1-Naphthalenepropanol, α-ethenyldecahydro-α,5,5,8a-tetramethyl-2-methylene-, [1S-[1α(S*),4aβ,8aα]]-
- Formula: C20H34O
- Molecular weight: 290.4834
- IUPAC Standard InChI: InChI=1S/C20H34O/c1-7-19(5,21)14-11-16-15(2)9-10-17-18(3,4)12-8-13-20(16,17)6/h7,16-17,21H,1-2,8-14H2,3-6H3/t16-,17?,19?,20+/m1/s1
- IUPAC Standard InChIKey: CECREIRZLPLYDM-OQUMVOOASA-N
- CAS Registry Number: 596-85-0
- Chemical structure:
This structure is also available as a 2d Mol file - Stereoisomers:
- Other names: Labda-8(20),14-dien-13-ol, (13R)-; Manool
- Permanent link for this species. Use this link for bookmarking this species for future reference.
- Information on this page:
- Other data available:
- Options:
Gas Chromatography
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Kovats' RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-5 | 2055. | Adams, González Elizondo, et al., 2006 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | DB-5 | 2057. | Barbosa, Paula, et al., 2005 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 240. C @ 15. min; Tstart: 60. C |
| Capillary | HP-5 | 2056. | Mita, Tsitsimpikou, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 3. K/min, 240. C @ 20. min; Tstart: 60. C |
| Capillary | SE-54 | 2055. | Adams, 2000 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | SE-54 | 2056. | Adams, 2000, 2 | 30. m/0.26 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | DB-5 | 2054. | Adams, 2000, 3 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
Kovats' RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | CP Sil 8 CB | 2057. | Radusiene, Judzentiene, et al., 2005 | 50. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C |
Van Den Dool and Kratz RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | SPB-1 | 2087. | Radulovic, Lazarevic, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 3. min, 5. K/min, 250. C @ 15. min |
| Capillary | HP-5MS | 2055. | Radulovic, Lazarevic, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 60. C @ 5. min, 4. K/min; Tend: 280. C |
| Capillary | DB-5 | 2048. | Rout, Rao, et al., 2007 | 25. m/0.25 mm/0.25 μm, He, 2. K/min, 200. C @ 60. min; Tstart: 60. C |
| Capillary | BP-1 | 2046. | Duquesnoy, Dinh, et al., 2006 | 50. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | BP-1 | 2048. | Gonny, Cavaleiro, et al., 2006 | 50. m/0.22 mm/0.25 μm, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C |
| Capillary | HP-5 | 2055. | Javidnia, Miri, et al., 2005 | He, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 260. C |
| Capillary | DB-5 | 2057. | Adams, Habte, et al., 2004 | 30. m/0.26 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 246. C |
| Capillary | HP-5MS | 2056. | Demetzos, Angelopoulou, et al., 2002 | 30. m/0.25 mm/0.25 μm, 50. C @ 5. min, 3. K/min; Tend: 280. C |
| Capillary | HP-5 | 2033. | Pitarokili, Couladis, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5 | 2055. | Couladis, Tzakou, et al., 2001 | 30. m/0.25 mm/0.50 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | RTX-5 MS | 2065. | Hudaib, Grazia Bellardi, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 70. C @ 10. min, 4. K/min, 210. C @ 10. min |
| Capillary | RTX-5 MS | 2080. | Hudaib, Grazia Bellardi, et al., 2001 | 30. m/0.25 mm/0.25 μm, He, 70. C @ 10. min, 4. K/min, 210. C @ 10. min |
| Capillary | HP-5 | 2057. | Lazari, Skaltsa, et al., 2000 | 30. m/0.25 mm/0.25 μm, He, 50. C @ 5. min, 4. K/min; Tend: 280. C |
Van Den Dool and Kratz RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | 5 % Phenyl methyl siloxane | 2057. | Sacchetti, Maietti, et al., 2005 | 30. m/0.32 mm/0.15 μm, He; Program: 45C => 1C/min => 100C => 5C/min => 250C (10min) |
| Capillary | HP-5 | 2050. | García, Alvarez, et al., 2002 | 50. m/0.2 mm/0.33 μm, He; Program: 50C(2min) => 5C/min => 150C => 10C/min => 250C(30min) |
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | HP-1 | 2056. | Alizadeh and Shaabani, 2012 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | HP-5 | 2048. | Velickovic, Ristic, et al., 2012 | 25. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C |
| Capillary | HP-5 | 2048. | Velickovic, Ristic, et al., 2012 | 25. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C |
| Capillary | HP-5 | 2048. | Velickovic, Ristic, et al., 2012 | 25. m/0.32 mm/0.52 μm, Hydrogen, 4. K/min, 280. C @ 10. min; Tstart: 40. C |
| Capillary | CP-Sil 5 CB | 2072. | Mothana, Hasson, et al., 2011 | 30. m/0.25 mm/0.26 μm, Nitrogen, 3. K/min, 280. C @ 22. min; Tstart: 45. C |
| Capillary | HP-5 | 2050. | Bousaada, Ammar, et al., 2008 | 30. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min |
| Capillary | HP-5 | 2055. | Saidana, Mahjoub, et al., 2008 | 30. m/0.25 mm/0.25 μm, Nitrogen, 50. C @ 1. min, 5. K/min, 280. C @ 1. min |
| Capillary | CP Sil 5 CB | 2051. | Baran, von Reuss, et al., 2007 | 30. m/0.32 mm/0.25 μm, N2, 4. K/min; Tstart: 60. C; Tend: 300. C |
| Capillary | SPB-1 | 2026. | Pinto, Salgueiro, et al., 2007 | 30. m/0.2 mm/0.2 μm, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C |
| Capillary | HP-5MS | 2057. | Vichi, Riu-Aumatell, et al., 2007 | 30. m/0.25 mm/0.25 μm, He, 40. C @ 5. min, 3. K/min, 250. C @ 10. min |
| Capillary | HP-5MS | 2027. | Pitarokili, Tzakou, et al., 2006 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5MS | 2057. | Petrakis, Roussis, et al., 2005 | 3. K/min; Column length: 30. m; Column diameter: 0.2 mm; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5 MS | 2057. | Urdampilleta, Amat, et al., 2005 | 30. m/0.25 mm/0.25 μm, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-1 | 2027. | Velasco-Negueruela, Pérez-Alonso, et al., 2005 | 50. m/0.25 mm/0.25 μm, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | RTX-5Sil | 2068. | Dudai, Larkov, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 4. K/min, 200. C @ 10. min; Tstart: 70. C |
| Capillary | HP-5 | 2052. | Pitarokili, Tzakou, et al., 2003 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 280. C |
| Capillary | HP-5 | 2050. | Velickovic, Randjelovic, et al., 2003 | 25. m/0.32 mm/0.53 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C |
| Capillary | HP-5 | 2057. | Velickovic, Randjelovic, et al., 2003 | 25. m/0.32 mm/0.53 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C |
| Capillary | HP-5 | 2048. | Velickovic, Ristic, et al., 2003 | 25. m/0.32 mm/0.53 μm, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C |
| Capillary | HP-5 | 2057. | Velickovic, Ristic, et al., 2003 | 25. m/0.32 mm/0.53 μm, Helium, 4. K/min; Tstart: 40. C; Tend: 280. C |
| Capillary | DB-5 | 2070. | Krauze-Baranowska, Mardarowicz, et al., 2002 | 30. m/0.25 mm/0.25 μm, He, 35. C @ 2. min, 3. K/min, 280. C @ 15. min |
| Capillary | HP-5 | 2056. | Velickovic, Randjelovic, et al., 2002 | 30. m/0.25 mm/0.25 μm, H2, 4. K/min; Tstart: 40. C; Tend: 280. C |
| Capillary | DB-5 | 2063. | Santos-Gomes and Fernandes-Ferreira, 2001 | 30. m/0.25 mm/0.25 μm, H2, 3. K/min; Tstart: 60. C; Tend: 285. C |
| Capillary | DB-5 | 2065. | Zoghbi, Andrade, et al., 1999 | 30. m/0.25 mm/0.25 μm, He, 3. K/min; Tstart: 60. C; Tend: 240. C |
| Capillary | DB-1 | 2042. | Perry, Baxter, et al., 1986 | 10. m/0.25 mm/0.25 μm, H2, 5. K/min; Tstart: 50. C; Tend: 250. C |
Normal alkane RI, non-polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | TR-5 MS | 2047. | Kurashov, Mitrukova, et al., 2014 | 15. m/0.25 mm/0.25 μm, Helium; Program: 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min) |
| Capillary | TR-5 MS | 2067. | Kurashov, Krylova, et al., 2013 | 15. m/0.25 mm/0.25 μm, Helium; Program: 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 mion) 15 0C/min -> 240 0C (10 min) |
| Capillary | HP-5 | 2057. | Velickovic, Ristic, et al., 2012 | 25. m/0.32 mm/0.52 μm, Hydrogen; Program: not specified |
| Capillary | DB-5 | 2056. | Yusuf and Bewaji, 2011 | Helium; Column length: 30. m; Column diameter: 0.32 mm; Program: not specified |
| Capillary | HP-5 | 2063. | Vichi, Aumatell, et al., 2008 | 30. m/0.25 mm/0.25 μm, Helium; Program: 130 0C 5 0C/min -> 240 0C 15 0C/min -> 320 0C (10 min) |
| Capillary | HP-5MS | 2052. | Deng, Xu, et al., 2006 | 30. m/0.25 mm/0.25 μm, He; Program: 50C(2min) => 6C/min => 200C => 10C/min => 270C(10min) |
| Capillary | CP Sil 8 CB | 2056. | Mockute, Nivinskiene, et al., 2003 | 50. m/0.32 mm/0.25 μm, He; Program: 60C(1min) => 5C/min => 160C => 10C/min => 250C(5min) |
| Capillary | DB-5 | 2053. | Pichette, Garneau, et al., 1998 | Column length: 30. m; Column diameter: 0.25 mm; Program: 60 0C (2 min) 2 0C/min -> 140 0C 1 0C/min -> 190 0C 2 0C/min -> 210 0C (28 min) |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Adams, González Elizondo, et al., 2006
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Systematics of smooth leaf margin Juniperus of the western hemisphere based on leaf essential oils and RAPD DNA fingerprinting,
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Baran, von Reuss, et al., 2007
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Composition of the essential oil of Abies koreana Wils.,
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Pinto, Salgueiro, et al., 2007
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Vichi, Riu-Aumatell, et al., 2007
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Pitarokili, Tzakou, et al., 2006
Pitarokili, D.; Tzakou, O.; Loukis, A.,
Essential oil composition of Salvia verticillata, S. verbenaca, S. glutinosa and S. candidissima growing wild in Greece,
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Petrakis, Roussis, et al., 2005
Petrakis, P.V.; Roussis, V.; Papadimitriou, D.; Vagias, C.; Tsitsimpikou, C.,
The effect of terpenoid extracts from 15 pine species on the feeding behavioural sequence of the late instars of the pine processionary caterpillar Thaumetopoea pityocampa,
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Urdampilleta, Amat, et al., 2005
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Biosystematic and chemosystematic studies in five South Americal species of Conyza (Asteraceae),
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Velasco-Negueruela, Pérez-Alonso, et al., 2005
Velasco-Negueruela, A.; Pérez-Alonso, M.J.; Palá-Paúl, J.; Iñigo, A.; López, G.,
The volatile oil composition of the berries of Juniperus macrocarpa Sibth. and Sm., gathered in Spain,
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. [all data]
Notes
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