5-acetyl-2,3-1H-pyrrolizine
- Formula: C9H11NO
- Molecular weight: 149.1897
- IUPAC Standard InChI: InChI=1S/C9H11NO/c1-7(11)9-5-4-8-3-2-6-10(8)9/h4-5H,2-3,6H2,1H3
- IUPAC Standard InChIKey: NWSCEJHRUVCUSX-UHFFFAOYSA-N
- CAS Registry Number: 55041-85-5
- Chemical structure:
This structure is also available as a 2d Mol file - Other names: 5-acetyl-2,3-dihydro-1H-pyrrolizine; 5-acetyl-2,3-dihydro-lH-pyrrolizine
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Gas Chromatography
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Normal alkane RI, non-polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | DB-1 | 1335. | Buttery, Ling, et al., 1997 | 30. C @ 25. min, 4. K/min, 200. C @ 20. min; Column length: 60. m; Column diameter: 0.25 mm |
| Capillary | DB-1 | 1382. | Chen, Lu, et al., 1997 | He, 4. K/min; Column length: 60. m; Column diameter: 0.32 mm; Tstart: 50. C; Tend: 280. C |
| Capillary | OV-101 | 1354. | Roberts and Acree, 1994 | 12. m/0.32 mm/0.52 μm, 35. C @ 3. min, 4. K/min; Tend: 225. C |
Normal alkane RI, polar column, temperature ramp
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Carbowax 20M | 2033. | Roberts and Acree, 1994 | 25. m/0.32 mm/0.3 μm, 35. C @ 3. min, 4. K/min; Tend: 200. C |
| Capillary | Carbowax 20M | 2021. | Tressl, Rewicki, et al., 1985 | 2. K/min; Column length: 25. m; Column diameter: 0.32 mm; Tstart: 70. C; Tend: 180. C |
Normal alkane RI, polar column, custom temperature program
| Column type | Active phase | I | Reference | Comment |
|---|---|---|---|---|
| Capillary | Carbowax 20M | 2021. | Peppard and Ramus, 1988 | He; Program: not specified |
References
Go To: Top, Gas Chromatography, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Buttery, Ling, et al., 1997
Buttery, R.G.; Ling, L.C.; Stern, D.J.,
Studies on popcorn aroma and flavor volatiles,
J. Agric. Food Chem., 1997, 45, 3, 837-843, https://doi.org/10.1021/jf9604807
. [all data]
Chen, Lu, et al., 1997
Chen, C.-W.; Lu, G.; Ho, C.-T.,
Generation of proline-specific Maillard compounds by the reaction of 2-deoxyglucose with proline,
J. Agric. Food Chem., 1997, 45, 8, 2996-2999, https://doi.org/10.1021/jf970197n
. [all data]
Roberts and Acree, 1994
Roberts, D.D.; Acree, T.E.,
Gas chromatography - olfactometry of glucose - proline Maillard reaction products
in American Chemical Society, Symposium Series -- Volume 543, American Chemical Society, Washington, 1994, 71-79. [all data]
Tressl, Rewicki, et al., 1985
Tressl, R.; Rewicki, D.; Helak, B.; Kamperschröer, H.; Martin, N.,
Formation of 2,3-dihydro-1H-pyrrolizines as proline specific Maillard products,
J. Agric. Food Chem., 1985, 33, 5, 919-923, https://doi.org/10.1021/jf00065a036
. [all data]
Peppard and Ramus, 1988
Peppard, T.L.; Ramus, S.A.,
Use of Kovats' gas chromatographic retention indices in beer flavor studies,
Am. Soc. Brew. Chem. Proc., 1988, 46, 2, 26-30. [all data]
Notes
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- Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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