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6«beta»-Hydroxymethandienone, 2TMS derivative


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySE-542919.Schänzer, Opfermann, et al., 19925. K/min; Column length: 17. m; Phase thickness: 0.33 «mu»m; Tstart: 200. C; Tend: 320. C

Normal alkane RI, non-polar column, custom temperature program

View large format table.

Column type Active phase I Reference Comment
CapillaryDB-12915.Bowers, 199630. m/0.25 mm/0.25 «mu»m, Helium; Program: 170 0C 20 0C/min -> 260 0C 2.7 0C/min -> 305 0C 20 0C/min -> 320 0C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Schänzer, Opfermann, et al., 1992
Schänzer, W.; Opfermann, G.; Donike, M., 17-Epimerization of 17«alpha»-methyl anabolic steroids in humans: metabolism and synthesis of 17«alpha»-hydroxy-17«beta»-methyl steroids, Steroids, 1992, 57, 11, 537-550, https://doi.org/10.1016/0039-128X(92)90023-3 . [all data]

Bowers, 1996
Bowers, L.D., Separation and confirmation of anabolic steroids with quadrupole ion trap tandem mass spectrometry, J. Chromatogr. B, 1996, 687, 1, 69-78, https://doi.org/10.1016/S0378-4347(96)00231-9 . [all data]


Notes

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