9H-Fluorene, 2-nitro-

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Lee's RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5SE-52SE-52SE-52
Column length (m) 30.60.12.30.30.
Carrier gas Helium HydrogenHeHe
Substrate      
Column diameter (mm) 0.250.24 0.30.2
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 50.50.120.25.25.
Tend (C) 310.280.285.295.295.
Heat rate (K/min) 6.6.3.4.4.
Initial hold (min) 1.5    
Final hold (min) 10.    
I 351.77350.98353.06352.17352.12
ReferencePedersen, Durant, et al., 2005Helmig and Arey, 1991Boenke and Ballschmiter, 1987White, Robbat, et al., 1983White, Robbat, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase SE-52SE-52SE-52SE-52
Column length (m) 30.30.30.20.
Carrier gas HeHeHeH2
Substrate     
Column diameter (mm) 0.30.30.30.30
Phase thickness (μm) 0.250.250.250.25
Tstart (C) 100.40.70.40.
Tend (C) 300.300.300.265.
Heat rate (K/min) 4.4.4.4.
Initial hold (min)    2.
Final hold (min)     
I 352.22352.60352.42353.06
ReferenceWhite, Robbat, et al., 1983White, Robbat, et al., 1983White, Robbat, et al., 1983Vassilaros, Kong, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Lee's RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pedersen, Durant, et al., 2005
Pedersen, D.U.; Durant, J.L.; Taghizadeh, K.; Hemond, H.F.; Lafleur, A.L.; Cass, G.R., Human cell mutagenes in respirable airborne particles from the Northeastern United States. 2. Quantification of mutagenes and other organic compounds., Environ. Sci. Technol., 2005, 39, 24, 9547-9560, https://doi.org/10.1021/es050886c . [all data]

Helmig and Arey, 1991
Helmig, D.; Arey, J., Analytical chemistry of airborne nitrofluorenes, Int. J. Environ. Anal. Chem., 1991, 43, 4, 219-233, https://doi.org/10.1080/03067319108027526 . [all data]

Boenke and Ballschmiter, 1987
Boenke, A.; Ballschmiter, K., Fused quinones as retention index marker in high resolution gas chromatography with electron-capture detection (HRGC/ECD) of oxidized aromatic compounds, Fresenius J. Anal. Chem., 1987, 327, 1, 44-45, https://doi.org/10.1007/BF00474554 . [all data]

White, Robbat, et al., 1983
White, C.M.; Robbat, A., Jr.; Hoes, R.M., Gas chromatographic retention characteristics of nitrated polycyclic aromatic hydrocarbons on SE-52, Chromatographia, 1983, 17, 11, 605-612, https://doi.org/10.1007/BF02261944 . [all data]

Vassilaros, Kong, et al., 1982
Vassilaros, D.L.; Kong, R.C.; Later, D.W.; Lee, M.L., Linear retention index system for polycyclic aromatic compounds. Critical evaluation and additional indices, J. Chromatogr., 1982, 252, 1-20, https://doi.org/10.1016/S0021-9673(01)88394-1 . [all data]


Notes

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