Diethylpropion
- Formula: C13H19NO
- Molecular weight: 205.2961
- IUPAC Standard InChIKey: XXEPPPIWZFICOJ-UHFFFAOYSA-N
- CAS Registry Number: 90-84-6
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: Amfepramone; 1-Propanone, 2-(diethylamino)-1-phenyl-; Diethylcathionine; Propiophenone, 2-(diethylamino)-; α-Benzoyltriethylamine; Adiposon; Amfepramon; Amphepramon; Amphepramone; Anorex; Cegramine; Danylen; Derfon; Diethylpropione; Dobesin; Frekentine; Magrene; Neobes; Nopropiophenone; Obesitex; Silutin; Tepanil; Tylinal; 2-(Diethylaminopropio)phenone; α-Diethylaminopropiophenone; Fenyl-(1-diethylaminoethyl)keton; 1-Phenyl-2-diethylamino-1-propanone; UR 1423; 2-(Diethylamino)-1-phenyl-1-propanone; Tenuate; Magrex Retard; Menutil; Moderatan; Nu-Dispoz
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Gas Chromatography
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, isothermal
Column type | Active phase | Temperature (C) | I | Reference | Comment |
---|---|---|---|---|---|
Capillary | BP-1 | 130. | 1476. | Japp, Gill, et al., 1987 | 25. m/0.22 mm/0.25 μm, N2 |
Capillary | BP-1 | 130. | 1489. | Japp, Gill, et al., 1987 | 25. m/0.53 mm/1. μm, N2 |
Packed | Apiezon L | 160. | 1490. | Huber, Kenndler, et al., 1979 | |
Packed | Apiezon L | 160. | 1518. | Donike and Stratmann, 1976 | Chromosorb W |
Kovats' RI, non-polar column, custom temperature program
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Packed | OV-101 | 1490. | McLinden and Stenhouse, 1979 | N2, Chromosorb W; Column length: 2. m; Program: not specified |
Packed | SE-30 | 1480. | Moffat, Stead, et al., 1974 | Column length: 2. m; Program: not specified |
Kovats' RI, polar column, isothermal
Column type | Active phase | Temperature (C) | I | Reference | Comment |
---|---|---|---|---|---|
Packed | PEG-20M | 160. | 1965. | Huber, Kenndler, et al., 1979 | N2 |
Packed | PEG-20M | 160. | 1965. | Donike and Stratmann, 1976 | Chromosorb W |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | VF-5MS | 1515. | Tretyakov, 2014 | 30. m/0.25 mm/0.25 μm, He; Tstart: 60. C; Tend: 270. C |
Capillary | SE-30 | 1470. | Anderson and Stafford, 1983 | 15. m/0.25 mm/0.25 μm, He, 5. K/min; Tstart: 100. C; Tend: 295. C |
Packed | SE-30 | 1495. | Perrigo and Peel, 1981 | N2, Chromosorb W, 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 1.8 m |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | BP-1 | 1483. | Stowell and Wilson, 1987 | 12. m/0.22 mm/0.25 μm, He; Program: 120C => 8C/min => 270C => 25C/min => 300C |
Normal alkane RI, non-polar column, isothermal
Column type | Active phase | Temperature (C) | I | Reference | Comment |
---|---|---|---|---|---|
Capillary | Apieson L / KOH | 150. | 1472. | Caddy, Fish, et al., 1973 | |
Capillary | Apieson L / KOH | 150. | 1477. | Caddy, Fish, et al., 1973 | |
Capillary | Apieson L / KOH | 150. | 1478. | Caddy, Fish, et al., 1973 | |
Capillary | Apieson L / KOH | 190. | 1495. | Caddy, Fish, et al., 1973 | |
Capillary | Apieson L / KOH | 190. | 1500. | Caddy, Fish, et al., 1973 | |
Capillary | Apieson L / KOH | 190. | 1503. | Caddy, Fish, et al., 1973 |
Normal alkane RI, non-polar column, temperature ramp
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | BP-1 | 1470. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He, 5. K/min; Tstart: 100. C; Tend: 295. C |
Packed | OV-1 | 1465. | Marozzi, Gambaro, et al., 1982 | Gas Chrom P, 2.5 K/min; Column length: 2. m; Tstart: 120. C; Tend: 200. C |
Packed | SE-30 | 1475. | Marozzi, Gambaro, et al., 1982 | Gas Chrom P, 2.5 K/min; Column length: 2. m; Tstart: 120. C; Tend: 200. C |
Normal alkane RI, non-polar column, custom temperature program
Column type | Active phase | I | Reference | Comment |
---|---|---|---|---|
Capillary | BP-1 | 1483. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He; Program: 120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min) |
Capillary | BP-1 | 1480. | Stowell and Wilson, 1985 | 12. m/0.22 mm/0.25 μm, He; Program: not specified |
Capillary | OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc. | 1470. | Waggott and Davies, 1984 | Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified |
Other | Methyl Silicone | 1486. | Ardrey and Moffat, 1981 | Program: not specified |
Capillary | Methyl Silicone | 1485. | Pearson and Brown, 1978 | Program: not specified |
Normal alkane RI, polar column, isothermal
Column type | Active phase | Temperature (C) | I | Reference | Comment |
---|---|---|---|---|---|
Capillary | Carbowax 20M / KOH | 150. | 1982. | Caddy, Fish, et al., 1973 | |
Capillary | Carbowax 20M / KOH | 150. | 1991. | Caddy, Fish, et al., 1973 | |
Capillary | Carbowax 20M / KOH | 150. | 1999. | Caddy, Fish, et al., 1973 | |
Capillary | Carbowax 20M / KOH | 190. | 2011. | Caddy, Fish, et al., 1973 | |
Capillary | Carbowax 20M / KOH | 190. | 2023. | Caddy, Fish, et al., 1973 | |
Capillary | Carbowax 20M / KOH | 190. | 2032. | Caddy, Fish, et al., 1973 |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Japp, Gill, et al., 1987
Japp, M.; Gill, R.; Osselton, M.D.,
Comparison of drug retention indices determined on packed, wide bore capillary and narrow bore capillary columns,
J. Forensic Sci., 1987, 32, 6, 1574-1586. [all data]
Huber, Kenndler, et al., 1979
Huber, J.F.K.; Kenndler, E.; Reich, G.,
Quantitation of the Information Content of Multi-Dimensional Gas Chromatography and Low- Resolution Mass Spectrometry in the Identification of Doping Drugs,
J. Chromatogr., 1979, 172, 1, 15-30, https://doi.org/10.1016/S0021-9673(00)90941-5
. [all data]
Donike and Stratmann, 1976
Donike, M.; Stratmann, D.,
Gas-chromatographische identifizierung von stimulantien der phenyläthylaminreihe mit hilfe der retnetions-indices,
Z. Anal. Chem., 1976, 279, 2, 129-131, https://doi.org/10.1007/BF00440798
. [all data]
McLinden and Stenhouse, 1979
McLinden, V.J.; Stenhouse, A.M.,
A chromatography system for drug identification,
Forensic Sci. Int., 1979, 13, 71-79, https://doi.org/10.1016/0379-0738(79)90265-2
. [all data]
Moffat, Stead, et al., 1974
Moffat, A.C.; Stead, A.H.; Smalldon, K.W.,
Optimum use of paper, thin-layer and gas-liquid chromatography for the identification of basic drugs. III. Gas-liquid chromatography,
J. Chromatogr., 1974, 90, 1, 19-33, https://doi.org/10.1016/S0021-9673(01)94770-3
. [all data]
Tretyakov, 2014
Tretyakov, K.V.,
Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]
Anderson and Stafford, 1983
Anderson, W.H.; Stafford, D.T.,
Applications of capillary gas chromatography in routine toxicological analyses,
J. Hi. Res. Chromatogr. Chromatogr. Comm., 1983, 6, 5, 247-254, https://doi.org/10.1002/jhrc.1240060506
. [all data]
Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W.,
The use of retention indices and temperature-programmed gas chromatography in analytical toxicology,
J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219
. [all data]
Stowell and Wilson, 1987
Stowell, A.; Wilson, L.W.,
A simple approach to the interlaboratory transfer of drug retention indices determined by temperature programmed capillary gas chromatography,
J. Forensic Sci., 1987, 32, 5, 1214-1220. [all data]
Caddy, Fish, et al., 1973
Caddy, B.; Fish, F.; Scott, D.,
Chromatographic screening for drugs of abuse using capillary columds. II. Peak identification on support coated open tubular columns for a series of central nervous system stimulating drugs,
Chromatographia, 1973, 6, 7, 293-300, https://doi.org/10.1007/BF02269329
. [all data]
Stowell and Wilson, 1985
Stowell, A.; Wilson, L.,
Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]
Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F.,
Use of the retention index in gas chromatographic studies of drugs,
J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185
. [all data]
Waggott and Davies, 1984
Waggott, A.; Davies, I.W.,
Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]
Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C.,
Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase,
J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1
. [all data]
Pearson and Brown, 1978
Pearson, E.F.; Brown, C.,
The development and applications of the computer system of the Home Office Central Research Establishment, Instrument Applications in Forensic Drug Chemistry, Proceedings of the International Symposium, May 29-30, 1978, 1978, 299. [all data]
Notes
Go To: Top, Gas Chromatography, References
- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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