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1-Nitropyrene

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spec Data Center, S.E. Stein, director

Lee's RI, non-polar column, temperature ramp

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Column typeActive phaseIReferenceComment
CapillaryHP-5421.53Pedersen, Durant, et al., 200530. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 1.5 min, 6. K/min, 310. C @ 10. min
CapillarySPB-5420.6Knobloch and Engewald, 199340. C @ 2. min, 4. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 300. C
CapillarySE-52421.48Boenke and Ballschmiter, 1987Hydrogen, 3. K/min; Column length: 12. m; Tstart: 120. C; Tend: 285. C
CapillarySE-52421.08White, Robbat, et al., 198330. m/0.3 mm/0.25 «mu»m, He, 4. K/min; Tstart: 25. C; Tend: 295. C
CapillarySE-52421.13White, Robbat, et al., 198330. m/0.3 mm/0.25 «mu»m, He, 4. K/min; Tstart: 100. C; Tend: 300. C
CapillarySE-52421.18White, Robbat, et al., 198330. m/0.3 mm/0.25 «mu»m, He, 4. K/min; Tstart: 40. C; Tend: 300. C
CapillarySE-52421.39White, Robbat, et al., 198330. m/0.3 mm/0.25 «mu»m, He, 4. K/min; Tstart: 70. C; Tend: 300. C
CapillarySE-52421.48Vassilaros, Kong, et al., 198220. m/0.30 mm/0.25 «mu»m, H2, 40. C @ 2. min, 4. K/min; Tend: 265. C

Lee's RI, non-polar column, custom temperature program

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Column typeActive phaseIReferenceComment
CapillaryDB-5419.25Ciccioli, Cecinato, et al., 1988Column diameter: 0.32 mm; Phase thickness: 1.0 «mu»m; Program: 30 0C 20 0C/min -> 180 0C (3 min) 3 0C/min -> 270 0C
CapillaryDB-5421.08Ciccioli, Cecinato, et al., 1988Column diameter: 0.32 mm; Phase thickness: 1.0 «mu»m; Program: not specified
CapillaryDB-5421.26Ciccioli, Cecinato, et al., 1988Column diameter: 0.32 mm; Phase thickness: 1.0 «mu»m; Program: not specified
CapillaryDB-5421.27Ciccioli, Cecinato, et al., 1988Column diameter: 0.32 mm; Phase thickness: 1.0 «mu»m; Program: not specified
CapillaryOV-101425.5Tucminen, Wickstrom, et al., 1986Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Pedersen, Durant, et al., 2005
Pedersen, D.U.; Durant, J.L.; Taghizadeh, K.; Hemond, H.F.; Lafleur, A.L.; Cass, G.R., Human cell mutagenes in respirable airborne particles from the Northeastern United States. 2. Quantification of mutagenes and other organic compounds., Environ. Sci. Technol., 2005, 39, 24, 9547-9560. [doi:10.1021/es050886c] [all data]

Knobloch and Engewald, 1993
Knobloch, T.; Engewald, W., Identification of some polar polycyclic compounds in emissions from brown-coal-fired residential stoves, J. Hi. Res. Chromatogr., 1993, 16, 4, 239-242. [doi:10.1002/jhrc.1240160407] [all data]

Boenke and Ballschmiter, 1987
Boenke, A.; Ballschmiter, K., Fused quinones as retention index marker in high resolution gas chromatography with electron-capture detection (HRGC/ECD) of oxidized aromatic compounds, Fresenius J. Anal. Chem., 1987, 327, 1, 44-45. [doi:10.1007/BF00474554] [all data]

White, Robbat, et al., 1983
White, C.M.; Robbat, A., Jr.; Hoes, R.M., Gas chromatographic retention characteristics of nitrated polycyclic aromatic hydrocarbons on SE-52, Chromatographia, 1983, 17, 11, 605-612. [doi:10.1007/BF02261944] [all data]

Vassilaros, Kong, et al., 1982
Vassilaros, D.L.; Kong, R.C.; Later, D.W.; Lee, M.L., Linear retention index system for polycyclic aromatic compounds. Critical evaluation and additional indices, J. Chromatogr., 1982, 252, 1-20. [doi:10.1016/S0021-9673(01)88394-1] [all data]

Ciccioli, Cecinato, et al., 1988
Ciccioli, P.; Cecinato, A.; Brancaleoni, E.; Liberti, A., Short capillary column for the separation and identification of mononitrofluoranthene and mononitropyrene isomers present in air and emission samples, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1988, 11, 4, 306-312. [doi:10.1002/jhrc.1240110402] [all data]

Tucminen, Wickstrom, et al., 1986
Tucminen, A.; Wickstrom, K.; Pyysalo, H., Determination of Polycyclic Aromatic Compounds by GLC-Selected Ion Monitoring (SIM) Technique, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 8, 469-471. [doi:10.1002/jhrc.1240090813] [all data]


Notes

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