2-Butanol, 1,2-diphenyl-4-(methylamino)-3-methyl-, propionate


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-1DB-1SE-30
Column length (m) 30.15.15.15.15.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.750.250.250.250.25
Phase thickness (μm) 1.00.250.250.250.25
Tstart (C) 160.120.120.120.100.
Tend (C) 280.280.280.280.295.
Heat rate (K/min) 10.8.8.8.5.
Initial hold (min)      
Final hold (min) 12.5.5.5. 
I 2394.2364.2388.2407.2370.
ReferenceChrist, Noomano, et al., 1988Perrigo, Ballantyne, et al., 1984Perrigo, Ballantyne, et al., 1984Perrigo, Ballantyne, et al., 1984Anderson and Stafford, 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase SE-30
Column length (m) 1.8
Carrier gas N2
Substrate Chromosorb W
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 130.
Tend (C) 290.
Heat rate (K/min) 8.
Initial hold (min) 2.
Final hold (min) 8.
I 2380.
ReferencePerrigo and Peel, 1981
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Christ, Noomano, et al., 1988
Christ, D.W.; Noomano, P.; Rosas, M.; Rhone, D., Retention indices by wide-bore capillary gas chromatography with nitrogen-phosphorus detection, J. Anal. Toxicol., 1988, 12, 2, 84-88, https://doi.org/10.1093/jat/12.2.84 . [all data]

Perrigo, Ballantyne, et al., 1984
Perrigo, B.J.; Ballantyne, D.J.; Peel, H.W., Condierations in developing a data base for drugs on a DBI capillary column, J. Can. Soc. Forensic Sci., 1984, 17, 2, 41-49, https://doi.org/10.1080/00085030.1984.10757360 . [all data]

Anderson and Stafford, 1983
Anderson, W.H.; Stafford, D.T., Applications of capillary gas chromatography in routine toxicological analyses, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1983, 6, 5, 247-254, https://doi.org/10.1002/jhrc.1240060506 . [all data]

Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W., The use of retention indices and temperature-programmed gas chromatography in analytical toxicology, J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219 . [all data]


Notes

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