Terpinen-4-ol


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-1RTX-1RTX-1
Column length (m) 30.60.30.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 300.250.240.230.230.
Heat rate (K/min) 4.3.3.2.2.
Initial hold (min) 3.1.   
Final hold (min) 15.20. 5.5.
I 1176.1176.1162.1164.1164.
ReferenceBertuzzi, Tirillini, et al., 2013Sardashti, Valizadeh, et al., 2013Alizadeh and Shaabani, 2012Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Mega-5Optima-5 MSHP-5 MSHP-5HP-5
Column length (m) 25.30.30.25.25.
Carrier gas HeliumHeliumHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.520.52
Tstart (C) 50.35.40.40.40.
Tend (C) 220.250.250.280.280.
Heat rate (K/min) 3.10.3.4.4.
Initial hold (min) 1.3.1.  
Final hold (min) 5.5.3.10.10.
I 1177.1183.1179.1174.1174.
ReferenceDell'Agli, Sanna, et al., 2012Goeminne, Vandendriessche, et al., 2012Jian-Yu, Zhu, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1HP-5 MSHP-1CP-Sil 5 CB
Column length (m) 25.60.30.30.25.
Carrier gas HydrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.220.250.250.25
Phase thickness (μm) 0.520.250.250.250.15
Tstart (C) 40.60.50.60.50.
Tend (C) 280.230.250.240.220.
Heat rate (K/min) 4.2.7.3. 
Initial hold (min)   1.  
Final hold (min) 10.45.5.  
I 1174.1157.1177.1143.1175.
ReferenceVelickovic, Ristic, et al., 2012Yapi, Boti, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011Ameen, Usman, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5 MSDB-1HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.40.50.
Tend (C) 240.250.270.210.180.
Heat rate (K/min) 3.3.3.5.2.
Initial hold (min)  5.   
Final hold (min)  20.   
I 1177.1181.1192.1186.1171.
ReferenceBertoli, Lepnardi, et al., 2011Cao, Li, et al., 2011Cui, Yang, et al., 2011Fathi, Sahari, et al., 2011Hammami, Kamoun, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5VF-5 MSVF-5 MSSE-30 MSCP-Sil 5 CB
Column length (m) 30.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 60.30.30.50.45.
Tend (C) 240.260.260.250.280.
Heat rate (K/min) 3.2.2.5.3.
Initial hold (min)    5. 
Final hold (min)  28.28.10.22.
I 1177.1182.1184.1178.1166.
ReferenceKarimi, Farmani, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011Menichini, Tundis, et al., 2011Mothana, Hasson, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methylsiloxane + 5 % Ph-groupsZB-5ZB-5HP-5ZB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumNitrogenNitrogenHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.50.60.
Tend (C) 230.200.200.250.290.
Heat rate (K/min) 7.5.5.5.5.
Initial hold (min) 2.5.5.5. 
Final hold (min) 20. 5.5. 
I 1176.1185.1183.1177.1179.
ReferenceNadim, Malik, et al., 2011Vazques, Aimar, et al., 2011Vazquez, Demmel, et al., 2011Abderrahim, Belhamel, et al., 2010Boix, Victorio, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5 MSDB-5 MSRTX-1DB-5DB-5
Column length (m) 30.25.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.300.220.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.50.
Tend (C) 290.240.230.280.250.
Heat rate (K/min) 5.3.2.3.2.
Initial hold (min)      
Final hold (min)   30.  
I 1184.1182.1164.1172.1177.
ReferenceBoix, Victorio, et al., 2010Chalchat, Figueredo, et al., 2010Dib, Djabou, et al., 2010Georgiou, Koutsaviti, et al., 2010Ho, Wang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-1BP-1HP-5SPB-1
Column length (m) 30.25. 30.30.
Carrier gas HeliumNitrogenNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.20
Phase thickness (μm) 0.250.25 0.250.20
Tstart (C) 70.60.60.50.70.
Tend (C) 290.250.220.240.220.
Heat rate (K/min) 5.4.5.3.3.
Initial hold (min)  1.10.5. 
Final hold (min)  10.30. 15.
I 1182.1166.1166.1178.1157.
ReferenceLazarevic, Radulovic, et al., 2010Mirjalili, Salehi, et al., 2010Mishra, Chaudhary, et al., 2010Monsef-Esfahani, Miri, et al., 2010Neves, Rosa, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.100.70.70.70.
Tend (C) 220.220.290.290.290.
Heat rate (K/min) 5.2.5.5.5.
Initial hold (min) 10.    
Final hold (min)   10. 10.
I 1179.1179.1182.1184.1184.
ReferenceOgunwande, Flamini, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5 MSDB-1-MSCP Sil 5 CBDB-1
Column length (m) 10.10.60.25.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.100.100.250.250.25
Phase thickness (μm) 0.100.100.250.150.25
Tstart (C) 50.50.30.50.50.
Tend (C) 250.250.200.230.220.
Heat rate (K/min) 10.10.2.3.4.
Initial hold (min)   4. 2.
Final hold (min)   35. 2.
I 1179.1182.1157.1175.1157.
ReferenceScandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010Takeoka, Hobbs, et al., 2010Usman, Zubair, et al., 2010Xu, Tang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSE-54HP-5 MSSPB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.53
Phase thickness (μm) 0.250.250.250.250.50
Tstart (C) 40.50.60.60.50.
Tend (C) 250.250.260.250.210.
Heat rate (K/min) 10.7.2.2.3.
Initial hold (min) 1.1.5.8.5.
Final hold (min) 3.5.999.15.45.
I 1177.1186.1174.1191.1203.
ReferenceYang, Zhang, et al., 2010Zouari, Zouari, et al., 2010Dayisoylu and Alma, 2009Farhat, Ginies, et al., 2009Gilani, Shah, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5HP-5MS
Column length (m) 30.30.50.30.60.
Carrier gas HeliumHeliumNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.200.250.25
Phase thickness (μm) 0.250.250.320.250.25
Tstart (C) 50.60.60.70.70.
Tend (C) 250.210.220.240.250.
Heat rate (K/min) 5.3.5.5.3.
Initial hold (min) 2. 3.  
Final hold (min)      
I 1177.1173.1177.1178.1183.
ReferenceHo, Wang, et al., 2009Jaimand, Rezaee, et al., 2009Kazemi and Akhavani, 2009Lawal and Oyedelji, 2009Males, Plazibat, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1RTX-1DB-5DB-5
Column length (m) 25.60.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.200.220.220.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.60.60.45.40.
Tend (C) 240.230.230.250.250.
Heat rate (K/min) 3.2.2.3.3.
Initial hold (min)    3.1.
Final hold (min) 7.30.30.5.10.
I 1176.1164.1164.1178.1167.
ReferenceMaridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Porto, Decorti, et al., 2009Rahmi-Nasrabadi, Gholivand, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5DB-1 MSDB-5 MSHP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeliumNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 90.40.40.40.50.
Tend (C) 225.230.250.250.240.
Heat rate (K/min) 3.2.6.4.5.
Initial hold (min)   1.2. 
Final hold (min) 3. 4.2. 
I 1179.1178.1159.1185.1178.
ReferenceRetta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009Seo, Kim, et al., 2009Su, Wang, et al., 2009Wannes, Mhamdi, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5Ultra 2HP-5
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.320.250.250.200.25
Phase thickness (μm) 0.250.250.250.110.25
Tstart (C) 40.50.50.60.60.
Tend (C) 240.280.280.230.220.
Heat rate (K/min) 4.4.9.2.5.
Initial hold (min) 4. 3.5.10.
Final hold (min)   3.30. 
I 1183.1179.1177.1182.1180.
ReferenceZhannan, Shiqiong, et al., 2009Zhao, Zeng, et al., 2009Aicha, Ines, et al., 2008Byun and Shin, 2008Flamini, Tebano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSZB-1DB-5RTX-1Elite-1
Column length (m) 30.30.60.60.30.
Carrier gas HeliumNitrogenNitrogenHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.220.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.45.60.60.60.
Tend (C) 250.230.250.230.246.
Heat rate (K/min) 3.3.5.2.3.
Initial hold (min) 2.    
Final hold (min) 10. 10.35. 
I 1181.1156.1186.1161.1176.
ReferenceLo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Mosayebi, Amin, et al., 2008Paolini, Tomi, et al., 2008Raj, Baby, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSBPX-5RTX-5HP-5
Column length (m) 30.30.7.520.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.100.180.25
Phase thickness (μm) 0.250.2510.0.200.25
Tstart (C) 60.50.60.50.60.
Tend (C) 250.240.240.280.240.
Heat rate (K/min) 2.3.3.4.4.
Initial hold (min) 8.  1.2.
Final hold (min) 15.    
I 1179.1172.1206.1179.1180.
ReferenceSahraoui, Vian, et al., 2008Sarikurkcu, Tepe, et al., 2008Shellie, 2008Skalicka-Wozniak, Los, et al., 2008Verdian-rizi, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSOV-1HP-5HP-5 MSDB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.250.320.250.32
Tstart (C) 60.65.60.50.60.
Tend (C) 270.260.250.230.220.
Heat rate (K/min) 3.6.5.3.5.
Initial hold (min)   30.10.3.
Final hold (min)    10.5.
I 1185.1182.1175.1177.1179.
ReferenceVictorio, Alviano, et al., 2008Wang, Yi, et al., 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Amiri, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5MSHP-5MSDB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.260.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.280.280.240.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min)      
Final hold (min)      
I 1168.1167.1168.1177.1176.
ReferenceBaran, von Reuss, et al., 2007Basta, Pavlovic, et al., 2007Basta, Tzakou, et al., 2007Bos, Woerdenbag, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5DB-5HP-5
Column length (m) 30.30.60.30.30.
Carrier gas HeliumN2HeHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.260.25
Phase thickness (μm) 0.250.250.250.250.26
Tstart (C) 60.50.40.60.60.
Tend (C) 280.240.220.290.240.
Heat rate (K/min) 4.5.3.3.4.
Initial hold (min) 5.1.  2.
Final hold (min)  4.  20.
I 1174.1177.1192.1177.1178.
ReferenceCapetanos, Saroglou, et al., 2007Cheraif, Ben Jannet, et al., 2007Chyau, Tsai, et al., 2007Elfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSZP-5DB-1Col-Elite 5MS
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeNitrogenHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.60.30.
Tend (C) 250.250.260.250.246.
Heat rate (K/min) 2.2.6.4.3.
Initial hold (min) 8.8.7.1. 
Final hold (min) 15.15.1.10. 
I 1191.1170.1191.1168.1177.
ReferenceFerhat, Meklati, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Füssel, Dötterl, et al., 2007Ghasempour, Shirinpour, et al., 2007Gudaityte and Venskutonis R.P., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DBP-5RTX-5 MSBP-1DB-5
Column length (m) 30.25.30. 30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (μm) 0.250.220.25 0.25
Tstart (C) 60.40.45.60.60.
Tend (C) 240.250.210.220.300.
Heat rate (K/min) 2.3.3.5.3.
Initial hold (min)  1.   
Final hold (min) 20.10. 6. 
I 1154.1153.1180.1166.1168.
ReferenceHachicha, Skanji, et al., 2007Heravi and Sereshti, 2007Hudaib and Aburjai, 2007Kiran, Devi, et al., 2007Limberger, Scopel, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30HP-5DB-5MSAT-5ZB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 250.250.280.260.220.
Heat rate (K/min) 5.5.3.4.4.
Initial hold (min) 5.5.  5.
Final hold (min) 10.10.30. 20.
I 1178.1175.1146.1177.1178.
ReferenceLoizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Marongiu B., Piras A., et al., 2007Meccia, Rojas, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-1HP-5 MS
Column length (m) 30.30.25.50.25.
Carrier gas HeliumHeliumH2HeHelium
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 50.60.60.95.100.
Tend (C) 260.300.240.240.280.
Heat rate (K/min) 2.53.3.4.4.
Initial hold (min) 1.   3.
Final hold (min) 20.   5.
I 1154.1147.1180.1175.1186.
ReferenceMonser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Oliveira, Leitão, et al., 2007Pala-Paul, Brophy, et al., 2007Phutdhawong, Kawaree, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-5BPX-5DB-1HP-5 MS
Column length (m) 30.30.50.60.60.
Carrier gas HeHeHeNitrogenHydrogen
Substrate      
Column diameter (mm) 0.20.250.220.250.25
Phase thickness (μm) 0.20.251.0.250.25
Tstart (C) 70.50.50.60.60.
Tend (C) 220.250.300.250.260.
Heat rate (K/min) 3.2.4.4.4.
Initial hold (min)   1.1. 
Final hold (min) 15. 10.10.20.
I 1159.1176.1212.1168.1178.
ReferencePinto, Salgueiro, et al., 2007Raal, Orav, et al., 2007Rali, Wossa, et al., 2007Reza, Ebrahim, et al., 2007Rojas, Velasco, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5DBP-5DB-5
Column length (m) 60.60.30.25.30.
Carrier gas  HeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.220.25
Tstart (C) 60.60.50.40.60.
Tend (C) 250.250.240.250.320.
Heat rate (K/min) 5.5.4.3.10.
Initial hold (min)    1. 
Final hold (min)    10.4.
I 1162.1166.1175.1153.1187.
ReferenceSalehi, Asghari, et al., 2007Salehi, Fakhari, et al., 2007Sefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007Smelcerovic, Spiteller, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas   HeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25  0.25
Tstart (C) 40.40.60.60.60.
Tend (C) 210.250.200.200.280.
Heat rate (K/min) 2.2.2.2.3.
Initial hold (min)      
Final hold (min) 33.33.20.20. 
I 1176.1176.1166.1177.1140.
ReferenceSylvestre, Longtin, et al., 2007Sylvestre, Pichette, et al., 2007Tiwary, Nail, et al., 2007Tiwary, Nail, et al., 2007Tzakou, Bazos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.32
Tstart (C) 60.40.40.40.60.
Tend (C) 280.250.240.250.250.
Heat rate (K/min) 3.3.5.4.5.
Initial hold (min)  5.3.2.30.
Final hold (min)  10.10.5. 
I 1177.1175.1174.1178.1175.
ReferenceVagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Wenguang, Wenlai, et al., 2007Xu, Fan, et al., 2007Yassa and Akhani, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5DB-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.50.50.40.
Tend (C) 260.280.280.265.300.
Heat rate (K/min) 4.9.9.2.52.
Initial hold (min)  3.3.1. 
Final hold (min)  3.3.20. 
I 1175.31177.1178.1184.1191.
ReferenceZizovic, Stamenic, et al., 2007Abdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Bazargani, Almasirad, et al., 2006Biondi, Sari, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-5BP-1HP-5MSHP-1SPB-1
Column length (m) 60.50.30.50.30.
Carrier gas He HeHeHelium
Substrate      
Column diameter (mm) 0.250.220.250.20.20
Phase thickness (μm) 0.250.250.250.50.20
Tstart (C) 60.60.60.60.70.
Tend (C) 200.220.280.250.220.
Heat rate (K/min) 4.2.3.2.3.
Initial hold (min)      
Final hold (min) 20.20. 120.15.
I 1177.1162.1177.1164.1158.
ReferenceBorges, Rojas, et al., 2006Boti, Yao, et al., 2006Bozin, Mimicá-Dukic, et al., 2006Castel, Fernandez, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5DB-5HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas NitrogenN2He  
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 40.70.60.60.60.
Tend (C) 200.230.246.230.280.
Heat rate (K/min) 2.2.3.3.4.
Initial hold (min) 1.2.   
Final hold (min) 9.20. 15. 
I 1158.1176.1177.1177.1180.
ReferenceChen, Sheu, et al., 2006Choi, 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Damjanovic, Skala, et al., 2006Ebrahim Sajjadi and Mehregan, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1BP-1HP-5MSHP-5
Column length (m) 30.50.50.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.260.220.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.50.
Tend (C) 290.220.220.250.300.
Heat rate (K/min) 3.2.2.2.5.
Initial hold (min)     5.
Final hold (min)  20.20. 5.
I 1177.1161.1161.1177.1184.
ReferenceElfami, Komar, et al., 2006Fanciullino, Tomi, et al., 2006Fanciullino, Tomi, et al., 2006Farah, Afifi, et al., 2006Figuérédo, Cabassu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-5DB-1DB-5
Column length (m) 50.30.30.60.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 250.240.240.250.250.
Heat rate (K/min) 2.5.5.5.3.
Initial hold (min)  2.2.  
Final hold (min) 40.  10.10.
I 1162.1177.1177.1166.1177.
ReferenceFilippi, Lanfranchi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Hadian, Sonboli, et al., 2006Havlik, Kokoska, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5BP-1Methyl SiliconeRTX-1
Column length (m) 30.30. 25.30.
Carrier gas  HeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 40.60.60.90.60.
Tend (C) 220.240.220.220.300.
Heat rate (K/min) 3.4.5.7.4.
Initial hold (min)    2. 
Final hold (min) 3. 6.  
I 1177.1177.1166.1176.1161.
ReferenceHymete, Rohloff, et al., 2006Ibañez and Usubillaga, 2006Kiran, Bhavani, et al., 2006Kitchlu, Bakshi, et al., 2006Kula, Izydorczyk, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1CP Sil 5 CBHP-5 MSHP-5
Column length (m) 60.60.30.30.30.
Carrier gas   N2NitrogenN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.52
Tstart (C) 70.70.50.50.50.
Tend (C) 230.230.200.280.280.
Heat rate (K/min) 2.2.5.5.5.
Initial hold (min) 2.2.   
Final hold (min) 20.20. 5.5.
I 1162.1162.1167.1179.1179.
ReferenceLan Phi N.T., Nishiyama C., et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Martin, Joseph, et al., 2006Marzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5CP-Sil 5 CB
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeHeHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.15
Tstart (C) 60.60.60.50.50.
Tend (C) 220.260.220.250.230.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)  4.5.5. 
Final hold (min)      
I 1179.1179.1180.1180.1165.
ReferenceMorteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani, Saeedi, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Navaei and Mirza, 2006Olawore, Usman, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5SE-52DB-5DB-1
Column length (m) 30.25.50.30.50.
Carrier gas HeN2HeliumHeN2
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (μm) 0.250.15 0.250.25
Tstart (C) 50.50.50.60.95.
Tend (C) 250.200.240.280.240.
Heat rate (K/min) 2.4.3.5.4.
Initial hold (min)  3. 0.5 
Final hold (min)    2. 
I 1166.1185.1180.1179.1171.
ReferenceOrav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Ozcan, Chalchat, et al., 2006Ozel, Gogus, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5SPB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeliumHydrogenHydrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.70.70.
Tend (C) 260.220.250.280.280.
Heat rate (K/min) 4.5.4.4.4.
Initial hold (min)  10.2.4.4.
Final hold (min)   20.  
I 1180.1177.1177.1177.1177.
ReferencePetrovic, Ristic, et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marquez, et al., 2006Pino, Marbot, et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HydrogenHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.60.50.60.60.
Tend (C) 280.280.250.200.260.
Heat rate (K/min) 4.3.10.2.5.
Initial hold (min) 4. 5.  
Final hold (min)    60. 
I 1177.1142.1179.1179.1182.
ReferencePino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Robinson, 2006Rout, Naik, et al., 2006Sabulal, Dan, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSZB-5DB-1DB-5DB-1
Column length (m) 30.30.60.30.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.40.70.40.40.
Tend (C) 280.300.230.240.250.
Heat rate (K/min) 4.2.2.4.4.
Initial hold (min)   2.  
Final hold (min)   20.  
I 1180.1191.1164.1177.1157.
ReferenceSajjadi, 2006Sari M., Biondi D.M., et al., 2006Sawamura, Onishi, et al., 2006Sefidkon and Jamzad, 2006Sefidkon, Jamzad, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5DB-1SPB-5
Column length (m) 30.30.25.60. 
Carrier gas HeHeN2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.20.25 
Phase thickness (μm) 0.250.250.330.25 
Tstart (C) 40.60.30.60.50.
Tend (C) 260.280.280.250.250.
Heat rate (K/min) 2.3.3.5.5.
Initial hold (min) 5.5.  3.
Final hold (min) 20.  10.15.
I 1175.1177.1184.1165.1177.
ReferenceSenatore, Landolfi, et al., 2006Setzer, Noletto, et al., 2006Shafi, Jose, et al., 2006Sonboli, Mirjalili, et al., 2006Stojanovic, Palic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1HP-5SPB-1
Column length (m) 30.30.50.30.50.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.60.90.60.50.
Tend (C) 230.240.240.250.220.
Heat rate (K/min) 3.4.4.10.4.
Initial hold (min) 3.  2.1.
Final hold (min) 10.  10.10.
I 1175.1179.1157.1186.1158.
ReferenceTohar, Mohd, et al., 2006Trilles, Bombarda, et al., 2006Velasco-Negueruela, Pérez-Alonso, et al., 2006Wang, Yang, et al., 2006Wong, Lim, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5SE-30DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 50.40.90.60.60.
Tend (C) 250.250.220.210.280.
Heat rate (K/min) 4.4.7.3.3.
Initial hold (min) 1. 2.5. 
Final hold (min) 10.    
I 1152.1169.1160.1175.1165.
ReferenceWong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Ahuja, Bakshi, et al., 2005Askari and Sefidkon, 2005Basta, Tzakou, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-1DB-5Methyl Silicone
Column length (m) 50.30.25.50.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.20.2490.250.30.3
Phase thickness (μm) 0.50.250.250.25 
Tstart (C) 60.60.50.60.50.
Tend (C) 250.290.250.240.240.
Heat rate (K/min) 2.3.3.2.3.
Initial hold (min)   3.  
Final hold (min) 60.    
I 1163.1177.1170.1179.1175.
ReferenceBendimerad and Bendiab, 2005Bos, Stojanova, et al., 2005Cégiéla-Carlioz, Bessière, et al., 2005Chagonda and Chalchat, 2005Chalchat and Özcan, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-1HP-5HP-5
Column length (m) 25.60.50.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.20.250.20.250.25
Phase thickness (μm) 0.330.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 240.250.250.30.300.
Heat rate (K/min) 3.5.2.4.5.
Initial hold (min)   60.3.5.
Final hold (min) 7.  15.5.
I 1174.1169.1160.1177.1184.
ReferenceDuarte, Figueira, et al., 2005Fakhari, Salehi, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Ferretti, Maggi, et al., 2005Figuérédo, Cabassu, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRSL-200HP-5DB-1DB-5
Column length (m) 25.30.25.30.30.
Carrier gas He H2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm)  0.250.520.25 
Tstart (C) 50.40.40.50.60.
Tend (C) 250.280.240.265.240.
Heat rate (K/min) 3.6.4.2.53.
Initial hold (min) 3.2. 1. 
Final hold (min) 10.10. 30. 
I 1179.1177.1175.1153.1173.
ReferenceGhasemi Y., Faridi P., et al., 2005Jirovetz, Buchbauer, et al., 2005Jovanovic, Kitic, et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Khayyat and Karimi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5DB-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 60.60.30.60.60.
Tend (C) 240.240.260.230.220.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)   2. 5.
Final hold (min)   28.  
I 1175.1180.1178.11171.1177.
ReferenceKhayyat and Karimi, 2005Khayyat and Karimi, 2005Leffingwell and Alford, 2005Limberger, Sobral, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBDB-5HP-5DB-5
Column length (m) 30.25.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.15 0.250.25
Tstart (C) 60.50.40.70.40.
Tend (C) 220.230.220.240.250.
Heat rate (K/min) 4.3.4.5.5.
Initial hold (min) 4. 1. 0.5
Final hold (min)     2.
I 1179.1165.1172.1179.1179.
ReferenceMorteza-Semnani and Saeedi, 2005Ogunwande, Olawore, et al., 2005de Oliveira, Dias, et al., 2005Oyedeji, Yani, et al., 2005Özel, Gögüs, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSHP-5MSHP-5MSDB-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.25 0.320.25 
Tstart (C) 50.60.60.60.60.
Tend (C) 280.280.250.200.240.
Heat rate (K/min) 8.3.5.2.5.
Initial hold (min) 2. 3.  
Final hold (min) 2.  80. 
I 1185.1177.1164.1183.1177.
ReferencePellati, Benvenuti, et al., 2005Petrakis, Roussis, et al., 2005Pourmortazavi, Ghadiri, et al., 2005Rout, Misra, et al., 2005Saeidnia, Gohari, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSDB-5DB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.275.280.220.250.
Heat rate (K/min) 4.4.4.3.5.
Initial hold (min)    4. 
Final hold (min)     10.
I 1178.1182.1175.1175.1171.
ReferenceSajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Salehi, Sefidkon, et al., 2005Salehi, Sonboli, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5HP-5MSDB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 265.240.260.280.240.
Heat rate (K/min) 2.54.2.3.3.
Initial hold (min) 1. 5.5. 
Final hold (min) 20. 20.  
I 1153.1177.1175.1174.1177.
ReferenceSarkhail, Amin, et al., 2005Sefidkon and Jamzad, 2005Senatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005da Silva, Andrade, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5PE-5DB-5HP-5MSRTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 300.230.230.280.250.
Heat rate (K/min) 3.5.3.3.5.
Initial hold (min)  2.   
Final hold (min)  4.20. 10.
I 1171.1168.1177.1183.1168.
ReferenceSimoes-Pires C.A., Debenedetti S., et al., 2005Singh, Raina, et al., 2005Skoula and Grayer, 2005Slavkovska, Couladis, et al., 2005Sonboli A., Fakhari A.R., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5MSHP-5 MSHP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.500.25
Tstart (C) 60.40.50.60.60.
Tend (C) 250.210.240.260.280.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)  2.3.  
Final hold (min) 10.33. 20. 
I 1165.1179.1207.1177.1140.
ReferenceSonboli, Salehi, et al., 2005Stevanovic, Garneau, et al., 2005Tepe B., Sokmen M., et al., 2005Topçu, Barla, et al., 2005Tzakou, Bazos, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1HP-5MSSPB-1
Column length (m) 30.30.50.30.50.
Carrier gas HeHelium  He
Substrate      
Column diameter (mm) 0.320.320.250.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.40.60.40.50.
Tend (C) 280.300.240.220.220.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)    5.3.
Final hold (min)  5. 10.30.
I 1150.1177.1152.1175.1166.
ReferenceTzakou and Constantinidis, 2005Utsunomia, Kawata, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005Vichi, Riu-Aumatell, et al., 2005Wong, Lee, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5CP Sil 5 CBDB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumN2He 
Substrate      
Column diameter (mm) 0.320.320.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.50.90.60.
Tend (C) 250.250.200.220.220.
Heat rate (K/min) 5.5.5.7.2.
Initial hold (min) 2.2. 2. 
Final hold (min) 5.5. 5.20.
I 1175.1175.1169.1161.1161.
ReferenceN/AN/AAgnaniet, Menut, et al., 2004Agnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5HP-5 MSHP-5MSDB-1
Column length (m) 60.60.30.30.25.
Carrier gas N2HeHeliumHe 
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.251.0.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 230.200.275.275.180.
Heat rate (K/min) 2.4.4.4.3.
Initial hold (min) 2.   10.
Final hold (min) 20.30.  10.
I 1175.1183.1179.1171.1178.
ReferenceChoi, 2004Gauvin, Ravaomanarivo, et al., 2004Ghannadi, Sajjadi, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004bin Jantan, Ayop, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5DB-5RTX-1SE-54
Column length (m) 25.60.60.30.30.
Carrier gas NitrogenHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.40.60.60.
Tend (C) 240.260.280.300.260.
Heat rate (K/min) 3.6.4.4.2.
Initial hold (min)  4.64. 5.
Final hold (min)  1.   
I 1177.1193.1175.1168.1175.
ReferenceJAvidnia, Mojab, et al., 2004Jürgens and Dötterl, 2004Kalvandi, Sefidkon, et al., 2004Kalemba and Thiem, 2004Kilic, Hafizoglu, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSDB-5RTX-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 230.240.300.300.280.
Heat rate (K/min) 5.3.3.4.3.
Initial hold (min) 2.    
Final hold (min) 10.    
I 1143.1178.1172.1161.1176.
ReferenceLi and Jiang, 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004Lis, Boczek, et al., 2004Malencic, Couladis, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5MSHP-5MSDB-5DB-5
Column length (m) 25.30.30.30.50.
Carrier gas N2HeHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25  
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.275.240.240.
Heat rate (K/min) 5.3.4.2.2.
Initial hold (min)      
Final hold (min)  30. 999.999.
I 1167.1143.1181.1176.1176.
ReferenceMallavarapu, Kulkarni, et al., 2004Marongiu, Piras, et al., 2004Mehrabani, Asadipour, et al., 2004Miyazawa, Fuhita, et al., 2004Miyazawa, Fujita, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30NB-30DB-1DB-1DB-1
Column length (m) 50.50.50.60.60.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.20.20.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.95.35.35.
Tend (C) 250.250.240.230.230.
Heat rate (K/min) 2.2.4.2.2.
Initial hold (min)    4.4.
Final hold (min)    25.25.
I 1166.1166.1159.1154.1156.
ReferenceOrav, Stulova, et al., 2004Orav, Stulova, et al., 2004Palá-Paúl, Velasco-Negueruela, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1NB-30NB-30DB-5
Column length (m) 60.60.50.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.20.200.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.35.50.50.35.
Tend (C) 230.230.250.250.220.
Heat rate (K/min) 2.2.2.2.2.5
Initial hold (min) 4.4.   
Final hold (min) 25.25.  6.
I 1156.1159.1166.1165.1177.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Raal, Arak, et al., 2004Raal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeHP-5 MSHP-5MSHP-5MSDB-1
Column length (m) 60.30.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 200.200.280.280.265.
Heat rate (K/min) 4.4.4.4.2.5
Initial hold (min) 1.1.  1.
Final hold (min) 20.20.  20.
I 1170.1170.1174.1177.1153.
ReferenceRojas, Usubillaga, et al., 2004Royas, Usubillaga, et al., 2004Sadeghpour, Asghari, et al., 2004Sajjadi and Shahpiri, 2004Sarkhail, Amin, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5DB-1HP-1
Column length (m) 60.60.30.60.30.
Carrier gas  Nitrogen HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 70.70.50.40.40.
Tend (C) 230.230.250.280.260.
Heat rate (K/min) 2.2.3.4.2.
Initial hold (min) 2.2.5.5.5.
Final hold (min) 20.   20.
I 1175.1175.1177.1160.1146.
ReferenceSawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Sefidkon, Jamzad, et al., 2004Sefidkon and Shaabani, 2004Senatore, Napolitano, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5BPX-5CP Sil 8 CB
Column length (m) 25.25.30.25.30.
Carrier gas N2H2HeHe 
Substrate      
Column diameter (mm) 0.20.320.250.220.32
Phase thickness (μm) 0.50.520.251.0.25
Tstart (C) 30.40.60.60.50.
Tend (C) 280.240.240.250.200.
Heat rate (K/min) 3.4.3.3.5.
Initial hold (min)    5.5.
Final hold (min)    10. 
I 1184.1177.1175.1203.1186.
ReferenceShafi, Nambiar, et al., 2004Simic, Sokovic, et al., 2004Tellez, Khan, et al., 2004Vilaseca, Guy, et al., 2004Wang, Guo, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HTHP-5MSHP-5DB-5
Column length (m) 30.27.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.2490.250.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 300.250.275.220.240.
Heat rate (K/min) 3.2.4.5.4.
Initial hold (min)  2. 10. 
Final hold (min)  20.   
I 1172.1160.1177.1168.1166.
ReferenceWoerdenbag, Windono, et al., 2004Yusufoglu, Celik, et al., 2004Afsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Cabanillas, Lopez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-1RTX-5SilDB-5
Column length (m) 60.30.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 70.60.50.70.50.
Tend (C) 230.280.250.200.220.
Heat rate (K/min) 2.3.4.4.3.
Initial hold (min) 2.    
Final hold (min) 20.  10. 
I 1176.1172.1158.1183.1189.
ReferenceChoi, 2003Couladis, Özcan, et al., 2003Dabiri and Sefidkon, 2003Dudai, Larkov, et al., 2003Edris and Farrag, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-1DB-1HP-5MS
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.60.70.50.60.
Tend (C) 200.220.200.200.275.
Heat rate (K/min) 3.5.10.5.4.
Initial hold (min)  20.   
Final hold (min)  20.   
I 1189.1182.1169.1161.1176.
ReferenceEdris, Shalaby, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghannadi, Aghazari, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSRSL-200RSL-200DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeHeH2H2He
Substrate      
Column diameter (mm) 0.250.250.320.320.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.50.
Tend (C) 280.275.280.280.220.
Heat rate (K/min) 4.4.6.6.3.
Initial hold (min)   5.5.2.
Final hold (min)   5.5.10.
I 1177.1178.1169.1175.1174.
ReferenceGhasemi, Asghari, et al., 2003Hajhashemi, Ghannadi, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2Juteau, Jerkovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30CP Sil 5 CBSPB-5DB-5DB-5MS
Column length (m) 12.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.320.250.25
Phase thickness (μm) 0.30.250.250.250.25
Tstart (C) 70.35.40.60.60.
Tend (C) 220.280.220.240.240.
Heat rate (K/min) 3.5.5.3.3.
Initial hold (min)  2.51.  
Final hold (min)   20.  
I 1161.1158.1188.1178.1179.
ReferenceKambouche and El-Abed, 2003Kanjilal, Kotoky, et al., 2003Ledauphin, Guichard, et al., 2003Machado, Zoghbi, et al., 2003Maia, Taveira, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5ZB-1HP-5DB-1
Column length (m) 30.50.30.30.50.
Carrier gas HeHeN2HeliumN2
Substrate      
Column diameter (mm) 0.250.20.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.50.45.70.95.
Tend (C) 280.220.230.210.240.
Heat rate (K/min) 3.3.3.2.4.
Initial hold (min)  2.   
Final hold (min) 30.  60. 
I 1168.1180.1156.1177.1171.
ReferenceMarongiu, Porcedda, et al., 2003Masotti, Juteau, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mookdasanit, Tamura, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1DB-1HP-5
Column length (m) 30.30.60.60.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.40.40.60.
Tend (C) 280.280.220.220.280.
Heat rate (K/min) 4.3.4.4.4.
Initial hold (min) 10.    
Final hold (min) 40.    
I 1177.1162.1163.1164.1178.
ReferencePino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Rasooli and Mirmostafa, 2003Rasooli and Mirmostafa, 2003Sajjadi and Mehregan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5CP Sil 5 CBDB-1
Column length (m) 60.30.60.25.60.
Carrier gas HeHe  N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.150.25
Tstart (C) 50.60.40.50.70.
Tend (C) 280.240.250.230.230.
Heat rate (K/min) 4.3.5.3.2.
Initial hold (min)   15. 2.
Final hold (min)     20.
I 1167.1180.1177.1172.1173.
ReferenceShahmir, Ahmadi, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003Taiwo and Bolanle, 2003Tu, Onishi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1Cross-Linked MethylsiliconeHP-5HP-5
Column length (m) 50.50.25.25.25.
Carrier gas HeN2HeH2H2
Substrate      
Column diameter (mm) 0.20.250.20.320.32
Phase thickness (μm) 0.50.250.330.530.53
Tstart (C) 60.90.70.40.40.
Tend (C) 220.240.250.280.280.
Heat rate (K/min) 2.4.4.4.4.
Initial hold (min)      
Final hold (min) 40.    
I 1157.1141.1157.1177.1177.
ReferenceValette, Fernandez, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003, 2Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 25.25.25.30.30.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.530.530.530.320.25
Tstart (C) 40.40.40.60.60.
Tend (C) 280.280.280.250.240.
Heat rate (K/min) 4.4.4.5.3.
Initial hold (min)    30. 
Final hold (min)      
I 1174.1174.1177.1180.1180.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Yassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5HP-1
Column length (m) 25.30.25.30.30.
Carrier gas N2He HeHe
Substrate      
Column diameter (mm) 0.250.2490.320.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 50.60.50.60.70.
Tend (C) 250.300.200.280.220.
Heat rate (K/min) 4.3.5.3.3.
Initial hold (min)      
Final hold (min) 10.5. 30.15.
I 1178.1177.1169.1168.1158.
ReferenceZrira, Elamrani, et al., 2003Bos, Koulman, et al., 2002Boyom, Keumedjio, et al., 2002Caredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5MSDB-5MSBP-1DB-5
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.500.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 75.60.60.60.50.
Tend (C) 200.280.280.220.250.
Heat rate (K/min) 3.3.3.5.4.
Initial hold (min) 4.    
Final hold (min) 8.  10. 
I 1177.1177.1177.1166.1177.
ReferenceCicció and Gómez-Laurito, 2002Congiu, Falconieri, et al., 2002Congiu, Falconieri, et al., 2002Das, Ram, et al., 2002Farah, Fechtal, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5PTE-5SE-30
Column length (m) 30.30.30.60.50.
Carrier gas N2HeHeH2He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.300.25
Tstart (C) 50.60.60.60.70.
Tend (C) 250.240.275.285.240.
Heat rate (K/min) 4.3.4.4.34.
Initial hold (min) 5.    
Final hold (min)      
I 1178.1180.1174.1177.1173.
ReferenceFarah, Fechtal. M., et al., 2002Flamini, Ertugrul, et al., 2002Ghannadi, Sajjadi, et al., 2002Gudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RSL-200CP Sil 8 CBDB-1SPB-5
Column length (m) 30.30.30.25.60.
Carrier gas H2H2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.230.25
Phase thickness (μm) 0.250.250.250.200.25
Tstart (C) 40.50.50.50.50.
Tend (C) 280.280.220.200.240.
Heat rate (K/min) 6.6.3.3.5.
Initial hold (min) 5.5.2.3.3.
Final hold (min) 5.5. 30.10.
I 1173.1172.1178.1181.1191.
ReferenceJirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002Juteau, Masotti, et al., 2002Khallouki, Younos, et al., 2002Kim and Lee, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 60.35.50.60.40.
Tend (C) 240.280.200.250.290.
Heat rate (K/min) 3.3.5.3.7.
Initial hold (min)  2.   
Final hold (min)  15.   
I 1176.1181.1170.1171.1184.
ReferenceKobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Kuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002Lin, Rouseff, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5DB-5DB-5MS
Column length (m) 30.30.25.30.30.
Carrier gas He N2HeHe
Substrate      
Column diameter (mm) 0.320.250.230.250.25
Phase thickness (μm) 0.250.250.150.250.25
Tstart (C) 40.60.50.60.60.
Tend (C) 290.275.250.240.240.
Heat rate (K/min) 7.4.3.3.3.
Initial hold (min)  4.   
Final hold (min)      
I 1177.1170.1174.1179.1177.
ReferenceLin, Rouseff, et al., 2002Lockwood, Asghari, et al., 2002Mahmout, Bessière, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5OV-101SPB-5DB-5
Column length (m) 30.30.50.30.30.
Carrier gas   HeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (μm) 0.250.250.50.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 240.240.250.250.300.
Heat rate (K/min) 3.3.2.4.2.
Initial hold (min)    2. 
Final hold (min)    20. 
I 1179.1183.1160.1177.1175.
ReferenceNovak, Langbehn, et al., 2002Novak, Langbehn, et al., 2002Orav, Kailas, et al., 2002Pino, Marbot, et al., 2002Ruberto, Biondi, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1DB-1DB-1
Column length (m) 25.60.60.60.50.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 60.40.40.40.60.
Tend (C) 220.250.280.280.240.
Heat rate (K/min) 3.4.4.4.3.
Initial hold (min)   5.5. 
Final hold (min)      
I 1173.1155.1159.1158.1152.
ReferenceSchwob, Bessière, et al., 2002Sefidkon, Dabiri, et al., 2002Sefidkon, Jalili, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5MSDB-5HP-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas H2HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 280.270.240.220.240.
Heat rate (K/min) 4.3.3.5.3.
Initial hold (min)    10. 
Final hold (min)      
I 1177.1175.1175.1178.1172.
ReferenceVelickovic, Randjelovic, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Campeol, Flamini, et al., 2001Cherchi, Deidda, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-1DB-1HP-5HP-5
Column length (m) 30.60.60.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.40.60.60.
Tend (C) 240.280.280.220.220.
Heat rate (K/min) 2.4.4.5.5.
Initial hold (min)  5.5.10.10.
Final hold (min)      
I 1158.31160.1162.1179.1179.
ReferenceChiasson, Bélanger, et al., 2001Dabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001Flamini, Cioni, et al., 2001Gallori, Flamini, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1RSL-200RTX-1SPB-5BP-1
Column length (m) 30.30.30.60.50.
Carrier gas N2H2N2HeliumHe
Substrate      
Column diameter (mm) 0.250.320.250.250.22
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.40.60.50.60.
Tend (C) 220.280.300.240.230.
Heat rate (K/min) 5.6.4.3.2.
Initial hold (min)  5. 3. 
Final hold (min)  5. 10.35.
I 1165.1172.1168.1190.1162.
ReferenceGupta, Mallavarapu, et al., 2001Jirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Kim and Lee, 2001Lota, de Rocca Serra, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-5MSDB-5MSDB-1OV-101
Column length (m) 25.30.30.60.50.
Carrier gas NitrogenHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 50.60.60.50.50.
Tend (C) 210.240.240.270.250.
Heat rate (K/min) 3.3.3.4.2.
Initial hold (min) 2.    
Final hold (min)  30.30.  
I 1160.1154.1154.1157.1161.
ReferenceLy, Yamauchi, et al., 2001Marongiu, Porcedda, et al., 2001Marongiu, Porcedda, et al., 2001Mirza, Ahmadi, et al., 2001Orav, Kailas, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-5DB-5DB-5
Column length (m) 50.30.30.60.30.
Carrier gas HeN2 HeH2
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (μm)  0.250.5 0.25
Tstart (C) 50.80.35.50.60.
Tend (C) 250.225.275.250.285.
Heat rate (K/min) 2.4.6.3.3.
Initial hold (min)    5. 
Final hold (min)      
I 1159.1151.1176.1177.1176.
ReferenceOrav and Kann, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Rouseff, Jella, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PTE-5DB-5SPB-1OV-101OV-101
Column length (m) 60.30.30.50.50.
Carrier gas H2HeHeN2N2
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (μm) 0.30.250.25  
Tstart (C) 60.60.50.80.80.
Tend (C) 285.240.250.200.200.
Heat rate (K/min) 4.33.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1177.1177.1156.1167.1167.
ReferenceStojanovic, Palic, et al., 2001Tellez M., Estell R., et al., 2001Vijayanand, Rao, et al., 2001Yang, 2001Yang, 2001, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-1HP-5DB-1
Column length (m) 25.60.30.30.25.
Carrier gas  N2 HeNitrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.50
Phase thickness (μm) 0.150.250.25 0.25
Tstart (C) 50.60.45.80.60.
Tend (C) 230.220.300.200.220.
Heat rate (K/min) 3.3.15.9.5.
Initial hold (min)  5.2.  
Final hold (min)  22.5.10. 
I 1159.1171.1205.1174.1166.
ReferenceAsekun and Ekundayo, 2000Bailac, Dellacasa, et al., 2000Hedin, McKibben, et al., 2000Lis-Balchin and Roth, 2000Mallavarapu, Rao, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1HP-5DB-1DB-5
Column length (m) 30.25.30.30.60.
Carrier gas N2N2HeHeHydrogen or helium (He2 wrote in original paper)
Substrate      
Column diameter (mm) 0.220.330.250.250.25
Phase thickness (μm) 0.251.00.250.250.30
Tstart (C) 70.60.60.40.60.
Tend (C) 230.275.275.260.285.
Heat rate (K/min) 4.4.4.2.4.3
Initial hold (min) 2.  5. 
Final hold (min) 20.  2. 
I 1175.1177.1176.1158.1177.
ReferenceMitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2Senatore, Napolitano, et al., 2000Simic, Andjelkovic, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5SE-30OV-101SPB-1
Column length (m) 50.30.25.25.50.
Carrier gas NitrogenHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.20.250.2
Phase thickness (μm)  0.25  0.33
Tstart (C) 40.60.60.50.60.
Tend (C) 200.240.230.200.260.
Heat rate (K/min) 2.3.3.5.4.
Initial hold (min) 10.    
Final hold (min)      
I 1170.1178.1161.1170.1168.
ReferenceTamura, Boonbumrung, et al., 2000Tellez, Dayan, et al., 2000Ali N.A.M. and Jantan, 1999Ayedoun, Adéoti, et al., 1999Choo, Wong, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30RTX-1DB-1OV-101CBP-1
Column length (m) 30.30.25.25.25.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.250.250.320.3
Phase thickness (μm) 0.250.250.25  
Tstart (C) 60.60.50.50.60.
Tend (C) 220.300.290.200.240.
Heat rate (K/min) 4.4.4.5.4.
Initial hold (min) 10.    
Final hold (min)      
I 1164.1170.1177.1170.1166.
ReferenceJassbi, Ahmad, et al., 1999Kalemba, 1999Koulman, 1999Kuiate, Zollo, et al., 1999Labuckas, Zygadlo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1BP-1OV-101SE-30OV-1
Column length (m) 25.25.50.25.25.
Carrier gas H2N2N2HeH2
Substrate      
Column diameter (mm) 0.320.500.20.20.25
Phase thickness (μm) 0.170.25  0.25
Tstart (C) 40.60.80.60.40.
Tend (C) 260.220.200.230.220.
Heat rate (K/min) 3.5.1.3.3.
Initial hold (min) 5.  10.5.
Final hold (min)  10.20. 5.
I 1160.1166.1173.1161.1158.
ReferenceLopes, Koketsu, et al., 1999Mallavarapu, Kulkarni, et al., 1999Menon, Chacko, et al., 1999Mohd and Jantan, 1999Oberhofer, Nikiforov, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1OV-101DB-5SE-30
Column length (m) 25.50.50.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.250.20
Tstart (C) 50.70.70.40.60.
Tend (C) 230.240.220.250.200.
Heat rate (K/min) 3.4.2.2.3.
Initial hold (min)   5.5.4.
Final hold (min)    60. 
I 1160.1152.1165.1148.1181.
ReferenceOyedeji, Olawore, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Pateira, Nogueira, et al., 1999Porta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBDB-1DB-5DB-1
Column length (m) 25.25.60.30.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.390.390.250.25 
Tstart (C) 60.60.40.40.60.
Tend (C) 220.220.280.220.230.
Heat rate (K/min) 5.5.4.4.3.
Initial hold (min) 5. 5.5. 
Final hold (min) 20.   5.
I 1166.1167.1164.1177.1168.
ReferenceRustaiyan, Masoudi, et al., 1999Rustaiyan and Nadji, 1999Sefidkon, Dabiri, et al., 1999Sefidkon and Khajavi, 1999Shafiee, Javidnia, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101SPB-5CP Sil 5 CBDB-5
Column length (m) 30.25.60.25.30.
Carrier gas HeNitrogenHeN2He
Substrate      
Column diameter (mm) 0.250.200.32 0.25
Phase thickness (μm) 0.25 1.0.390.25
Tstart (C) 60.60.40.60.60.
Tend (C) 240.220.200.220.240.
Heat rate (K/min) 3.4.3.5.3.
Initial hold (min)  0.5.  
Final hold (min)  0.2.  
I 1177.1169.1192.1170.1177.
ReferenceTellez, Canel, et al., 1999Tropnikova, Zenkevich, et al., 1999Viallon C., Verdier-Metz I., et al., 1999Weyerstahl, Marschall, et al., 1999Zoghbi, Andrade, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSPB-5SE-30OV-1CBP-1
Column length (m) 30.50.25.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.20.320.25
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.180.250.240.
Heat rate (K/min) 3.3.3.10.4.
Initial hold (min)   10.5. 
Final hold (min)  20. 20. 
I 1174.1179.1166.1166.1177.
ReferenceZoghbi, Andrade, et al., 1999, 2Doneanu and Anitescu, 1998Jantan, Ahmad, et al., 1998Kökdil, Kurucu, et al., 1998Lamarque, Maestri, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-101HP-101HP-1HP-5
Column length (m) 30.25.25.25.25.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.20.20.320.2
Phase thickness (μm) 0.250.20.2 0.33
Tstart (C) 60.70.70.35.70.
Tend (C) 240.200.200.250.290.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)  2.2. 8.
Final hold (min)  10.10. 20.
I 1179.1163.1168.1160.1178.
ReferenceMaia, Zohhbi, et al., 1998Milso, Mastelic, et al., 1998Milso, Mastelic, et al., 1998Ong and Acree, 1998Poiana, Sicari, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBOV-1
Column length (m) 25.25.25.25.30.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.32
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.50.50.60.40.
Tend (C) 200.290.290.300.270.
Heat rate (K/min) 5.4.4.6.2.
Initial hold (min)     4.
Final hold (min)      
I 1170.1154.1154.1154.1172.
ReferenceZollo, Biyiti, et al., 1998Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Kökdil, Kurucu, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-5CBP-1HP-1
Column length (m)  30.30.25.23.
Carrier gas  HeliumHeHeHe
Substrate      
Column diameter (mm)  0.250.250.220.32
Phase thickness (μm)  0.25  0.17
Tstart (C) 80.60.60.60.60.
Tend (C) 220.240.240.240.250.
Heat rate (K/min) 6.3.4.5.5.
Initial hold (min)     3.
Final hold (min)     30.
I 1148.1177.1176.1166.1158.
ReferenceSalgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Ayedoun, Adeoti, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101BP-1BP-1DB-5
Column length (m) 50.50.25.25.30.
Carrier gas N2HeN2N2 
Substrate      
Column diameter (mm) 0.250.250.500.500.25
Phase thickness (μm) 0.17    
Tstart (C) 50.50.60.60.40.
Tend (C) 220.250.220.220.210.
Heat rate (K/min) 5.2.5.5.2.
Initial hold (min)     2.
Final hold (min)     33.
I 1179.1159.1166.1167.1178.
ReferenceChacko, Jayalekshmy, et al., 1996Orav, Kailas, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Sohounhloue, Dangou, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1SPB-1DB-1DB-1DB-1
Column length (m) 25.50.60.60.60.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.320.20.250.320.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 60.40.80.80.70.
Tend (C) 220.200.210.210.270.
Heat rate (K/min) 4.3.3.4.2.5
Initial hold (min) 2.3.  5.
Final hold (min) 20.30.   
I 1158.1161.1175.1175.1168.
ReferenceThanh, Dung, et al., 1996Wong and Lai, 1996Nishimura, 1995Nishimura, 1995, 2Tirado, Stashenko, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5Methyl SiliconeMethyl SiliconeCP Sil 5 CB
Column length (m)   50.50.25.
Carrier gas   N2N2 
Substrate      
Column diameter (mm)   0.250.250.25
Phase thickness (μm)   0.170.17 
Tstart (C) 40.40.80.80.60.
Tend (C) 210.210.200.200.280.
Heat rate (K/min) 2.2.2.3.5.
Initial hold (min)      
Final hold (min)      
I 1176.1177.1175.1170.1167.
ReferenceCollin, Deslauriers, et al., 1993Collin, Deslauriers, et al., 1993Gopalakrishnan, Menon, et al., 1993Gopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-101OV-101OV-101DB-1
Column length (m) 25.50.50.52.60.
Carrier gas    HeliumHe
Substrate      
Column diameter (mm) 0.500.250.250.260.32
Phase thickness (μm)     1.2
Tstart (C) 60.80.80.40.30.
Tend (C) 220.200.200.200.240.
Heat rate (K/min) 5.2.2.3.3.
Initial hold (min)    0.10.
Final hold (min)    0. 
I 1170.1167.1169.1161.1160.
ReferenceMallavarapu, Ramesh, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Tkachenko and Zenkevich, 1993Ciccioli, Cecinato, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-1DB-1CP Sil 8 CBRSL-150
Column length (m) 30.30.60.25.30.
Carrier gas HydrogenN2   
Substrate      
Column diameter (mm) 0.25 0.320.200.32
Phase thickness (μm) 0.25   0.20
Tstart (C) 60.80.50.60.30.
Tend (C) 250.220.230.230.200.
Heat rate (K/min) 2.4.4.3.3.
Initial hold (min) 5.  10. 
Final hold (min) 2. 10.  
I 1174.1155.1159.1182.1161.
ReferenceKollmannsberger, Nitz, et al., 1992Velasco-Negueruela, Pérez Alonso, et al., 1991Binder, Benson, et al., 1990Jantan and Goh, 1990Ronse and De Pooter, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101DB-1BP-1
Column length (m) 25.50.50.60.50.
Carrier gas  N2N2 H2
Substrate      
Column diameter (mm) 0.330.250.250.320.30
Phase thickness (μm)      
Tstart (C) 45.80.80.50.40.
Tend (C) 180.200.200.250.250.
Heat rate (K/min) 3.2.2.4.10.
Initial hold (min) 3.  0.11.
Final hold (min)    5. 
I 1161.1168.1169.1160.1166.
ReferenceWyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder and Flath, 1989Brophy, Davies, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30OV-101OV-101OV-101DB-1
Column length (m) 40.50.50.50.60.
Carrier gas HeN2N2N2He
Substrate      
Column diameter (mm) 0.500.250.250.250.32
Phase thickness (μm) 0.75    
Tstart (C) 30.80.80.80.30.
Tend (C) 220.200.200.200.210.
Heat rate (K/min) 3.2.2.2.2.
Initial hold (min)     4.
Final hold (min)      
I 1163.1169.1166.1169.1158.
Referencede Pooter, de Buyck, et al., 1989Sugisawa, Yamamoto, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Takeoka and Butter, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-1OV-1OV-101OV-101
Column length (m) 60.50.60.50.50.
Carrier gas HeHeHelium  
Substrate      
Column diameter (mm) 0.320.200.500.300.30
Phase thickness (μm)  0.201.2  
Tstart (C) 30.30.40.40.40.
Tend (C) 210.220.220.230.230.
Heat rate (K/min) 2.2.2.3.53.5
Initial hold (min) 4.  5.5.
Final hold (min)      
I 1159.1161.1161.1159.1170.
ReferenceTakeoka and Butter, 1989de Pooter, Nicolai, et al., 1988Wahab, Aboutabl, et al., 1987Nykanen, 1986Nykanen, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-1OV-1OV-101OV-101
Column length (m) 50.40. 30.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.300.5 0.50.31
Phase thickness (μm)  0.75 0.8 
Tstart (C) 40.30.40.40.0.
Tend (C) 230.220.220.220.225.
Heat rate (K/min) 3.53.2.2.3.
Initial hold (min) 5.   1.
Final hold (min)      
I 1183.1162.1164.1165.1156.
ReferenceNykanen, 1986de Pooter, de Buyck, et al., 1986De Pooter, De Buyck, et al., 1986De Pooter and Schamp, 1986del Rosario, de Lumen, et al., 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1SE-30+IgepalSE-30+Igepal
Column length (m) 60.100.100.
Carrier gas    
Substrate    
Column diameter (mm) 0.320.250.25
Phase thickness (μm)    
Tstart (C) 50.70.70.
Tend (C) 250.170.170.
Heat rate (K/min) 4.1.1.
Initial hold (min) 0.1  
Final hold (min) 5.  
I 1159.1172.1175.
ReferenceFlath, Mon, et al., 1983Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Velickovic, D.T.; Ristic, M.S.; Karabegovic, I.T.; Stojicevic, S.S.; Lazic, M.L., The influence of the distillation method on the chemical composition of the essential oil of sage (Salvia officinalis L.), Advanced Technologies, 2012, 1, 1, 47-51. [all data]

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Edris, A.E.; Farrag, E.S., Antifungal activity of peppermint and sweet basil essential oils and their major aroma constituents on some plant pathogenic fungi from the vapor phase, Nahrung/Food, 2003, 47, 2, 117-121, https://doi.org/10.1002/food.200390021 . [all data]

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Kim and Lee, 2002
Kim, N.-S.; Lee, D.-S., Comparison of different extraction methods for the analysis of fragrances from Lavandula species by gas chromatography-mass spectrometry, J. Chromatogr. A, 2002, 982, 1, 31-47, https://doi.org/10.1016/S0021-9673(02)01445-0 . [all data]

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Lin, J.; Rouseff, R.L.; Barros, S.; Naim, M., Aroma composition changes in early season grapefruit juice produced from thermal concentration, J. Agric. Food Chem., 2002, 50, 4, 813-819, https://doi.org/10.1021/jf011154g . [all data]

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Sefidkon, 2002
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Chiasson, Bélanger, et al., 2001
Chiasson, H.; Bélanger, A.; Bostanian, N.; Vincent, C.; Poliquin, A., Acaricidal properties of Artemisia absinthium and Tanacetum vulgare (Asteraceae) essential oils obtained by three methods of extraction, J. Econ. Entomol., 2001, 94, 1, 167-171, https://doi.org/10.1603/0022-0493-94.1.167 . [all data]

Dabiri and Sefidkon, 2001
Dabiri, M.; Sefidkon, F., Analysis of the essential oil from aerial parts of Perovskia atriplicifolia Benth. at different stages of plant growth, Flavour Fragr. J., 2001, 16, 6, 435-438, https://doi.org/10.1002/ffj.988 . [all data]

Flamini, Cioni, et al., 2001
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Koulman, 1999
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Pateira, L.; Nogueira, T.; Antunes, A.; Venancio, F.; Tavares, R.; Capelo, J., Two chemotypes of Crithmum maritimum L. from Portugal, Flavour Fragr. J., 1999, 14, 5, 333-343, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<333::AID-FFJ839>3.0.CO;2-V . [all data]

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Porta, G.D.; Porcedda, S.; Marongiu, B.; Reverchon, E., Isolation of eucalyptus oil by supercritical fluid extraction, Flavour Fragr. J., 1999, 14, 4, 214-218, https://doi.org/10.1002/(SICI)1099-1026(199907/08)14:4<214::AID-FFJ814>3.0.CO;2-H . [all data]

Prikhod'ko, Klyuev, et al., 1999
Prikhod'ko, A.B.; Klyuev, N.A.; Volkovich, S.V.; Emets, T.I.; Petrenko, V.V.; Dolya, E.V., Component composition od the essential oil of Thymus dimorphus, Chem. Nat. Comp., 1999, 35, 1, 46-51, https://doi.org/10.1007/BF02238208 . [all data]

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Rustaiyan, A.; Masoudi, S.; Monfared, A.; Komeilizadeh, H., Volatile constituents of three Salvia species grown wild in Iran, Flavour Fragr. J., 1999, 14, 5, 276-278, https://doi.org/10.1002/(SICI)1099-1026(199909/10)14:5<276::AID-FFJ825>3.0.CO;2-Y . [all data]

Rustaiyan and Nadji, 1999
Rustaiyan, A.; Nadji, K., Composition of the essential oils of Nepeta ispahanica Boiss. and Nepeta binaludensis Jamzad from Iran, Flavour Fragr. J., 1999, 14, 1, 35-37, https://doi.org/10.1002/(SICI)1099-1026(199901/02)14:1<35::AID-FFJ776>3.0.CO;2-N . [all data]

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Sefidkon, F.; Dabiri, M.; Rahimi-Bidgoly, A., The effect of distillation methods and stage of plant growth on the essential oil content and composition of Thymus kotschyanus Boiss. Hohen, Flavour Fragr. J., 1999, 14, 6, 405-408,