3,5-Dihydroxybenzoic acid, 3TMS derivative
- Formula: C16H30O4Si3
- Molecular weight: 370.6635
- IUPAC Standard InChI: InChI=1S/C16H30O4Si3/c1-21(2,3)18-14-10-13(16(17)20-23(7,8)9)11-15(12-14)19-22(4,5)6/h10-12H,1-9H3
- IUPAC Standard InChIKey: ASTWSDQOZSFLPZ-UHFFFAOYSA-N
- CAS Registry Number: 79314-27-5
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 3,5-Bis(trimethylsiloxy)benzoic acid, trimethylsilyl ester; 3,5-Dihydroxybenzoic acid, bis(trimethylsilyl) ether, trimethylsilyl ester; Benzoic acid, 3,5-bis-(trimethylsilyloxy), trimethylsilyl ester; Benzoic acid, 3,5-dihydroxy, tris-TMS; Trimethylsilyl 3,5-bis[(trimethylsilyl)oxy]benzoate; Benzoic acid, 3,5-dihydroxy, TMS
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
- Options:
Van Den Dool and Kratz RI, non-polar column, temperature ramp
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Packed | Packed |
|---|---|---|
| Active phase | OV-1 | OV-1 |
| Column length (m) | 2. | 2. |
| Carrier gas | N2 | He |
| Substrate | Supelcoport | Chromosorb W HP (80-100 mesh) |
| Column diameter (mm) | ||
| Phase thickness (μm) | ||
| Tstart (C) | 80. | 100. |
| Tend (C) | 240. | 325. |
| Heat rate (K/min) | 4. | 10. |
| Initial hold (min) | ||
| Final hold (min) | ||
| I | 1828. | 1830. |
| Reference | Mattsson and Petersson, 1977 | Butts, 1972 |
| Comment | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Mattsson and Petersson, 1977
Mattsson, M.; Petersson, G.,
Reference GLC Data for the Analysis of Phenolic Compounds as Trimethylsilyl Derivatives,
J. Chromatogr. Sci., 1977, 15, 12, 546-554, https://doi.org/10.1093/chromsci/15.12.546
. [all data]
Butts, 1972
Butts, W.C.,
Two-Column Gas Chromatography of Trimethylsilyl Derivatives of Biochemically Significant Compounds,
Anal. Biochemistry, 1972, 46, 1, 187-199, https://doi.org/10.1016/0003-2697(72)90411-3
. [all data]
Notes
Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References
- Symbols used in this document:
Tend Final temperature Tstart Initial temperature - Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
- The National Institute of Standards and Technology (NIST) uses its best efforts to deliver a high quality copy of the Database and to verify that the data contained therein have been selected on the basis of sound scientific judgment. However, NIST makes no warranties to that effect, and NIST shall not be liable for any damage that may result from errors or omissions in the Database.
- Customer support for NIST Standard Reference Data products.