Högnadóttir and Rouseff, 2003
Högnadóttir, Á.; Rouseff, R.L., Identification of aroma active compounds in organce essence oil using gas chromatography-olfactometry and gas chromatography-mass spectrometry, J. Chromatogr. A, 2003, 998, 1-2, 201-211, https://doi.org/10.1016/S0021-9673(03)00524-7 . [all data]

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Isidorov, V.A.; Vinogorova, V.T.; Rafalowski, K., HS-SPME analysis of volatile organic compounds of coniferous needle litter, Atmos. Environ., 2003, 37, 33, 4645-4650, https://doi.org/10.1016/j.atmosenv.2003.07.005 . [all data]

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Jantan, I.; Ling, Y.E.; Romli, S.; Ayop, N.; Ahmad, A.S., A comparative study of the constituents of the essential oils of three Cinnamomum species from Malaysia, J. Essent. Oil Res., 2003, 15, 6, 387-391, https://doi.org/10.1080/10412905.2003.9698618 . [all data]

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bin Jantan, I.; Yassin, M.S.M.; Chin, C.B.; Chen, L.L.; Sim. N.L., Antifungal activity of the essential oils of nine Zingiberaceae species, Pharm. Biol., 2003, 41, 5, 392-397, https://doi.org/10.1076/phbi.41.5.392.15941 . [all data]

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Javidnia, K.; Miri, R.; Azarpira, A.; Tabaei, S.M.H., Composition of the essential oil of Stachys setifera C.A. Mey ssp. iranica growing in Iran, Flavour Fragr. J., 2003, 18, 4, 299-300, https://doi.org/10.1002/ffj.1165 . [all data]

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Karioti, A.; Skaltsa, H.; Demetzos, C.; Perdetzoglou, D.; Economakis, C.D.; Salem, A.B., Effect of nitrogen concentration of the nutrient solution on the volatile constituents of leaves of Salvia fruticosa Mill. in solution culture, J. Agric. Food Chem., 2003, 51, 22, 6505-6508, https://doi.org/10.1021/jf030308k . [all data]

Lalel, Singh, et al., 2003
Lalel, H.J.D.; Singh, Z.; Chye Tan, S., Glycosidically-bound aroma volatile compounds in the skin and pulp of 'Kensington Pride' mango fruit at different stages of maturity, Postharvest Biol. Technol., 2003, 29, 2, 205-218, https://doi.org/10.1016/S0925-5214(02)00250-8 . [all data]

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Macchioni, F.; Cioni, P.L.; Flamini, G.; Morelli, I.; Maccioni, S.; Ansaldi, M., Chemical composition of essential oils from needles, branches and cones of Pinus pinea, P. halepensis, P. pinaster and P. nigra from central Italy, Flavour Fragr. J., 2003, 18, 2, 139-143, https://doi.org/10.1002/ffj.1178 . [all data]

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Mimica-Dukic, N.; Kujundzic, S.; Sokovic, M.; Couladis, M., Essential oil composition and antifungal activity of Foeniculum vulgare Mill. obtained by different distillation conditions, Phytother. Res., 2003, 17, 4, 368-371, https://doi.org/10.1002/ptr.1159 . [all data]

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Pino, J.; Almora, K.; Marbot, R., Volatile components of papaya (Carica papaya L., maradol variety) fruit, Flavour Fragr. J., 2003, 18, 6, 492-496, https://doi.org/10.1002/ffj.1248 . [all data]

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Pino, J.; Marbot, R.; Rosado, A.; Vázquez, C., Volatile constituents of fruits of Garcinia dulcis Kurz. from Cuba, Flavour Fragr. J., 2003, 18, 4, 271-274, https://doi.org/10.1002/ffj.1187 . [all data]

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Salido, S.; Altarejos, J.; Nogueras, M.; Sánchez, A.; Luque, P., Chemical composition and seasonal variations of rosemary oil from Southern Spain, J. Essent. Oil Res., 2003, 15, 1, 10-14, https://doi.org/10.1080/10412905.2003.9712248 . [all data]

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Senatore, F.; Lentini, F.; Venza, F.; Bruno, M.; Napolitano, F., Composition and antibacterial activity of the essential oil of Anisochilus carnosus (Linn. fil.) Benth., a Tamil plant acclimatized in Sicily, Flavour Fragr. J., 2003, 18, 3, 202-204, https://doi.org/10.1002/ffj.1183 . [all data]

Shellie, Marriott, et al., 2003
Shellie, R.; Marriott, P.; Zappia, G.; Mondello, L.; Dugo, G., Interactive use of linear retention indices on polar and apolar columns with an MS-Library for reliable characterization of Australian tea tree and other Melaleuca sp. oils, J. Essent. Oil Res., 2003, 15, 5, 305-312, https://doi.org/10.1080/10412905.2003.9698597 . [all data]

Shellie and Marriott, 2003
Shellie, R.A.; Marriott, P.J., Comprehensive two-dimensional gas chromatography-mass spectrometry analysis of Pelargonium graveolens essential oil using rapid scanning quadrupole mass spectrometry, Analyst, 2003, 128, 7, 879-883, https://doi.org/10.1039/b304371a . [all data]

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Skaltsa, H.D.; Demetzos, C.; Lazari, D.; Sokovic, M., Essential oil analysis and antimicrobial activity of eight Stachys species from Greece, Phytochemistry, 2003, 64, 3, 743-752, https://doi.org/10.1016/S0031-9422(03)00386-8 . [all data]

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

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Tampieri, M.P.; Galuppi, R.; Carelle, M.S.; Macchioni, F.; Cioni, P.L.; Morelli, I., Effect of selected essential oils and pure compounds on Saprolegnia parasitica, Pharm. Biol., 2003, 41, 8, 584-591, https://doi.org/10.1080/13880200390501839 . [all data]

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Tsiri, D.; Kretsi, O.; Chinou, I.B.; Spyropoulos, C.G., Composition of fruit volatiles and annual changes in the volatiles of leaves of Eucalyptus camaldulensis Dehn. growing in Greece, Flavour Fragr. J., 2003, 18, 3, 244-247, https://doi.org/10.1002/ffj.1220 . [all data]

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Tzakou, O.; Couladis, M.; Slavkovska, V.; Mimica-Dukic, N.; Jancic, R., The essential oil composition of Salvia brachyodon Vandas, Flavour Fragr. J., 2003, 18, 1, 2-4, https://doi.org/10.1002/ffj.1132 . [all data]

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Chevance, F.F.V.; Farmer, L.J., Identification of major volatile odor compounds in frankfurters, J. Agric. Food Chem., 1999, 47, 12, 5151-5160, https://doi.org/10.1021/jf990515d . [all data]

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Gautzsch and Zinn, 1996
Gautzsch, R.; Zinn, P., Use of incremental models to estimate the retention indexes of aromatic compounds, Chromatographia, 1996, 43, 3/4, 163-176, https://doi.org/10.1007/BF02292946 . [all data]

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Hayes, P.C., Jr.; Pitzer, E.W., Kovats indices as a tool in characterizing hydrocarbon fuels in temperature programmed glass capillary gas chromatography. Part 1. Qualitative identification, Inhouse rpt. for Air Force Wright Aeronautical Labs., Air Force Wright Aeronautical Labs., Wright-Patterson AFB, Ohio, 1981, 75. [all data]

Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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