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Stigmasterol

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type PackedPackedPackedPackedPacked
Active phase SE-30SE-30SE-30E-301E-301
Column length (m) 1.21.21.21.21.2
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 230.240.250.210.220.
I 3148.3170.3172.3143.3138.
ReferenceKeiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedCapillary
Active phase E-301E-301E-301E-301CP Sil 5 CB
Column length (m) 1.21.21.21.250.
Carrier gas N2N2N2N2H2
Substrate      
Column diameter (mm)     0.22
Phase thickness (mum)     0.12
Temperature (C) 220.230.230.240.270.
I 3166.3142.3191.3164.3213.
ReferenceKeiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990Keiser, Retunskii, et al., 1990van Gelder, Jonker, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase SE-30SE-30SE-30SE-30SE-30
Column length (m) 1.21.21.21.21.2
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm)      
Phase thickness (mum)      
Temperature (C) 230.240.250.240.240.
I 3148.3170.3172.3140.3142.
ReferenceKeiser, Yazlovetsky, et al., 1986Keiser, Yazlovetsky, et al., 1986Keiser, Yazlovetsky, et al., 1986Keiser, Yazlovetsky, et al., 1986Keiser, Yazlovetsky, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m) 1.2
Carrier gas N2
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Temperature (C) 240.
I 3145.
ReferenceKeiser, Yazlovetsky, et al., 1986
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Keiser, Retunskii, et al., 1990
Keiser, L.S.; Retunskii, V.N.; Yazlovetskii, I.G., Gas chromatographic identification of sterols in insects. Estimation of retention data reproducibility, Zh. Anal. Khim., 1990, 45, 1767-1773. [all data]

van Gelder, Jonker, et al., 1988
van Gelder, W.M.J.; Jonker, H.H.; Huizing, H.J.; Scheffer, J.J.C., Capillary gas chromatography of steroidal alkaloids from Solanaceae. Retention indices and simultaneous flame ionization/nitrogen-specific detection, J. Chromatogr., 1988, 442, 133-145, https://doi.org/10.1016/S0021-9673(00)94463-7 . [all data]

Keiser, Yazlovetsky, et al., 1986
Keiser, L.S.; Yazlovetsky, I.G.; Retunsky, V.N., Gas-chromatographic indentification of sterols in insects with the use of two-dimentional three-phase diagrams plotted on the basis of logarithmic retention indices, J. Anal. Chem. USSR (Engl. Transl.), 1986, 41, 9, 1166-1172. [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, isothermal, References